Polymeric pigment systems and methods
A technology of polyurethane polymers and pigments, applied in the field of pigment systems, can solve problems such as nozzle clogging, polymers that are not soluble in printing, and difficulties
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[0090] 1(a) – Manufacture of polyurethane prepolymers
[0091] Fill 93.55g of Polyol 220-056N (polyether polyol having an average molecular weight of 2000 available from Dow Chemical), 9.55 g of dimethylpropionic acid (DMPA) and 19.11 g of NMP. The mixture was stirred with two PTFE stirrers under 1 mm vacuum. Then, the reactor was purged with nitrogen and heated to 100 °C to produce a clear pale yellow solution. The solution was heated under vacuum for 20 minutes using a dry ice-IPA trap (trap). The vessel was then backflushed with dry nitrogen and cooled to 60°C. Slowly add 21.78 g of TDI using a 60 mL plastic syringe at 59°C (available from Bayer's TD-80). The temperature initially dropped to 57°C, followed by a rapid exotherm requiring cooling air to keep the temperature below 70°C. Then, the remaining TDI was added to the mixture where the temperature was raised to about 73°C. Add 8 drops of tin catalyst (dibutyltin dilaurate) and set the temperature to 80°C. Mix...
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