Kalium phosphocreatine and chemosynthesis method thereof
A technology of potassium creatine phosphate and sodium creatine phosphate, which is applied in the field of creatine phosphate potassium and its chemical synthesis, can solve the problems that creatine phosphate cannot achieve the best external environment, absorption is not ideal, and the purity is not high enough to achieve recovery High efficiency, improved purity, and reasonable process conditions
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Embodiment 1
[0032] Sodium Creatine Phosphate 1%
[0033] Potassium chloride 0.5%
[0034] The organic solvent is absolute ethanol.
[0035] The chemical synthesis method is: take 1 mole of creatine phosphate sodium in a beaker, add 200ml of water to make it dissolve into a 5% solution, and set aside; select a positive resin 723 column with a diameter of 2 cm, add 3% hydrochloric acid solution to soak the resin, and make it Completely wet; add sodium creatine phosphate to the resin column several times to make it fully adsorbed and replace creatine phosphate: add 0.5 mole of potassium chloride to the replaced creatine phosphate solution, and stir while adding to make it Dissolve completely; Concentrate the solution until a white viscous solid appears, add a small amount of absolute ethanol, precipitate, rotate to evaporate until there is no distillate, take out the viscous solid, and dry it in vacuum at 65°C for 15 hours to obtain creatine phosphate potassium. The yield was 71.4%.
Embodiment 2
[0037] Sodium Creatine Phosphate 1%
[0038] Potassium chloride 0.75%
[0039] The organic solvent is absolute ethanol.
[0040] The chemical synthesis method is: take 1 mole of creatine phosphate sodium in a beaker, add 200ml of water to make it dissolve into a 5% solution, and set aside; select a positive resin 723 column with a diameter of 2 cm, add 3% hydrochloric acid solution to soak the resin, and make it Completely wet; then add creatine phosphate sodium into the resin column several times to make it fully adsorbed and replace creatine phosphate: add 0.75 moles of potassium chloride to the replaced creatine phosphate solution, and stir while adding to make it Dissolve completely; Concentrate the solution until a white viscous solid appears, add a small amount of absolute ethanol, precipitate, rotate to evaporate until there is no distillate, take out the viscous solid, and dry it in vacuum at 65°C for 15 hours to obtain creatine phosphate potassium. The yield was 75...
Embodiment 3
[0042] Sodium Creatine Phosphate 1%
[0043] Potassium chloride 1%
[0044] The organic solvent is ethanol
[0045] The chemical synthesis method is: take 1 mole of creatine phosphate sodium in a beaker, add 200ml of water to make it dissolve into a 5% solution, and set aside; select a positive resin 723 column with a diameter of 2 cm, add 3% hydrochloric acid solution to soak the resin, and make it Completely wet; then add creatine phosphate sodium into the resin column several times to make it fully adsorbed and replace creatine phosphate: add 1 mole of potassium chloride to the replaced creatine phosphate solution, and stir while adding to make it Dissolve completely; Concentrate the solution until a white viscous solid appears, add a small amount of absolute ethanol, precipitate, rotate to evaporate until there is no distillate, take out the viscous solid, and dry it in vacuum at 65°C for 15 hours to obtain creatine phosphate potassium. The yield was 78.9%.
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