Method of storing nitrogen trifluoride
一种三氟化氮、钼钢的技术,应用在三氟化氮、化学仪器和方法、气体贮运装置等方向,能够解决不适于贮存、没有确定硝酸酸度、硝酸很难被控制等问题
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[0023] The present invention can be better understood through the following examples, which are for the purpose of illustration only and should not be construed as limiting the present invention.
[0024] Add ammonia and fluorine gas to the melt of ammonium hydrofluoride to prepare impure NF 3 gas. Refining the gas thus prepared into low-temperature high-purity liquid-phase NF 3 , and then collect the gaseous NF in a storage vessel 3 . Load 20Kg of collected NF in the manganese steel container and the chromium-molybdenum steel container made by DDI process respectively 3 gas. Place each container at room temperature and detect NF over time 3 The pH of the gas changes. The manganese steel container used contained 1.5 wt% manganese and the chromium-molybdenum steel container used contained 1.5 wt% chromium and 0.5 wt% molybdenum. N was analyzed by gas chromatography (Valco, PDD detector) 2 O content. In addition, HNO was analyzed by 3 : Determine the total acidity by N...
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