3,4-ring-opening polyacylation grayananes diterpene compound and preparation method thereof
A technology for polyacylating Trichosanthes and compounds, which is applied in the field of phytochemistry, can solve problems such as no patents or literature reports, and achieve the effects of simple and easy separation method, novel structure and high efficiency
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[0023] Example
[0024] After crushing 11 kg of dried leaves of Pieris formosa D. Don, they were immersed in a 25L acetone aqueous solution with a volume concentration of 75% to completely submerge the acetone aqueous solution, and soaked at room temperature for 48 hours to obtain an extract. Repeat the extraction twice and combine to obtain 50L extract;
[0025] The prior art vacuum concentration method is used for vacuum distillation until there is no acetone smell; according to the volume ratio of extract: petroleum ether = 1:1, the extract is extracted three times with petroleum ether at room temperature, and the amount of petroleum ether is 10L each time After the petroleum ether is recovered, the extract is obtained; according to the volume ratio of the extract: ethyl acetate = 1:1, the extract is extracted three times with ethyl acetate at room temperature, the amount of ethyl acetate is 10L each time, and concentrated under reduced pressure Then, 550g ethyl acetate extract...
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