Natural antibacterial textile containing extract of Baikal skullcap root and preparation process thereof
A Scutellaria baicalensis extract, natural antibacterial technology, applied in the field of textiles, to achieve good antibacterial rate, obvious antibacterial effect, and simple preparation process
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Embodiment 1
[0019] Example 1 A preparation method of natural antibacterial textiles containing Scutellaria baicalensis extract
[0020] (1) Preparation of microcapsules: Weigh 10 parts of Scutellaria baicalensis extract, 1 part of polyvinyl alcohol, 30 parts of glutaraldehyde, and 2 parts of emulsifier, mix the scutellaria baicalensis extract and polyvinyl alcohol aqueous solution, mix well and inject 1 part of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed, and the rotation speed is 700r / min to prepare emulsion A; mix glutaraldehyde with 5 drops of 10% hydrochloric acid aqueous solution, mix well and inject another part of the continuous phase n-hexane containing 1 part of emulsifier High-speed emulsification in alkanes, rotating speed 700, to prepare emulsion B; mix the two emulsions A and B at 10°C, and stir at high speed for 0.5h, filter, wash with petroleum ether for 3 times, and freeze-dry at -10°C to obtain microcapsules;
[0021] (2) Use the print...
Embodiment 2
[0029] Embodiment 2 A kind of preparation method of natural antibacterial textile containing Scutellaria baicalensis extract
[0030] (1) Preparation of microcapsules: Weigh 30 parts of Scutellaria baicalensis extract, 10 parts of polyvinyl alcohol, 60 parts of glutaraldehyde, and 30 parts of emulsifier, mix the scutellaria baicalensis extract and polyvinyl alcohol aqueous solution, mix well and inject 15 parts of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed and the rotation speed is 2500r / min to prepare emulsion A; mix glutaraldehyde with 10 drops of 30% hydrochloric acid aqueous solution, mix well and inject another part of the continuous phase n-hexane containing 15 parts of emulsifier Emulsion B was prepared by high-speed emulsification in alkanes at a speed of 2500r / min; the two emulsions A and B were mixed at 30°C, stirred at high speed for 2 hours, filtered, washed 5 times with petroleum ether, and freeze-dried at -5°C to obtain microc...
Embodiment 3
[0039] Embodiment 3 A kind of preparation method of natural antibacterial textile containing Scutellaria baicalensis extract
[0040] (1) Preparation of microcapsules: Weigh 20 parts of scutellaria baicalensis extract, 5 parts of polyvinyl alcohol, 40 parts of glutaraldehyde, and 20 parts of emulsifier, mix the scutellaria baicalensis extract and polyvinyl alcohol aqueous solution, mix well and inject 10 parts of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed and the rotation speed is 2000r / min to prepare emulsion A; mix glutaraldehyde with 7 drops of 20% hydrochloric acid aqueous solution, mix well and inject another continuous phase n-hexane containing 10 parts of emulsifier Emulsion B was prepared by high-speed emulsification in alkanes at a speed of 2000r / min; the two emulsions A and B were mixed at 20°C, stirred at high speed for 1 hour, filtered, washed 4 times with petroleum ether, and freeze-dried at -8°C to obtain microcapsules;
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