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Preparation device and method for alkali residue liquid desulfurizing agent

A preparation device and desulfurizer technology, which is applied in the field of alkali slag liquid desulfurizer preparation device, can solve the problems of poor production process stability, high filter cloth damage rate, and low degree of automation control, so as to avoid mechanical solid-liquid separation and avoid loading and unloading And transport, improve the effect of desulfurization effect

Active Publication Date: 2015-08-26
TANGSHAN SANYOU CHEM IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Both of these two processes require a mechanical solid-liquid separation process to achieve solid-liquid separation and chlorine reduction, resulting in the agglomeration of solid particles of the desulfurizer. Low activity, large circulating volume of desulfurization liquid, high operating cost
At the same time, the energy consumption of mechanical solid-liquid separation and chlorine reduction process is high. The plate and frame filter press needs to be equipped with a double-stage pressurized pump and an air compressor station. The damage rate of the filter cloth is high, resulting in high production costs. Pulp caused difficulties. As the first generation technology, the process of preparing liquid desulfurizer by plate-and-frame filter press and coulter crusher has been discontinued since 2012; Agglomeration is reduced, and the quality and activity of the desulfurizer is relatively improved. Therefore, compared with the first-generation process technology, the desulfurization efficiency of the desulfurization tower and the quality of desulfurization gypsum products are improved, but the energy consumption of the centrifuge is still high.
Both of the above two processes require loading, unloading and transportation of solid materials, the degree of automation control is low, and the stability of the entire production process is poor

Method used

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  • Preparation device and method for alkali residue liquid desulfurizing agent
  • Preparation device and method for alkali residue liquid desulfurizing agent

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A preparation device for alkali slag liquid desulfurizer, see attached figure 1 , in the figure: alkali slag delivery pump 1, first pipeline 2, gravity sand chamber 3, second pipeline 4, seventh pipeline 5, first overflow pipeline 6, main collection pipeline 7, second overflow pipeline Flow pipeline 8, chlorine reduction tank 9, third pipeline 10, sixth pipeline 11, finished product buffer tank 12, desulfurization agent delivery pump 13, auxiliary agent tank 14, sedimentation aid pump 15, fourth pipeline 16 , the fifth pipeline 17, the thickener 18, the eighth pipeline 19, the ninth pipeline 20.

[0030] In this embodiment, the alkali slag delivery pump 1 is connected to the desanding device through the first pipeline 2, and the desandering device adopts a gravity sand settler 3, and the solid material in the gravity sand settler 3 is directly settled during the solid-liquid separation process; The top of the gravity sand settler 3 is connected with the thickener ...

Embodiment 2

[0041] A preparation device for alkali slag liquid desulfurizer, see attached figure 2 , in the figure: alkali slag delivery pump 1, first pipeline 2, hydrocyclone desander 3, second pipeline 4, seventh pipeline 5, first overflow pipeline 6, total collection pipeline 7, second pipeline Overflow pipeline 8, chlorine reduction tank 9, third pipeline 10, sixth pipeline 11, finished product buffer tank 12, desulfurization agent delivery pump 13, auxiliary agent tank 14, sedimentation aid pump 15, fourth pipeline 16, the fifth pipeline 17, the thick sand settler 18, the eighth pipeline 19, the ninth pipeline 20, and the tenth pipeline 21.

[0042] The difference with Embodiment 1 is: the side wall of the thick sand settler 18 is connected with the top of the chlorine reduction barrel 9 through the fifth pipeline 17, and the bottom end of the thick sand settler 18 is connected with the tenth pipeline 21. Collect the total pipeline 7 connections.

[0043] During the solid-liq...

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Abstract

The invention relates to a preparation device and method for a desulfurizing agent, in particular to a preparation device and method for an alkali residue liquid desulfurizing agent. The preparation device comprises an alkali residue conveying pump, wherein the alkali residue conveying pump is connected with a sand removal device through a first pipeline; the top end of the sand removal device is connected with a thickener through a second pipeline; the upper part of the thickener is connected with a main collection pipeline through a first overflow pipeline; the thickener is connected with a chlorine reducing bucket through a fifth pipeline; an assistant preparation tank is connected with a middle layer of the chlorine reducing bucket; a washing water pipeline is connected with a lower layer of the chlorine reducing bucket; the bottom of the chlorine reducing bucket is connected with a finished product buffer bucket through a sixth pipeline; an upper layer of the chlorine reducing bucket is connected with the main collection pipeline through a second overflow pipeline. The preparation method comprises the following steps: performing gravitational sand settling, thickening and settling and chlorine reduction by washing, performing settling and thickening, discharging the liquid desulfurizing agent from the bottom of the chlorine reducing bucket, and enabling the liquid desulfurizing agent to enter the buffer bucket for storage. Compared with the prior art, the application of high-energy equipment such as a pressure filter, a centrifuge and the like is avoided, mechanical solid-liquid separation of waste alkali residue liquid is avoided, and the flue gas desulfurization effect is effectively improved.

Description

technical field [0001] The invention relates to a device and method for preparing a desulfurizing agent, in particular to a device and a method for preparing an alkali slag liquid desulfurizing agent. Background technique [0002] Utilizing the by-product alkali slag waste liquid in the ammonia-soda method soda ash production to produce alkali slag liquid desulfurizer, which is used in the production of boiler flue gas desulfurizer, is a new technology for resource utilization of alkali slag waste. At present, there are two production processes of alkali slag desulfurizer: the first process is that the waste liquid of alkali slag is desanded, then enters the filter press for solid-liquid separation, and then adds water to the coulter crusher to reduce chlorine to make a liquid desulfurizer ; The second process is that the alkali slag waste liquid enters the two-stage decanter centrifuge to realize solid-liquid separation and chlorine reduction after desanding, and then it is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D53/78B01D53/48
Inventor 冯树红辛兵王秉钧韩立山云玉娥刘忠华王同国宋自利郑存强吕晓英赵振旺韩庆龙张焕峰王荣瑞赵会聪谢秋利李兴生赵丽贤李宏刚魏智义韦一
Owner TANGSHAN SANYOU CHEM IND
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