A manganese-based coordination compound with antitumor activity
A technology of coordination compounds and anti-tumor activity, which is applied in the field of preparation of coordination compounds to achieve good anti-tumor activity and simple synthesis method
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[0019] In order to make the content of the present invention easier to understand, the technical solutions of the present invention will be further described below in conjunction with specific embodiments, but the present invention is not limited thereto.
[0020] Dissolve 2.05 mmol of 2,6-pyridinedicarboxylic acid and 1.2 mmol of manganese acetate tetrahydrate in 5 mL of deionized water respectively, then mix them evenly, put them into a stainless steel reaction kettle lined with polytetrafluoroethylene, and keep at 120°C After 5 days of constant temperature reaction, the temperature was naturally lowered, filtered and rinsed with deionized water, and then dried to obtain colorless columnar crystals, which were manganese-based coordination compounds [Mn(C 7 h 3 NO 4 )] H 2 O, the yield is about 34% (calculated as Mn).
[0021] 1. [Mn(C 7 h 3 NO 4 )] H 2 Characterization of O single crystals
[0022] a. The X-ray single crystal diffraction experiment of coordination co...
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