Preparation method of spherical lead oxide atmospheric mineral dust
A lead oxide, spherical technology, applied in the field of atmospheric environmental science, can solve the problems of few preparation methods, harm to human health, unfavorable research on lead oxide atmospheric mineral dust, etc.
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Embodiment 1
[0017] Embodiment 1: the preparation of spherical lead oxide atmospheric mineral dust
[0018] (1) prepare respectively the lead acetate solution of 45mmol / L, the hexamethylenetetramine solution of 45mmol / L, the trisodium citrate solution of 15mmol / L, the molar ratio of the three is 1:1:0.3;
[0019] (2) Mix the prepared lead acetate solution, hexamethylenetetramine solution, and trisodium citrate solution, heat in a water bath at 75°C for 2 hours, and filter to obtain spherical lead oxide. The scanning electron microscope picture is as follows figure 1 shown.
Embodiment 2
[0020] Embodiment 2: the preparation of spherical lead oxide atmospheric mineral dust
[0021] (1) prepare respectively 40mmol / L lead acetate solution, 40mmol / L hexamethylenetetramine solution, 10mmol / L trisodium citrate solution, the molar ratio of the three is 1:1:0.4;
[0022] (2) Mix the prepared lead acetate solution, hexamethylenetetramine solution and trisodium citrate solution, heat in a water bath at 60°C for 3 hours, and filter to obtain spherical lead oxide.
Embodiment 3
[0023] Embodiment 3: the preparation of spherical lead oxide atmospheric mineral dust
[0024] (1) prepare respectively 50mmol / L lead acetate solution, 50mmol / L hexamethylenetetramine solution, 20mmol / L trisodium citrate solution, the molar ratio of the three is 1:1:0.0.2;
[0025] (2) Mix the prepared lead acetate solution, hexamethylenetetramine solution and trisodium citrate solution, heat in a water bath at 90°C for 1 hour, and filter to obtain spherical lead oxide.
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