Novel light emission compound and organic light emitting device comprising same
A technology of light-emitting compounds and chemical formulas, applied in the field of organic light-emitting elements and new light-emitting compounds, can solve the problems of high driving voltage, practical difficulties, short life, etc., and achieve the effects of low driving voltage, low power consumption, and long life.
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Embodiment 1
[0096] Example 1: Synthesis of Compound 1
[0097]
[0098] 2.0 g of the above Intermediate 01, 4.6 g of 9-(3'-bromo-[1,1'-biphenyl]-3-yl)-9H-carbazole, 1.4 g of t-BuONa, 0.35 g of Pd 2 (dba) 3 , 0.5ml (t-Bu) 3 P was dissolved in 30 ml of toluene, followed by reflux stirring. After confirming the termination of the reaction by TLC, the organic layer was extracted with MC, filtered under reduced pressure, and purified by column purification to obtain 1.77 g of compound 1 (yield: 35%).
[0099] m / z: 525.18 (100.0%), 526.19 (40.3%), 527.19 (8.1%), 528.19 (1.2%), 526.18 (1.1%)
Embodiment 2
[0100] Example 2: Synthesis of Compound 2
[0101]
[0102] Compound 2 was synthesized by the same method as Compound 1 except that the above-mentioned Intermediate 05 was used.
[0103] m / z: 526.18 (100.0%), 527.18 (40.5%), 528.19 (7.5%), 529.19 (1.0%)
Embodiment 3
[0104] Example 3: Synthesis of Compound 3
[0105]
[0106] Compound 3 was synthesized by the same method as Compound 1 except that the above-mentioned Intermediate 33 was used.
[0107] m / z: 542.16 (100.0%), 543.16 (40.0%), 544.16 (8.3%), 544.15 (4.5%), 545.16 (1.9%), 543.15 (1.5%)
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