Ciliate desert-grass effective parts formulation resin processing method

A technology of effective parts and treatment methods, which is applied in the field of resin treatment of effective parts of Artemisia argyi, and can solve problems such as unfavorable recovery of liver diseases and liver damage

Inactive Publication Date: 2006-06-21
斯拉甫·艾白
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, many drugs must be oxidized, decomposed, and excreted in the liver, and some can directly cause liver damage, which is not conducive to the recovery of liver disease

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] a. First, crush the whole Artemisia argyi into powder, extract it with 60% ethanol to obtain an Artemisia ethanol extract for use, dissolve the extract with ethyl acetate to obtain the ethyl acetate part, and use 3% sodium hydroxide Process to obtain the alkaline aqueous solution of Artemisia annua extractum;

[0027] b. Pretreat the macroporous resin by conventional methods, wet-pack the column with ethanol, and wash the column with 95% ethanol until the ethanol liquid and water are mixed in a ratio of 1:5 until it is not white and turbid, and then use a large amount of Wash off the ethanol with distilled water until there is no ethanol smell in the water;

[0028] c. Weigh the pretreated resin and soak it in the alkaline aqueous solution of Artemisia annua extract for 24 hours, filter the solution, wash the macroporous resin with distilled water until it is colorless, then elute with ethanol, concentrate, and dry in vacuum to prepare Oral solid dosage form and liquid...

Embodiment 2

[0030] a. First, crush the whole herb of Artemisia argyi into powder, extract it with 75% ethanol to obtain an ethanol extract of Artemisia argyi for later use, dissolve the extract with ethyl acetate to obtain the ethyl acetate part, and use 8% sodium hydroxide Process to obtain the alkaline aqueous solution of Artemisia annua extractum;

[0031] b. Pretreat the macroporous resin by conventional methods, wet-pack the column with ethanol, and wash the column with 95% ethanol until the ethanol liquid and water are mixed in a ratio of 1:5 until it is not white and turbid, and then use a large amount of Wash off the ethanol with distilled water until there is no ethanol smell in the water;

[0032] c. Weigh the pretreated resin and soak it in 95% ethanol solution of Artemisia saponica extract for 24 hours, filter off the solution, wash the macroporous resin with distilled water until it is colorless, then elute with acetone, concentrate, and dry in vacuo into oral solid dosage f...

Embodiment 3

[0034] a. First, crush the whole herb of Artemisia argyi into powder, extract it with 95% ethanol to obtain an ethanol extract of Artemisia argyi for later use, dissolve the extract in ethyl acetate to obtain the part of ethyl acetate, and use 12% sodium hydroxide Process to obtain the alkaline aqueous solution of Artemisia annua extractum;

[0035] b. Pretreat the macroporous resin by conventional methods, wet-pack the column with ethanol, and wash the column with 95% ethanol until the ethanol liquid and water are mixed in a ratio of 1:5 until it is not white and turbid, and then use a large amount of Wash off the ethanol with distilled water until there is no ethanol smell in the water;

[0036] c. Weigh the pretreated resin and soak it in the alkaline aqueous solution of Artemisia annua extract for 24 hours, filter the solution, wash the macroporous resin with distilled water until it is colorless, then elute with acetone, concentrate, and dry in vacuo. Oral solid dosage f...

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PUM

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Abstract

The present invention relates to the resin treating process of shortstalk monkshood preparation. The process includes crushing whole herb of shortstalk monkshood, alcohol extraction to obtain shortstalk monkshood extractum, dissolving the extractum with ethyl acetate to obtain the effective part of shortstalk monkshood, treating with sodium hydroxide aqua to obtain alkali water solution of shortstalk monkshood extractum, soaking pre-treated resin in the alkali water solution or alcohol solution of shortstalk monkshood extractum, washing the resin with distilled water, eluting with alcohol or acetone, concentration, vacuum drying and other steps to prepare solid or liquid preparation. The preparation is used for oral taking to treat viral hepatitis and various kinds of liver damage, and has the features of small dosage, high curative effect and no toxic side effect.

Description

technical field [0001] The invention relates to a method for treating the effective part preparation of Artemisia argyi with resin. Background technique [0002] A dry whole herb of Artemisia rupestris L. Harvest and dry in July and August. The total length of this product is 10-50 cm. Roots and rhizomes are cylindrical, khaki to taupe, long with a few short fibrous roots, and the section is light yellow. Stems single or several, curved at the rhizome, 1.5-3 cm in diameter, young branches and flowering branches densely covered with short hairs on the upper part, old branches or branches smooth, with inconspicuous thin stripes, the surface is often purple, and the cross section is white , hollow. Functions and indications: clearing away heat and detoxification, invigorating the stomach and eliminating food, dispelling wind and activating blood circulation. For colds, allergies, food accumulation, snakebite, boils. [0003] Viral hepatitis and liver i...

Claims

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Application Information

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IPC IPC(8): A61K36/28A61P1/14A61P1/16A61P17/02A61P31/14A61P37/08A61P39/02
Inventor斯拉甫·艾白
Owner斯拉甫·艾白