Fatty group polyamidoimide, its preparation method and its application
A polyamide-imide and aliphatic technology, which is applied in the field of preparation of polymer compounds, can solve the problems of difficult processing and molding, high rigidity, etc., and achieves the effects of simple and mild synthesis process, improved softness and solubility, and rich sources.
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Embodiment 1
[0033] According to the molar ratio of reactant HDI and CA 3:2, weigh CA 1.9214 g, HDI 2.400 ml, add DMAc solvent 30.0 ml, add catalyst 4-dimethylaminopyridine 0.0126 g at 60 o C temperature was reacted for 12 hours, and the product was precipitated and filtered with a mixture of 45 ml of water and 15 ml of ethanol, and at 60 o After drying in a C oven for 12 hours, a solid soluble polyamide-imide was obtained. Yield 69%.
Embodiment 2
[0035] Method is the same as Example 1, but the reaction time is 6 hours. Yield 79%.
Embodiment 3
[0037] Method is with embodiment 2, but does not add catalyzer, and temperature of reaction is 70 o c. Yield 78%.
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