Preparation method of oilfield demulsifier by utilizing waste grease
A waste oil and demulsifier technology, which is applied in the direction of dehydration/demulsification by chemical methods, can solve the problems of unsatisfactory dehydration effect of polyether demulsifiers, complicated demulsification and dehydration of emulsified crude oil, and increased dehydration costs, and achieves ideal results. , less epoxide, and clear water
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[0016] The present invention is further described below through specific examples, but the examples are not limitations of the present invention.
[0017] A method for preparing oil field demulsifier by using waste oil, comprising the following steps:
[0018] Add 1000 grams of waste oil (recovered gutter oil) into the reactor, heat it up, control the vacuum at 110°C for 2 hours, then add 90 grams of acetic acid and 20 grams of sulfuric acid, stir at 75°C for 1 hour, and then Add 450 grams of hydrogen peroxide dropwise into the reactor, stir for 3 hours, then add 800 grams of ethylenediamine, react at 150°C for 6 hours, remove unreacted substances under reduced pressure, and obtain modified waste oil;
[0019] Add 100 grams of the prepared modified waste oil into the reactor, then add 10 grams of potassium hydroxide into the reactor, heat up, and feed 500 grams of ethylene oxide, control the temperature at 170 ° C, and maintain the pressure at 0.3 Below MPa, make it fully rea...
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