Novel light-emitting compound and organic light-emitting element containing same
A technology of organic light-emitting elements and light-emitting compounds, applied in the field of organic light-emitting elements and new light-emitting compounds, which can solve the problems of high driving voltage, difficulty in practical application, and low efficiency, and achieve the effects of low driving voltage, low power consumption, and high efficiency
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Embodiment 1
[0096] Embodiment 1: the synthesis of compound 1
[0097]
[0098] 2.0g of the above intermediate 01, 4.6g of 9-(3'-bromo-[1,1'-biphenyl]-3-yl)-9H-carbazole, 1.4g of t-BuONa, 0.35g of PD 2 (dba) 3 , 0.5ml of (t-Bu) 3 P was dissolved in 30 ml of toluene, and then stirred under reflux. After confirming the termination of the reaction by TLC, the organic layer was extracted with MC, filtered under reduced pressure, and purified on a column to obtain 1.77 g of compound 1 (yield 35%).
[0099] m / z: 525.18 (100.0%), 526.19 (40.3%), 527.19 (8.1%), 528.19 (1.2%), 526.18 (1.1%)
Embodiment 2
[0100] Embodiment 2: the synthesis of compound 2
[0101]
[0102] Compound 2 was synthesized by the same method as Compound 1 except using the above-mentioned Intermediate 05.
[0103] m / z: 526.18 (100.0%), 527.18 (40.5%), 528.19 (7.5%), 529.19 (1.0%)
Embodiment 3
[0104] Embodiment 3: the synthesis of compound 3
[0105]
[0106] Compound 3 was synthesized by the same method as Compound 1 except using the above-mentioned Intermediate 33.
[0107]m / z: 542.16 (100.0%), 543.16 (40.0%), 544.16 (8.3%), 544.15 (4.5%), 545.16 (1.9%), 543.15 (1.5%)
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