A kind of epoxy resin insulation material and its preparation method and application

A technology for epoxy resin and insulating material, applied in the field of epoxy resin insulating material and its preparation, can solve the problems of insufficient hydrophobicity and poor low temperature toughness, solve the problem of filler settlement, improve mechanical strength and impact strength, Evenly dispersed effect

Active Publication Date: 2022-04-22
GLOBAL ENERGY INTERCONNECTION RES INST CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] Therefore, the technical problem to be solved by the present invention is to overcome the technical defects of the epoxy resin materials in the prior art, such as relatively insufficient hydrophobic performance and obvious deterioration of low-temperature toughness in practical applications, thereby providing an epoxy resin insulating material and Its preparation method and application

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  • A kind of epoxy resin insulation material and its preparation method and application
  • A kind of epoxy resin insulation material and its preparation method and application
  • A kind of epoxy resin insulation material and its preparation method and application

Examples

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Embodiment 1

[0047] This embodiment provides an epoxy resin insulating material, including, 100g 3,4-epoxycyclohexanecarboxylate-3′,4′-epoxycyclohexane methyl ester, 108g methyltetrahydrophthalophthalate Acid anhydride, 0.6g dimethylbenzylamine, 20g silicone modified resin, 20g particle toughening agent (rubber elastomer particles, the average particle diameter is 40μm), 130g active silica powder, 2g KH560; wherein, active silica powder includes The mass ratio of the first particle fraction and the second particle fraction is 7:3, the median diameter of the first particle fraction is 32 μm; the median diameter of the second particle fraction is 12 μm;

[0048] The preparation method of above-mentioned epoxy resin insulating material comprises,

[0049] Mix 3,4-epoxycyclohexanecarboxylic acid-3′,4′-epoxycyclohexanemethyl ester, silicone modified resin, KH560, and granular toughening agent in a stirring tank, raise the temperature to 80°C, and Vacuum stirring under the condition of 200Pa fo...

Embodiment 2

[0056] This embodiment provides an epoxy resin insulating material, including, 100g 3,4-epoxycyclohexanecarboxylate-3',4'-epoxycyclohexane methyl ester, 125g methyltetrahydrophthalophthalate Acid anhydride, 0.7g dimethylbenzylamine, 40g silicone modified resin, 20g particle toughening agent (rubber elastomer particles, average particle diameter is 40μm), 150g active silica powder, 2g KH560; wherein, active silica powder includes The mass ratio of the first particle fraction and the second particle fraction is 7:3, the median diameter of the first particle fraction is 32 μm; the median diameter of the second particle fraction is 12 μm;

[0057] The preparation method of above-mentioned epoxy resin insulating material comprises,

[0058] Mix 3,4-epoxycyclohexanecarboxylic acid-3′,4′-epoxycyclohexanemethyl ester, silicone modified resin, KH560, and granular toughening agent in a stirring tank, raise the temperature to 80°C, and Vacuum stirring under the condition of 200Pa for 2h...

Embodiment 3

[0065] This embodiment provides an epoxy resin insulating material, comprising, 100g bis((3,4-epoxycyclohexyl)methyl)adipate, 101g methyltetrahydrophthalic anhydride, 0.7g di Methylbenzylamine, 40g organosilicon modified resin, 20g particle toughening agent (rubber elastomer particle, average particle diameter is 40 μ m), 137g active microsilica powder, 2g KH560; Wherein, active microsilica powder comprises mass ratio and is 7: 3. The first particle fraction and the second particle fraction, the median diameter of the first particle fraction is 32 μm; the median diameter of the second particle fraction is 12 μm;

[0066] The preparation method of above-mentioned epoxy resin insulating material comprises,

[0067] Mix bis((3,4-epoxycyclohexyl)methyl)adipate, silicone modified resin, KH560, and particle toughening agent in a stirring tank, raise the temperature to 80°C, and Stir in vacuum for 2 hours under the condition to prepare the premixed modified cycloaliphatic epoxy resi...

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Abstract

The invention belongs to the technical field of preparation of electrical insulating materials, and in particular relates to an epoxy resin insulating material and its preparation method and application. The raw materials of the epoxy resin insulating material include 92-107 parts of epoxy resin, 20-50 parts of silicone modified resin and 130-190 parts of filler, and the Si-CH in the silicone modified resin 3 The molar content is 23.33%‑47.17%. This insulating material contains a large amount of Si‑CH 3 The silicone modified resin can modify the epoxy resin, which can make the epoxy resin have better hydrophobicity and water repellency. At the same time, the silicone modified resin can also form a network crosslinked structure with the epoxy resin, improving The mechanical strength and impact strength of epoxy resin insulation materials; by adding fillers to the epoxy resin, the hydrophobicity, low-temperature brittleness and impact strength of the epoxy resin can be further improved in combination with physical filling modification technology.

Description

technical field [0001] The invention belongs to the technical field of preparation of electrical insulating materials, and in particular relates to an epoxy resin insulating material and its preparation method and application. Background technique [0002] External insulation is the area where most accidents occur in power systems. The level of external insulation significantly affects the safe operation of power systems. The improvement and promotion of external insulation performance has always been one of the focuses of power system research. All kinds of line insulators need to meet the technical requirements of electrical performance, mechanical performance and aging resistance in the long-term complex and harsh operating environment. External insulation materials are naturally one of the key contents of the external insulation research of power systems. As far as the overall application of external insulating materials is concerned, electric porcelain and glass are the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L63/00C08K7/26C08G59/32C08G59/30
CPCC08L63/00C08G59/306C08G59/3281C08L2205/03C08L2205/025C08L2203/20C08L2201/08C08K2201/014C08K2201/003C08K7/26
Inventor 尹立张翀田野王琨杨威陈新刘一涛张卓颜丙越陈赟李飞邢照亮史晓宁
Owner GLOBAL ENERGY INTERCONNECTION RES INST CO LTD
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