Method for extracting norcamphanone derivative and purine alkaloidal compounds from unicorn beetle
A technology of unicorn and compound, which is applied in the field of natural product extraction, can solve the problems of lack of basic research on activity and medicinal substances, and achieve the effect of improving medicinal value, simplifying the extraction process, and avoiding damage
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Embodiment 1
[0063] The method for extracting norcanone derivatives and purine alkaloid compounds from the unicorn, comprising the following steps:
[0064] Step 1. Take 1000g of the imago imago, wash it with clear water and dry it in the air, then place it in an oven at 30°C and dry it to constant weight, take it out and pulverize it to obtain the imago unicorn powder, and set aside; Under the condition of ℃, soak 40h with the dichloromethane of 5 times of the weight of the unicorn powder, use ultrasonic wave to assist extraction in the immersion process, filter, add the dichloromethane of 5 times of the weight of the unicorn powder to the obtained filter residue again, at 22 Soak for 40 hours under the condition of ℃, use ultrasonic to assist extraction during the soaking process, filter after the extraction is completed, place the obtained filter residue in a ventilated place and air-dry at room temperature to obtain insect residue, and set aside;
[0065] Step 2. Add methanol solution ...
Embodiment 2
[0072] The method for extracting norcanone derivatives and purine alkaloid compounds from the unicorn, comprising the following steps:
[0073] Step 1. Take 1500g of the adult unicorn, wash it with clear water, and dry it in the air, then place it in an oven at 50°C and dry it to constant weight, take it out and pulverize it to obtain the unicorn powder, and set aside; put the unicorn powder at 24 Under the condition of ℃, soak 44h with dichloromethane of 10 times the weight of unicorn powder, use ultrasonic wave to assist extraction in the soaking process, filter, and add 10 times of the weight of unicorn powder to the obtained filter residue in dichloromethane again, at 24 Soak for 44 hours under the condition of ℃, use ultrasonic wave to assist extraction during the soaking process, filter after the extraction is completed, and place the obtained filter residue in a ventilated place to air dry at room temperature to obtain worm residue for later use;
[0074]Step 2. Add met...
Embodiment 3
[0081] The method for extracting norcanone derivatives and purine alkaloid compounds from the unicorn, comprising the following steps:
[0082] Step 1. Take 2500g of the imago unicorn, wash it with clear water, and dry it in the air, then place it in an oven at 65°C and dry it to constant weight, take it out and crush it to obtain the unicorn powder, and set aside; put the unicorn powder at 26 Under the condition of ℃, soak 48h with the dichloromethane of 15 times of the weight of the unicorn powder, and use ultrasonic wave to assist extraction in the soaking process, filter, add the dichloromethane of 15 times of the weight of the unicorn powder to the obtained filter residue again, at 26 Soak for 48 hours under the condition of ℃, use ultrasonic wave to assist extraction during the soaking process, filter after the extraction is completed, and place the obtained filter residue in a ventilated place to dry at room temperature to obtain insect residue, which is ready for use; ...
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