Lithium ion battery anode material and preparation method thereof
A technology for lithium ion batteries and negative electrode materials, applied in battery electrodes, secondary batteries, circuits, etc., can solve the problem that the specific capacity of negative electrode materials cannot meet the needs, and achieve improved cycle stability, excellent discharge specific capacity, and volume expansion mitigation. Effect
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Embodiment 1
[0023] In the negative electrode material of the lithium ion battery, the negative electrode active material is a composite of nickel sulfide, indium sulfide and graphene. The material is a self-supporting structure.
[0024] The preparation method of described lithium-ion battery negative electrode material, comprises the following steps:
[0025] (1) Preparation of foamed nickel-graphene composite material: Cut the commercially available nickel foam into strips of 2 cm × 4 cm, immerse in 80 mL of graphene solution with a concentration of 2 mg / mL for 40 minutes, and then let it stand for 15 minutes before taking it out. spare;
[0026] (2) Preparation of indium sulfide-nickel sulfide composite graphene material: First, put 1.5g of indium nitrate nonahydrate and 0.8g of thioacetamide in 25mL of deionized water, and stir evenly to obtain a mixed solution; then mix the obtained mixed solution with the step ( The foamed nickel-graphene composite material prepared in 1) was plac...
Embodiment 2
[0031] In the negative electrode material of the lithium ion battery, the negative electrode active material is a composite of nickel sulfide, indium sulfide and graphene. The material is a self-supporting structure.
[0032] The preparation method of described lithium-ion battery negative electrode material, comprises the following steps:
[0033] (1) Preparation of foamed nickel-graphene composite material: Cut the foamed nickel into strips of 2cm×4cm, immerse in 50mL graphene solution with a concentration of 1mg / mL and sonicate for 30 minutes, then let it stand for 10 minutes, take it out, and set aside;
[0034] (2) Preparation of indium sulfide-nickel sulfide composite graphene material: first place 1g of indium nitrate nonahydrate and 0.5g of thioacetamide in 20mL of deionized water, and stir to obtain a mixed solution; then mix the obtained mixed solution with step (1 The foamed nickel-graphene composite material prepared in ) was placed in the lining of a 50mL polytet...
Embodiment 3
[0036] In the negative electrode material of the lithium ion battery, the negative electrode active material is a composite of nickel sulfide, indium sulfide and graphene. The material is a self-supporting structure.
[0037] The preparation method of described lithium-ion battery negative electrode material, comprises the following steps:
[0038] (1) Preparation of foamed nickel-graphene composite material: Cut the foamed nickel into strips of 2cm×4cm, immerse in 100mL of graphene solution with a concentration of 2mg / mL and sonicate for 60 minutes, then let it stand for 20 minutes, take it out, and set aside;
[0039](2) Preparation of indium sulfide-nickel sulfide composite graphene material: first, put 2g of indium nitrate nonahydrate and 1g of thioacetamide in 30mL of deionized water, and stir evenly to obtain a mixed solution; then mix the obtained mixed solution with step (1) The foamed nickel-graphene composite material prepared in was placed in the lining of a 50mL p...
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