Electrode film, electrode, method for manufacturing electrode, and electrical storage device
A manufacturing method and electrode film technology, which can be used in electrode manufacturing, hybrid/electric double-layer capacitor manufacturing, secondary battery manufacturing, etc., and can solve problems such as insufficiency
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[0047] As the preparation method of the dispersion liquid, there may be mentioned: a method of adding and mixing a predetermined amount of active material and conductive ion-containing inorganic particles in a solvent; adding a predetermined amount of active material to a mixture of conductive ion-containing inorganic particles Solvent and mixed method; disperse a specified amount of inorganic particles containing conductive ions in a solvent to obtain a dispersion of inorganic particles containing conductive ions, and add a specified amount of active material to the dispersion and mix it; Disperse a specified amount of inorganic particles containing conductive ions in a solvent to obtain a dispersion of inorganic particles containing conductive ions, disperse a specified amount of active material in a solvent to obtain an active material dispersion, and then mix the two dispersions; A method in which a predetermined amount of active material is dispersed in a solvent to obtain...
Embodiment 1
[0063] Lithium cobalt oxide (Cellseed 10-N manufactured by Nippon Chemical Industry Co., Ltd.; average particle diameter 12 μm) was used as an active material, and Denka black (DB: 50% extruded product manufactured by Denki Kagaku Kogyo; average particle diameter 32 nm) was used as a conductive agent. Lithium silicate (lithium silicate 35: manufactured by Nissan Chemical Industries, Ltd., aqueous solution solid content concentration 23 wt %, average particle diameter 1.3 μm) was used as the inorganic particles containing conductive ions.
[0064] 10.4 g of lithium silicate was added to a mixture of 36.0 g of lithium cobaltate and 2.8 g of Denka black, and further pure water was added and mixed to prepare a slurry having a solid content concentration of 50% by weight. This slurry contained 36.0 g of lithium cobaltate, 2.8 g of Denka black, and 2.4 g of lithium silicate. That is, the amount of the conductive ion-containing inorganic particles was 6.6 parts by weight relative to ...
Embodiment 2
[0067] As inorganic particles containing conductive ions, 8.4 g of potassium silicate (manufactured by Wako Pure Chemical Industries, Ltd., aqueous solution solid content concentration 28 wt %, average particle diameter 0.7 μm) was used instead of lithium silicate. Similarly, a slurry having a solid content concentration of 44% by weight was prepared. This slurry contained 36.0 g of lithium cobaltate, 2.8 g of Denka black, and 2.4 g of potassium silicate. That is, the amount of the conductive ion-containing inorganic particles per 100 parts by weight of the active material was 6.6 parts by weight. Next, electrodes were fabricated in the same manner as in Example 1. The film thickness of the electrode film after drying was 28 μm.
[0068] One electrode having a size of 3.0 cm×3.0 cm was cut out from the obtained electrode, and the weight, film thickness, and surface resistance of the electrode film were measured. For the measurement of the surface resistance, Loresta (manufa...
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