High-nuclear zinc cluster compound based on sulfur-containing triazole ligand and preparation method thereof
A technology of clusters and triazoles, which is applied in the field of complex synthesis, can solve the problems of difficulty in obtaining single crystals, low solubility of complexes, and easy precipitation, etc., and achieve the effect of improving solubility and wide application prospects
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[0017] Synthesis of high-nuclear zinc clusters based on sulfur-containing triazole ligands:
[0018] Weigh 0.2mmol (0.0294g) H 3 L, 0.2mmol (0.0745g) Zn(ClO 4 ) 2 ·6H 2 O,0.2mmol(0.0617g)Cd(NO 3 ) 2 4H 2 O was mixed in 10 mL of DMF, and the obtained mixture was stirred and reacted for 6 h at room temperature, and then filtered to obtain a colorless solution. The filtrate was allowed to stand for slow volatilization, and after 25 days, colorless cubic crystals were precipitated from the mother liquor, separated, washed, and dried.
[0019] see figure 1 In the molecular structure diagram of the zinc cluster compound of the present invention, for the convenience of observation, the peripheral guest solvent molecules are deleted. It can be clearly observed from the figure that the zinc cluster compound of the present invention is a 24-nuclear double-layer ring cluster compound composed of twenty-four zinc ions, twenty-four ligands and six coordinated water molecules, Ther...
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