Novel light-emitting compound and organic light-emitting element containing same
A technology for organic light-emitting elements and light-emitting compounds, applied in the field of organic light-emitting elements and new light-emitting compounds, can solve the problems of high driving voltage, practical difficulties, low efficiency, etc., and achieve the effects of low driving voltage, low power consumption, and high efficiency
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Embodiment 1
[0097] Example 1: Synthesis of Compound 1
[0098]
[0099] 2.5g of the above intermediate A, 3.99g of 4-bromo-2,6-diphenylpyridine, 1.54g of t-BuONa, 0.40g of Pd 2 (dba) 3 , 0.5ml (t-Bu) 3 P was dissolved in 40 ml of toluene, and then stirred under reflux. After confirming the termination of the reaction by TLC, the organic layer was extracted with MC, filtered under reduced pressure, and purified on a column to obtain 2.58 g of compound 1 (yield 52%).
[0100] m / z: 462.21 (100.0%), 463.21 (37.5%), 464.22 (6.7%)
Embodiment 2
[0101] Example 2: Synthesis of Compound 2
[0102] Compound 2 was synthesized by the same method as compound 1 except that 2-bromo-4,6-diphenylpyridine was used instead of 4-bromo-2,6-diphenylpyridine to react.
[0103] m / z: 462.21 (100.0%), 463.21 (37.5%), 464.22 (6.7%)
Embodiment 3
[0104] Example 3: Synthesis of Compound 3
[0105]
[0106] Compound 3 was synthesized by the same method as compound 1 except that 4-bromo-2,6-diphenylpyrimidine was used instead of 4-bromo-2,6-diphenylpyridine to react.
[0107] m / z: 463.20 (100.0%), 464.21 (36.0%), 465.21 (6.7%), 464.20 (1.1%)
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