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Preparation method of melon and fruit perfume for cigarettes

A technology for tobacco spice, melon and fruit, applied in the directions of essential oils/spice, tobacco, application, etc., can solve problems such as differences in the extraction efficiency of active components, and achieve the effects of simple and easy operation, high extraction efficiency, and simple process

Inactive Publication Date: 2014-06-18
CHINA TOBACCO ANHUI IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Different concentrations of alcohol have different extraction efficiencies for active ingredients in natural products

Method used

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  • Preparation method of melon and fruit perfume for cigarettes
  • Preparation method of melon and fruit perfume for cigarettes
  • Preparation method of melon and fruit perfume for cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Embodiment 1: using pears as raw materials to prepare tobacco spices, the steps are as follows:

[0019] A, pears are completely pulverized, and solid-liquid separation is obtained to obtain pear juice and pear pulp;

[0020] B, concentrating under reduced pressure, remove the moisture in the pear juice, obtain pear juice extract;

[0021] C. Merge pear juice extract and pulverized pear pulp, add 5 times the weight of 75% alcohol solution, heat to 60°C for extraction for 3 hours, then lower the temperature to terminate the extraction;

[0022] D, solid-liquid separation, obtain extract A and extract residue;

[0023] E. Add 3 times the weight of 48% alcohol solution to the extraction residue, heat to 60°C for 3 hours, then lower the temperature to terminate the extraction;

[0024] F, solid-liquid separation to obtain extract B;

[0025] G. Combine the extract A and the extract B, concentrate under reduced pressure until the specific gravity of the solution is 1.15, ...

Embodiment 2

[0026] Embodiment 2: using grapes as raw material to prepare flavoring for tobacco, the steps are as follows:

[0027] A, grapes are pulverized, and solid-liquid separation is carried out to obtain grape juice and grape pulp;

[0028] B, concentrating under reduced pressure, remove the moisture in the grape juice, obtain grape juice extract;

[0029] C. Merge the grape juice extract and crushed grape pulp, add 5 times the weight of 80% alcohol solution, heat to 60 ° C for 3 hours, and then lower the temperature to terminate the extraction;

[0030] D, solid-liquid separation, obtain extract C and extract residue;

[0031] E. Add 3 times the weight of 45% alcohol solution to the extraction residue, heat to 60°C for 3 hours, then lower the temperature to terminate the extraction;

[0032] F, solid-liquid separation to obtain extract D;

[0033] G. Combine the extract C and the extract D, concentrate under reduced pressure until the specific gravity of the solution is 1.21, an...

Embodiment 3

[0034] Embodiment 3: using hawthorn as raw material to prepare tobacco spices, the steps are as follows:

[0035] A, hawthorn is crushed to obtain hawthorn fruit juice and hawthorn pulp;

[0036] B, concentrating under reduced pressure, remove the moisture in the hawthorn fruit juice, obtain the hawthorn fruit juice extract;

[0037] C. Merge the hawthorn juice extract and crushed hawthorn pulp, add 5 times the weight of 75% alcohol solution, heat to 60°C for extraction for 3 hours, then lower the temperature to terminate the extraction;

[0038] D, solid-liquid separation, to obtain extract E and extraction residue;

[0039] E. Add 3 times the weight of 50% alcohol solution to the extraction residue, heat to 60°C for 3 hours, then lower the temperature to terminate the extraction;

[0040] F, solid-liquid separation to obtain extract F;

[0041] G. Combine extract E and extract F, concentrate under reduced pressure until the specific gravity of the solution is 1.25, and ob...

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Abstract

The invention discloses a preparation method of melon and fruit perfume for cigarettes. The preparation method comprises the following steps: (1) smashing melon and fruit raw materials, and carrying out solid-liquid separation so as to obtain fruit juice and solid fruit flesh; (2) carrying out reduced pressure concentration on the fruit juice to remove water so as to obtain fruit juice extract; (3) combining the fruit juice extract and the solid fruit flesh, and adding 3-6 times by weight of alcoholic solution with the concentration of 70%-80% for extraction so as to obtain a primary extract solution and residues, wherein the extraction temperature is 50-80 DEG C, and the extraction time is 1-4 hours; (4) adding 3-6 times by weight of alcoholic solution with the concentration of 40%-50% to the residues for extraction, and carrying out solid-liquid separation so as to obtain a secondary extract solution, wherein the extraction temperature is 50-80 DEG C, and the extraction time is 1-4 hours; (5) combining the extract solutions, and carrying out reduced pressure concentration to remove solvents so as to obtain the melon and fruit perfume for the cigarettes. The preparation method is simple, convenient and practicable; by adopting the preparation method, the extraction rates of reducing sugar, organic acid, flavone, polyphenol and glucoside in melons and fruits are increased, and meanwhile, the amount of amino acids, protein and macromolecular polysaccharides dissolved in the perfume is reduced.

Description

Technical field: [0001] The invention relates to a preparation method of melon and fruit flavoring for tobacco. Background technique: [0002] Melon and fruit extracts are very commonly used tobacco flavors, such as apple extracts, grape extracts, fruit juice concentrates, etc. When they are added to cigarettes, they can reduce the irritation of cigarettes, increase the sweetness of cigarettes, and improve the aroma quality of tobacco . Most of the volatile oils, reducing sugars, organic acids, vitamins, flavonoids, polyphenols, glycosides and other substances contained in melons and fruits have a good additive effect on tobacco, while amino acids, proteins, starch, pectin, and other polysaccharide compounds have a good effect on tobacco. Tobacco often has negative effects on tobacco. [0003] Common melon and fruit extracts are fruit extracts prepared by extracting fruit juice from melons and fruits, concentrating them into fruit juice extracts, or using enzyme preparatio...

Claims

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Application Information

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IPC IPC(8): C11B9/00A24B15/24
Inventor 邹鹏舒俊生郭东锋刘非徐峻鲍穗戴魁
Owner CHINA TOBACCO ANHUI IND CO LTD
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