The invention relates to the technical field of
chemical production, in particular to a high-purity
nitrous oxide rectification process and rectification device.The high-purity
nitrous oxide rectification process comprises the following steps that firstly, crude
nitrous oxide with the purity being 99.5 wt% is selected and conveyed to a heavy component removal
tower A under conveying of a pump body; 2, the temperature of a hot side inlet of a heavy component removal
tower reboiler C is 40-50 DEG C, the temperature of a hot side outlet of the heavy component removal
tower reboiler C is 30-40 DEG C, the temperature of a
cold side inlet of a heavy component removal tower condenser B is 30-40 DEG C, and the temperature of a
cold side outlet of the heavy component removal tower condenser B is 20-25 DEG C; 3, most nitrous
oxide and other light components are conveyed into a light component removal tower D through a first A outlet of a heavy component removal tower condenser B and a
first light component pipeline; 4, the temperature of a hot side inlet of a light component removal tower
reboiler F is 40-50 DEG C; 5, nitrous
oxide is separated from other light components, and the separated nitrous
oxide enters a light component removal tower condenser E to be condensed; the working efficiency of the heavy component removal tower A and the light component removal tower D is improved, and meanwhile, the purity and the stability of nitrous oxide are improved.