Self-organized metal alloys for wear applications
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Fabrication of Alloys
[0046]Unless otherwise specified, the alloys in the examples are prepared as follows. Commercially pure powders (selected from Ag, Ni, Fe and Cu) are combined in the atomic amounts specified and then subjected to high-energy ball milling using a SPEX 8000 mill in an argon glove box for 12 h at ambient temperature (50° C.). Ball milling forces the mixing of matrix and Ag into a nanocomposite. The ball-milled powders are then compacted by warm pressing at 300° C. with a 1 GPa load under high vacuum (1.5×10−8 torr), producing cylinders with density exceeding 99% of the theoretical density. Limited contamination of powders can occur during ball milling by milling tools; e.g., when Fe is the matrix, small Fe2O3-type precipitates can be formed during compaction and annealing. The size and density of these nanoscale precipitates can be measured by Z-contrast imaging. Lastly, hardness is measured by nanoindentation, which is performed by ASTM E2546.
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