A preparation method of flexible low working voltage polyaniline electrovariable emissivity film
A technology of polyaniline film and working voltage, applied in the direction of electrolytic organic material coating, etc., can solve the problems of high cost, complicated preparation process, high driving voltage, etc., and achieve the effect of high reflection, simple process and high infrared radiation
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specific Embodiment approach 1
[0021] Embodiment 1: This embodiment is a method for preparing a flexible low-voltage polyaniline electrovariable emissivity film, which is completed according to the following steps:
[0022] 1. Preparation of polymer solution:
[0023] At room temperature, dissolving sulfuric acid into deionized water, then adding aniline, and then stirring to obtain a polymer solution;
[0024] The mol ratio of sulfuric acid and aniline in the polymer solution described in step 1 is (1~5):1;
[0025] The volume ratio of the amount of aniline in the polymer solution described in step 1 to deionized water is (0.1mol~0.3mol):(100mL~200mL);
[0026] 2. Electrochemical deposition:
[0027] With the silver / silver chloride electrode as the reference electrode, the platinum electrode as the counter electrode, the gold-plated porous membrane or ITO as the working electrode, and the polymer solution obtained in step 1 as the electrolyte, the CHI660E electrochemical workstation was used to measure t...
specific Embodiment approach 2
[0034] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the mass fraction of sulfuric acid described in step 1 is 80%-98%. Other steps are the same as in the first embodiment.
specific Embodiment approach 3
[0035] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the stirring speed in step 1 is 500r / min-1000r / min, and the stirring time is 30min-35min. Other steps are the same as those in Embodiment 1 or 2.
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