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Liquor ethanol concentration online detection method of traditional Chinese medicine alcohol precipitation process

A technology of ethanol concentration and alcohol precipitation process, which is applied in measuring devices, specific gravity measurement, instruments, etc., can solve problems such as inaccurate control and inability to detect ethanol concentration online, achieve automatic production, improve batch stability and product quality Effect

Active Publication Date: 2014-12-24
苏州浙远自动化工程技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to provide an online detection method for the ethanol concentration of the medicinal liquid in the alcohol precipitation process of traditional Chinese medicine, so as to solve the problem that the ethanol concentration of the traditional Chinese medicine alcohol precipitation process cannot be detected online and lead to inaccurate control, so as to be used for judging the end point of the alcohol precipitation process. for precise control

Method used

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  • Liquor ethanol concentration online detection method of traditional Chinese medicine alcohol precipitation process
  • Liquor ethanol concentration online detection method of traditional Chinese medicine alcohol precipitation process
  • Liquor ethanol concentration online detection method of traditional Chinese medicine alcohol precipitation process

Examples

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Effect test

Embodiment 1

[0023] Put 20,000 ml of antiviral extract with a density of 1.22 at room temperature into the alcohol precipitation tank, turn on the stirring paddle 11, and slowly add 95% ethanol. Turn on the alcohol precipitation liquid output pump 9, transfer the alcohol precipitation mixed liquid to the mixed liquid sedimentation tank 2, filter through the filter plate 6 with a hole diameter of 120 μm, filter the medicinal liquid through the filter plate 6 through the filter screen 7 with a hole diameter of 90 μm, pass The liquid medicine in the filter screen 7 is then filtered through the filter head 8 with a pore size of 50 μm. When the liquid medicine appears in the vent hole 5 , the valve of the vent hole is closed, and the clear liquid enters the clear liquid measuring cell 3 . Open the sampling valve 12, take a sample every 1 minute, measure its ethanol concentration with an ethanol concentration meter, and read the density of the corresponding clear liquid sample online in real time...

Embodiment 2

[0028] Put 30,000 ml of orange red extract with a density of 1.25 at room temperature into the alcohol precipitation tank, open the stirring paddle 11, and slowly add 95% ethanol. Turn on the alcohol precipitation liquid output pump 9, transfer the alcohol precipitation mixed liquid to the mixed liquid sedimentation tank 2, filter through the filter plate 6 with a pore size of 140 μm, filter the medicinal liquid through the filter plate 6 through the filter screen 7 with a pore size of 100 μm, and pass The liquid medicine in the filter screen 7 is filtered through the filter head 8 with a pore size of 60 μm. When the liquid medicine appears in the exhaust hole 5 , the valve of the exhaust hole is closed, and the clear liquid enters the clear liquid measuring cell 3 . Open the sampling valve 12, take a sample every 1 minute, measure its ethanol concentration with an ethanol concentration meter, and read the density of the corresponding clear liquid sample online in real time thr...

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Abstract

The invention discloses a liquor ethanol concentration online detection method of a traditional Chinese medicine alcohol precipitation process. The liquor ethanol concentration online detection method comprises the following steps of firstly, pouring Chinese medical extract into an alcohol precipitation tank; starting an agitator blade; adding ethanol and mixing with the Chinese medical extract to obtain alcohol precipitation mixing solution; then starting an alcohol precipitation liquid output pump, transferring the alcohol precipitation mixing solution to a mixed solution settlement tank to obtain clear liquid after multi-stage filtering; transferring the clear liquid to a clear liquid determination pool; finally conveying the clear liquid to the alcohol precipitation tank by a clear liquid reflux pump to form a cycle; determining the density of the clear liquid in the clear liquid determination pool through an on-line densimeter online in real time; calibrating the concentration of ethanol in the clear liquid and the density of the clear liquid; building a corresponding function relation of the ethanol concentration and the density of the clear liquid in the clear liquid; and determining the ethanol concentration in the clear liquid through the corresponding function relation online in real time. Real-time online detection of the liquor ethanol concentration in the alcohol precipitation process is achieved; the liquor ethanol concentration online detection method can be applied to endpoint determination of the alcohol precipitation technology; and the batch stability and the product quality of the alcohol precipitation technology are improved.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicine pharmaceutical technology, in particular to a traditional Chinese medicine alcohol precipitation process, and relates to an on-line detection method for the alcohol concentration of medicinal liquid in the traditional Chinese medicine alcohol precipitation process. Background technique [0002] The ethanol concentration measurement in the alcohol precipitation process of the former traditional Chinese medicine generally adopts manual manual detection. During the detection process, it is easy to contaminate the liquid medicine, resulting in inaccurate measurement and affecting the quality of the liquid medicine. SUMMARY OF THE INVENTION [0003] The object of the present invention is to solve the problems such as inaccurate control due to inaccurate control that cannot be detected on-line in the present alcohol precipitation process of traditional Chinese medicine, and provides a method...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N9/36
Inventor 刘雪松陈勇李页瑞李强华王龙虎栾连军吴永江
Owner 苏州浙远自动化工程技术有限公司
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