A method for improving the dispersion of silica airgel in aqueous phase by atomization adsorption
A technology of silica and aerogel water, which is applied in chemical instruments and methods, climate sustainability, dyeing low molecular organic compound treatment, etc. performance, increased fire hazard, etc.
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Embodiment 1
[0025] A kind of atomization adsorption that the present invention proposes improves the method for silica airgel aqueous phase dispersibility, comprises the following steps:
[0026] S1, refine the silica airgel powder, and obtain the refined airgel after sieving;
[0027] S2. Atomize the organic solvent with a density greater than water, and then transport it from the top of the closed container into the closed container to form a coating reagent, and then evenly disperse the refined airgel in the closed container to form a powder mist, so that the powder mist Adsorbing the coating reagent to obtain a coated airgel; wherein, the bottom of the closed container is equipped with an aqueous dispersant solution, and is provided with a stirring device and an air blowing device;
[0028] S3. The airgel to be coated sinks to the surface of the dispersant aqueous solution, and the coated airgel with a density greater than or equal to water is stirred and dispersed in the aqueous solu...
Embodiment 2
[0030] A kind of atomization adsorption that the present invention proposes improves the method for silica airgel aqueous phase dispersibility, comprises the following steps:
[0031] S1. Put the silica airgel powder into the ball mill tank, add four kinds of agate balls with particle diameters of 8mm, 11mm, 14mm, and 20mm respectively, set the speed at 100r / min, and mill for 4h for refinement. Obtain fine airgel after sieving;
[0032] S2. Use a pressurized delivery pump to atomize 25mL of dichloromethane, and then add it from the top to the airtight container to disperse to form a coating reagent; use a powder delivery pump to transport 1g of refined airgel and evenly disperse it in the airtight container Forming a powder mist, so that the powder mist absorbs the coating reagent to obtain a coated airgel; wherein, the bottom of the airtight container is equipped with an aqueous solution of polyoxyethylene sorbitan monolaurate, and is provided with a stirring device, and on t...
Embodiment 3
[0036] A kind of atomization adsorption that the present invention proposes improves the method for silica airgel aqueous phase dispersibility, comprises the following steps:
[0037] S1. Put the silica airgel powder into the ball mill tank, add four kinds of balls with particle diameters of 8mm, 11mm, 14mm, and 20mm respectively, set the speed at 300r / min, mill for 2h to refine, and sieve Finally, a refined airgel is obtained;
[0038]S2. Use a pressurized delivery pump to atomize 15mL of carbon disulfide, then add it from the top into a closed container to disperse to form a coating reagent; use a powder delivery pump to transport 1g of refined airgel and evenly disperse it in a closed container to form a powder Body mist, so that the powder mist absorbs the coating reagent to obtain the coated aerogel; wherein, the bottom of the airtight container is equipped with a sodium stearate aqueous solution, and is provided with a stirring device and an air blowing device;
[0039]...
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