8784 results about "SILICONE DIOXIDE" patented technology

A method of continuous 3D printing to print an article is provided. The method includes displacing a nozzle of the 3D printer in a nozzle displacement direction; extruding the ink from the nozzle concurrently with the displacement of the nozzle to form an extrudate on the porous substrate; and displacing the rotating magnetic field in the nozzle displacement direction simultaneously with the displacement of the nozzle. The ink includes a plurality of magnetically responsive particles and a colloidal gel. The colloidal gel may include fumed silica in an aqueous solution.

The invention belongs to the technical field of polymer plastic materials, and particularly relates to a high-temperature-resistant anti-corrosion polytetrafluoroethylene material and a preparation method thereof. The polytetrafluoroethylene is prepared from the following raw materials in parts by weight: 50 to 60 parts of polytetrafluoroethylene, 5 to 10 parts of fluorinated modified graphene oxide, 3 to 5 parts of aluminum powder, 5 to 8 parts of modified silicon carbide fiber, 3 to 5 parts of silane modified nano silicon dioxide, 2 to 3 parts of polyphenylene sulfide, 2 to 3 parts of polyimide, 0.5 to 0.8 part of dispersing agent and 0.5 to 1 part of antioxidant. The heat conduction performance and the interface bonding force are improved through the fluorinated modified graphene oxide, the impact resistance and the wear resistance are enhanced through the silicon carbide fibers, and the corrosion resistance and the wear resistance are improved through the aluminum powder; silane modified silicon dioxide enhances the mechanical property of the composite material by improving the dispersity of the filler, and PPS and PI interact with the surface of the filler through polar groups in molecular chains, so that the interface strength is improved, and the toughness and the thermal stability are improved.

The invention relates to the field of pressure sensors, in particular to a pressure sensor and a processing method, and a chip comprises a silicon substrate, a silicon dioxide dielectric layer, a device layer, a metal electrode and packaging glass. The device layer comprises a silicon carbide single crystal device layer and a silicon device layer; the silicon carbide single crystal device layer is arranged on the silicon device layer; the silicon device layer, the silicon dioxide dielectric layer and the silicon substrate are connected in sequence; the device layer is etched to form a sensitive resistor device layer, an annular sealing region and a micro-channel; the sensitive resistance device layer is isolated from the annular sealing area through the micro-channel; the device layer, the silicon dioxide dielectric layer and the silicon substrate are etched to form a cross beam etching area; the silicon substrate is etched to form a silicon pressure cavity and a beam film; the metal electrode is arranged on the top of the device layer; and the packaging glass anode is bonded at the top of the device layer or the bottom of the silicon substrate so as to solve the problems of low high temperature resistance and low sensitivity of the MEMS pressure sensor.

The invention relates to the technical field of folding screen supporting films, and particularly discloses a double-layer buffering supporting film for a flexible folding display screen and a preparation method of the double-layer buffering supporting film. The double-layer buffer supporting film for the flexible folding display screen sequentially comprises a release film layer, a first adhesive layer, a first stainless steel layer, a second adhesive layer, a second stainless steel layer and a protective film layer from top to bottom, the first adhesive layer and the second adhesive layer are prepared by curing the same pressure-sensitive adhesive composition; the pressure-sensitive adhesive composition is prepared from the following raw materials: acrylate copolymer, hydrogenated rosin glyceride, hyperbranched polyesteramide-dopamine conjugate, acylhydrazone bond modified siloxane, a curing agent and a silane coupling agent; the protective film layer comprises the following raw materials: PET particles, nano silicon dioxide, an ethylene-vinyl acetate copolymer and an antioxidant. The double-layer buffer supporting film has the advantages of being high in supporting rigidity and interlayer peel strength, and serious folds caused by long-term repeated folding of the folding screen can be relieved.

The invention provides a preparation method of a porous carbon-silicon composite negative electrode material of a lithium battery. The preparation method comprises the following steps: constructing a multi-stage template system; carrying out carbon precursor impregnation and gradient temperature carbonization on the multistage template system; removing the template to form a gradient porous carbon carrier; carrying out gradient temperature zone silane deposition; and plasma-assisted carbon coating and nitrogen doping are carried out. According to the method, a silicon dioxide sphere hard template is combined with cetyltrimethylammonium bromide and a block copolymer soft template to form a porous carbon carrier with a micropore-mesopore-macropore three-stage structure, and gradient distribution of silicon in porous carbon is realized by utilizing a three-temperature-zone fluidized bed reactor and a pulse type deposition technology, so that the silicon-based porous carbon composite material is obtained. The problem of volume expansion of the silicon material is effectively relieved and the material cycling stability is improved. The porous carbon-silicon composite negative electrode material prepared by the invention has high specific surface area, excellent ion transmission channel and good structural stability, and can be applied to a high-energy-density lithium ion battery.

The invention discloses heat-resistant high borosilicate glass and a preparation method thereof, and belongs to the technical field of glass production, and the heat-resistant high borosilicate glass specifically comprises the following components in parts by weight: 66-83 parts of silicon dioxide, 15-25 parts of diboron trioxide, 5-9 parts of sodium oxide, 2-4 parts of aluminum oxide, 1-4 parts of a composite fluxing agent, 0.5-1.5 parts of a composite clarifying agent and 2-6 parts of a high heat-resistant modifier. The heat-resistant high borosilicate glass obtained by the invention has a linear thermal expansion coefficient of 3.15-3.31 * 10 <-6 > / K, a thermal shock resistance cycle number of 32-37, and a thermal shock resistance cycle upper limit temperature of 590-610 DEG C.

The invention relates to the technical field, and particularly discloses a nano-modified epoxy building thermal insulation material and a preparation method thereof. The nano modified epoxy building thermal insulation material is prepared from the following raw materials in parts by mass: 80 to 120 parts of Portland cement, 20 to 40 parts of slag powder, 5 to 10 parts of hollow mesoporous silicon dioxide, 0.1 to 1 part of pyrrole, 0.1 to 0.2 part of ammonium persulfate, 5 to 10 parts of nano silicon dioxide, 10 to 15 parts of bisphenol S epoxy resin, 1 to 5 parts of acrylic acid, 1 to 2 parts of polylysine, 0.01 to 0.1 part of catalyst and 1 to 2 parts of curing agent. The concrete is prepared from the following raw materials in parts by weight: 20-30 parts of epoxy resin, 4-8 parts of loaded aerogel, 0.1-1 part of polycarboxylate superplasticizer, 1-4 parts of composite fiber and 0.2-1.25 parts of hydrogen peroxide. The fireproof building material has excellent toughness, can better resist cracking and absorb energy, effectively avoids cracking and damage under the action of thermal stress, and ensures that the building material has a fireproof effect.

The invention discloses an MEMS device architecture, which comprises a cap layer, a device layer and a substrate layer, the cap layer is bonded with the device layer, the bonded whole is bonded with the substrate layer, the cap layer is manufactured based on a first silicon substrate, the bottom of the cap layer is provided with a cavity structure, and the cap layer is internally provided with a high-deep groove structure. A silicon dioxide film is arranged on the groove wall of the high-deep groove structure, polycrystalline silicon is deposited and filled in the high-deep groove structure, and a silicon dioxide layer is arranged on the upper surface of the first silicon substrate; the device layer is manufactured based on an SOI wafer and comprises a first silicon structure layer composed of top layer silicon, a buried oxide layer and a second silicon structure layer composed of back substrate silicon. The substrate layer comprises a second silicon substrate, a bottom layer cavity is formed in the top face of the second silicon substrate, and exhaust holes are formed in the bottom face of the second silicon substrate. According to the method, deep groove etching, polycrystalline silicon groove filling and bonding technologies are combined, advanced materials such as the SOI wafer and the polyimide layer are utilized, and excellent signal isolation and flexibility of various MEMS IMU applications are achieved.

The invention provides a hot in-place recycling asphalt mixture and a construction method, and relates to the technical field of asphalt mixtures, and the hot in-place recycling asphalt mixture is obtained by recycling old asphalt pavement materials in a high proportion, reducing new material consumption and carbon emission, realizing resource recycling and green construction and introducing a regenerant to recover the performance of aged asphalt. The high-temperature rut resistance, the low-temperature crack resistance, the fatigue resistance and the interface bonding strength of the mixture are synergistically improved by matching with the styrene butadiene rubber modifier, the basalt fiber, the nano silicon dioxide and other functional materials, and the mixture is ensured to be uniform and free of segregation through precise feeding sequence, high-pressure atomization spraying and forced stirring parameter control. The defects of gray materials, oil balls and the like are avoided, the compactness, the flatness and the overall structure stability of the regenerated pavement are improved, and the problems of performance degradation and insufficient durability of a traditional regenerated mixture are solved.

The invention belongs to the technical field of organic silicon coatings, and discloses a weather-resistant self-cleaning organic silicon coating as well as a preparation method and application thereof. The weather-resistant self-cleaning organic silicon coating is prepared from the following components in parts by weight: 50 to 100 parts of alpha, omega-dihydroxy polysiloxane; 20 to 50 parts of alkoxy modified fluorine-containing polysiloxane; 20 to 30 parts of MQ silicon resin; 0.01 to 0.05 part of a catalyst; and 100 to 250 parts of solvent oil. According to the organic silicon coating disclosed by the invention, specific alkoxy modified fluorine-containing polysiloxane is added as a hydrophobic modifier, so that the hydrophobic self-cleaning effect and adhesive force of a coating film can be remarkably improved. MQ silicon resin is adopted to replace conventional silicon dioxide to serve as reinforcing filler, compatibility of the MQ silicon resin and a silicon rubber matrix is better, the transparency of a coating film can be remarkably improved, and the application effect of the MQ silicon resin in the surface of a photovoltaic panel is improved.

A composite ozone catalyst, a preparation method and use thereof. The composite ozone catalyst of the present invention includes a co-carrier mixed with biochar and a silica-alumina-based material, and a metal element and a nitrogen element supported on the co-carrier. The preparation method includes mixing the biochar and the silica-alumina-based material powder and then placing the same in a metal precursor solution for impregnation, adding a polyvinyl pyrrolidone solution to the impregnated material, wet granulating to form a spherical material, and calcining the spherical material to obtain the composite ozone catalyst. The composite ozone catalyst has low production cost, simple preparation processes, good catalytic performance, and strong stability, which can meet the high-efficiency and low-consumption requirements of ozone catalytic oxidation in the advanced treatment of industrial wastewater.

The invention relates to a multi-layer composite black film and a preparation method thereof. The multi-layer composite black film is formed by sequentially stacking a base material layer, a multi-layer film system and a top covering layer, the multi-layer film system is formed by alternately stacking a plurality of absorption layers and a plurality of oxide layers, the number of the layers is 7-30, an initial layer is an oxide layer, the refractive indexes of the oxide layers are the same (1.4-1.5), the thickness ratio of the oxide layers to the absorption layers is larger than 2, and the thickness ratio of the top covering layer to the absorption layers is larger than 1. And the thicknesses of the two layers are increased and then reduced from the substrate layer to the top covering layer. A buffer layer with gradually changed oxygen content is arranged between the oxide layer and the absorption layer, and both the oxide layer and the top covering layer are made of silicon dioxide. The preparation method comprises the following steps: providing the substrate layer, alternately depositing the absorption layer and the oxide layer by using a magnetron sputtering or electron beam evaporation process to form a multilayer film system, then forming the top covering layer, controlling parameters such as vacuum degree, power, temperature and the like during deposition, and forming the buffer layer in the same cavity. The multilayer composite black film has the inner surface reflectivity of less than 1% and the appearance surface reflectivity of less than 5%, and is simple in structure and low in preparation cost.

The invention discloses a lithium battery diaphragm coating based on a nano material and application thereof, and relates to the technical field of lithium battery diaphragms. The coating comprises the following raw materials in parts by weight: 15-25 parts of polystyrene maleic anhydride copolymer modified polyvinylidene fluoride, 10-20 parts of polystyrene, 2-4 parts of nano silicon nitride, 3-6 parts of a boehmite / aluminum oxide and silicon dioxide composite material, 1-2 parts of a dispersing agent and 65-90 parts of a solvent, according to the lithium battery diaphragm coating provided by the invention, the wettability and absorptivity of a diaphragm to an electrolyte are remarkably improved, meanwhile, the lithium battery diaphragm coating also has excellent thermal stability, and the diaphragm can be effectively prevented from thermal shrinkage or melting under a high-temperature condition, so that the safety performance of a battery is remarkably enhanced.

The invention relates to the technical field of coating materials, and discloses a preparation method of a nano silicon dioxide / fluorocarbon resin durable super-hydrophobic composite coating and application of the nano silicon dioxide / fluorocarbon resin durable super-hydrophobic composite coating on a wind turbine blade. The adhesive force of the coating on the base material is enhanced; in the second step, an inorganic particle-organic resin hybrid state is formed by spraying a super-hydrophobic modified SiO2 dispersion liquid and combining a nano-particle self-settling assembly technology, required roughness and low surface energy are given to the coating, and conversion from hydrophobicity to super hydrophobicity is achieved.

The invention relates to ultrahigh-transmittance anti-reflection multifunctional coated photovoltaic glass and a preparation method thereof, and belongs to the technical field of photovoltaic glass, the photovoltaic glass comprises a photovoltaic glass substrate, the photovoltaic glass substrate is provided with a high-transmittance reflective coating, the high-transmittance reflective coating comprises a silicon dioxide layer, a titanium dioxide layer and a nanometer material layer, and the nanometer material layer is arranged on the silicon dioxide layer. The silicon dioxide layer and the titanium dioxide layer are arranged between the photovoltaic glass substrate and the nanometer material. The preparation method comprises the following steps: S1, preparing raw materials; s2, preparing a coating; s3, coating process; s4, performing surface treatment on the nano structure; s5, coating curing and surface treatment; and S6, testing and evaluating the performance. According to the ultrahigh-transmittance anti-reflection multifunctional coated photovoltaic glass, the performance and durability of a photovoltaic cell can be remarkably improved, by arranging the high-transmittance anti-reflection coating, the light transmittance of the photovoltaic glass is improved, the overall photoelectric conversion efficiency can be improved by 5-8%, and light reflection loss is remarkably reduced.

The invention discloses a high-strength directly-buried optical cable and a preparation method thereof. Comprising at least one reinforcing piece, at least one cable core, a water-blocking tape layer, an inner protective layer, an armor layer and a high-strength outer sheath, wherein the cable core surrounds the reinforcing piece, is twisted and is filled with water-blocking cable paste; the water-blocking tape layer wraps the cable core; the inner protective layer wraps the water-blocking tape layer; wherein the cable core is composed of a loose tube filled with water-blocking fiber paste and at least one light-guide fiber accommodated in the loose tube; wherein the high-strength outer sheath is prepared from the following raw materials in parts by weight: 80 to 85 parts of high-density polyethylene, 15 to 20 parts of nylon 612, 8 to 12 parts of compatilizer, 15 to 20 parts of modified silicon dioxide, 1 to 3 parts of antioxidant and 0.7 to 1.1 parts of lubricant. The high-strength directly-buried optical cable has excellent high strength, aging resistance and wear resistance, the service life of the optical cable is remarkably prolonged, and the transmission reliability of the optical cable is remarkably improved.

The invention provides a doped electrode material based on porous silicon carbon and a preparation method thereof.The preparation method comprises the steps that a resin base material is smashed and then put into a high-temperature furnace to be subjected to a carbonization process, the carbonization temperature ranges from 300 DEG C to 1500 DEG C, an alkaline additive, a phosphorus source material and a nitrogen source material are sequentially added in the temperature interval, and phosphorus-nitrogen co-doped porous carbon is obtained; the preparation method comprises the following steps: mixing a silicon dioxide microsphere template into phosphorus-nitrogen co-doped porous carbon, adding a first coating carbon source to carry out first coating treatment, and etching the silicon dioxide microsphere template by using an etching solution to obtain a prefabricated object with a cavity structure; and putting the prefabricated object with the cavity structure into a fluidized bed reactor, introducing silicon source gas and a surface activation auxiliary agent, carrying out deposition at 400-550 DEG C, and then adding a second coating carbon source to carry out secondary coating treatment, thereby obtaining the doped electrode material based on porous silicon carbon. Therefore, the expansion coefficient of the electrode material is effectively reduced, and the rate capability is improved.

The invention relates to a catalyst for ethylene oxide ring-opening polymerization and a preparation method thereof, and belongs to the technical field of high polymer material synthesis, and the catalyst is a composite structure based on a silicon dioxide nanoparticle loaded bimetal organic complex; a modified nitrogen-containing polydentate ligand is prepared by adopting a special method, is coordinated with metal ions through covalent bonds and is loaded on silicon dioxide nanoparticles; by utilizing the high dispersity and stability of the silicon dioxide nanoparticles and the synergistic catalytic effect of the bimetal organic complex, the catalytic effect is effectively improved, the polymerization process is accelerated, the polymerization stability is enhanced, the polymerization molecular weight is improved, and the distribution is narrow.

The invention relates to a mildew-proof silicone sealant with high curing rate and high adhesive strength, and belongs to the technical field of adhesives. The anti-mildew coating is prepared from alpha, omega-dihydroxy polydimethylsiloxane, dimethyl silicone oil, fumed silica, phenoxy resin coated nano calcium carbonate, a modified hydroxypropyl-gamma-cyclodextrin loaded mildew preventive, dibutyltin dilaurate, methyltrimethoxysilane and a curing accelerator. According to the mildew-proof silicone sealant with the high curing rate and the high adhesive strength, the surface drying time is 9-13 minutes, the 24-hour curing depth is 6.3-7.2 mm, the adhesive strength is 3.0-3.6 MPa, the tensile strength is 5.8-6.4 MPa, the shear strength is 3.0-3.9 MPa, the elongation at break is 410-457%, and the mildew-proof grade is 0 grade in 30 days, 60 days, 180 days and 360 days.

The invention discloses a copper-clad plate for a printed circuit board and a preparation method of the copper-clad plate, and relates to the technical field of printed circuit board materials. The invention discloses a preparation method of a copper-clad plate for a printed circuit board, which comprises the following steps of: soaking a reinforcing material in a glue solution, and drying to obtain a prepreg; carrying out hot-pressing treatment on the prepreg and copper foil to obtain a copper-clad plate; the glue solution comprises the following raw materials in parts by weight: 15-20 parts of vinyl-terminated polyphenyl ether, 20-25 parts of epoxy resin, 20-25 parts of difunctional silicon dioxide, 15-25 parts of an organic solvent, 0.3-0.6 part of a curing agent and 0.05-0.1 part of a curing accelerator; the difunctional silicon dioxide cross-linked polyphenyl ether and epoxy resin prepared by the preparation method disclosed by the invention are used as a resin material of a glue solution, and have the characteristics of good heat resistance and excellent mechanical properties.

The invention relates to the technical field of environmental materials and water treatment, in particular to a graphene amino silica gel composite adsorbent for heavy metal wastewater treatment and a preparation method thereof.The graphene amino silica gel composite adsorbent is prepared from # imgabs0 nanoparticles, an amino-functionalized silicon dioxide coating layer, carboxylated reduced graphene oxide, a polydopamine modification layer and tetraethyl orthosilicate; the coating is prepared from the following raw materials: 3-aminopropyltriethoxysilane, 3-mercaptopropyltrimethoxysilane, N-((4-vinyl benzyl) amino) diacetic acid, chitosan, beta-cyclodextrin, hexadecyl trimethyl ammonium bromide, polyethylene glycol, L-ascorbic acid, 1-ethyl-3-(3-dimethyl aminopropyl) carbodiimide hydrochloride and N-hydroxysuccinimide. The composite adsorbent shows excellent adsorption performance on various heavy metal ions, and the adsorption performance is far higher than that of traditional adsorption materials and existing composite adsorbents.

The invention relates to an aluminum alloy chemical mechanical polishing solution and a preparation method and application thereof.The polishing solution is prepared from, by mass, 20%-30% of grinding materials, 1%-5% of oxidizing agents, 0.01%-1% of complexing agents, 0.01%-1% of pH regulators and the balance deionized water; wherein the complexing agent is a mixture of a first complexing agent and a second complexing agent, the first complexing agent is short-carbon-chain organic acid with the carbon atom number of 2-4, and the second complexing agent is long-carbon-chain organic acid with the carbon atom number of 8-10; the grinding material is a mixture of aluminum oxide and silicon dioxide, and the silicon dioxide is a mixture with the particle size of 10-40 nm, 40-70 nm and 90-110 nm. Compared with the prior art, the method has the advantages that the removal rate can be increased, and the surface roughness of the workpiece is reduced.

The invention provides a back contact solar cell and a preparation method thereof, and relates to the technical field of back contact solar cells. The preparation method of the back contact solar cell comprises the steps that an isolation area, a P area and an N area are arranged on the back face of a silicon wafer, and the isolation area is located between the P area and the N area; forming a silicon dioxide mask layer only on the isolation region; after a silicon dioxide mask layer is formed on the isolation region, a P-type polycrystalline silicon layer is formed in the P region; after a silicon dioxide mask layer is formed on the isolation region, an N-type polycrystalline silicon layer is formed in the N region; and removing the silicon dioxide mask layer after the P-type polycrystalline silicon layer and the N-type polycrystalline silicon layer are formed. According to the scheme, high-temperature diffusion of impurity atoms can be blocked, and the problem that the photoelectric conversion efficiency of the battery is reduced due to the fact that boron and phosphorus impurity atoms exist at the junction of the P region and the N region at the same time is effectively solved.

A core-shell particle having an organic polymer core which is completely covered by a first inorganic oxide shell, wherein the first inorganic oxide shell has a silica (SiO2), an alumina (Al2O3), or a titania (TiO2); wherein the first inorganic oxide shell has a layer of a magnetic material which is disposed directly on the polymer core; further having a mesoporous second inorganic oxide shell, wherein the mesoporous second inorganic oxide shell covers the first inorganic oxide shell; wherein the mesoporous second inorganic oxide shell has silica (SiO2), alumina (Al2O3), or a titania (TiO2).

The invention provides a silicon-carbon composite material as well as a preparation method and application thereof. The silicon-carbon composite material comprises a porous carbon material; the silicon particles are distributed on the surface layer of the porous carbon material and in pore channels in the porous carbon material, the distribution concentration of the silicon particles in the surface layer of the porous carbon material is smaller than that of the silicon particles in the porous carbon material, and the particle size of the silicon particles in the surface layer of the porous carbon material is smaller than that of the silicon particles in the porous carbon material; the silicon dioxide layer is formed on the surface of the silicon particles; and the carbon coating layer is formed on the surface of the silicon dioxide layer. The lithium ion battery prepared by taking the silicon-carbon composite material as a positive electrode active material shows good electrochemical performance, and has relatively high specific capacity, good cycling stability and rate capability.

The invention discloses a preparation method of a permanent red pigment for an acid and alkali resistant coating, and belongs to the technical field of pigment preparation, a 2B acid derivative is diazotized and then coupled with 2-hydroxy-3-naphthoic acid, then a calcium chloride aqueous solution is added for color lake to obtain pigment particles, and finally the surfaces of the pigment particles are coated with silicon dioxide to obtain the permanent red pigment for the acid and alkali resistant coating. According to the permanent red pigment for the acid and alkali resistant coating prepared by the preparation method disclosed by the invention, the acid and alkali resistance and environmental stability of the pigment are further enhanced while the excellent characteristics of original pigment red 48: 2 are maintained, and the application performance of the pigment is remarkably improved.

The invention relates to the field of composite materials, and particularly discloses high-entropy nano ceramic fiber reinforced silicon dioxide aerogel and a preparation method thereof. The high-entropy nano ceramic fiber is successfully prepared through the steps of preparation of a precursor spinning solution, electrostatic spinning, high-temperature cracking, a sol-gel method and the like, and the high-entropy nano ceramic fiber is compounded into silicon dioxide aerogel. According to the invention, high-entropy nano ceramic fibers are compounded in silicon dioxide aerogel. The high-entropy nano ceramic fiber not only can greatly improve the heat insulation property of the silicon dioxide aerogel at high temperature, but also can remarkably improve the mechanical properties such as toughness of the silicon dioxide aerogel, so that the application scene of the material can be widened.

The invention relates to the technical field of high-performance polyester, in particular to a high-strength low-shrinkage polyester fiber and a preparation method thereof. The defects that existing polyester fibers are poor in strength and shrinkage resistance are overcome. The preparation method comprises the following steps: mixing the modified resin, the modified nano silicon dioxide, the composite antioxidant, the composite nucleating agent and the composite lubricant, and carrying out melt spinning. Wherein the modified resin is prepared from the following raw materials: dimethyl terephthalate, isophthalic acid, ethylene glycol and isosorbide; the modified nano silicon dioxide comprises nano silicon dioxide, KH570 and silver nitrate; the composite antioxidant comprises an antioxidant 1010, an antioxidant 168 and an antioxidant 1222; the composite nucleating agent comprises sodium benzoate and nano montmorillonite; the composite lubricant is prepared from ethylene bis stearamide and pentaerythritol stearate. The prepared polyester fiber is high in strength, high in shrinkage resistance and suitable for manufacturing of outdoor equipment.

The invention provides a SiO2 / TiO2 / PMMA radiation refrigeration film and a preparation method thereof, and relates to the technical field of passive daytime radiation refrigeration films. The radiation refrigeration film is prepared from the following raw materials: N, N-dimethylformamide, polymethyl methacrylate, silicon dioxide and titanium dioxide. The invention relates to a preparation method of a SiO2 / TiO2 / PMMA radiation refrigeration film. The preparation method comprises the steps of preparing silicon dioxide, preparing titanium dioxide, synthesizing composite sol and preparing the SiO2 / TiO2 / PMMA radiation refrigeration film. The SiO2 / TiO2 / PMMA radiation refrigeration film prepared by the invention has high reflectivity in the ultraviolet-visible-near infrared band and high emissivity in the infrared band, can realize 8.4 DEG C sub-environment refrigeration, and is low in cost and simple in process flow.

The invention discloses water-based formaldehyde-free woodworking glue and a preparation method thereof, and relates to the technical field of woodworking glue. When the water-based formaldehyde-free woodworking glue is prepared, firstly, n-butyllithium is used as an initiator to initiate cyclosiloxane and an acrylate monomer to be polymerized, then dimethyl chlorosilane is used for blocking to obtain pre-modified polyacrylate, and the pre-modified polyacrylate is used for preparing the water-based formaldehyde-free woodworking glue. Reacting the pre-modified polyacrylate with vinyl diphenylphosphine, and then reacting with 3-(4-bromophenyl)-1-propylene to obtain modified polyacrylate; secondly, reacting the 4-(trimethoxysilyl) butyraldehyde modified silicon dioxide with chitosan, and then reacting with mercaptoacetic acid to obtain modified silicon dioxide; finally, mixing the modified polyacrylate, the modified silicon dioxide, an emulsifier, a defoaming agent, pure water and a photoinitiator to obtain the water-based formaldehyde-free woodworking glue. The water-based formaldehyde-free woodworking glue prepared by the invention has flame retardance and antibacterial property.