Method for analyzing CO stable isotope mass number abundance ratio through chromatography-mass spectrometry
A stable isotope, mass number technology, applied in the direction of analyzing materials, measuring devices, material separation, etc., can solve the problem of insufficient detailed expression of carbon monoxide sources, single, etc., and achieve good application prospects and simple methods.
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[0024] Chromatography-mass spectrometry analysis CO stable isotope mass number abundance ratio method, comprising the following steps:
[0025] (1) Establish a mathematical model for the stable isotope ratio of carbon monoxide:
[0026] According to the carbon monoxide molecule is composed of five stable isotopes 12 C. 13 C. 16 O. 17 O. 18 O element composition, under different conditions, 6 kinds of carbon and oxygen elements with different mass numbers will be formed, as shown in Table 1:
[0027]
[0028] Accordingly, the mass abundance ratios of six stable isotopes of carbon dioxide can be obtained, namely Table 2:
[0029] .
[0030] (2) Pass the carrier gas with a purity greater than 99.999% through the purifier at an output pressure of 0.20~0.60 MPa, so that the purified carrier gas has a purity greater than 99.9999% or greater than 99.99999%.
[0031] (3) Pass the purified carrier gas into the chromatographic column of the gas chromatograph where the sample...
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