Antibacterial combination and preparation method thereof as well as application of antibacterial combination in preparation of antibacterial paper

A technology of antibacterial composition and antibacterial paper, which is applied in the field of antibacterial paper preparation and antibacterial composition, and can solve the problems that the application value of antibacterial activity has not been effectively applied.

Active Publication Date: 2014-07-02
YUNNAN YUXI TIPPING PAPER FACTORY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0012] At present, Atractylodes stearin is mainly used as a fixative rather than an antibacterial agent in the food industry,

Method used

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  • Antibacterial combination and preparation method thereof as well as application of antibacterial combination in preparation of antibacterial paper
  • Antibacterial combination and preparation method thereof as well as application of antibacterial combination in preparation of antibacterial paper
  • Antibacterial combination and preparation method thereof as well as application of antibacterial combination in preparation of antibacterial paper

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0059] Antibacterial activity of atractylodes stearin, silver-loaded antibacterial agent and their combination:

[0060] (1) Material

[0061] Atractylodes stearin, the dried rhizome of Atractylodes lanceolata on the market, the total volatile oil extract prepared by steam distillation according to the appendix method of the Chinese Pharmacopoeia (yield 6.3%), the sum of its atractylol and eucalyptol content detected by GC-MS is 75.6%;

[0062] Silica-loaded silver antibacterial agent, prepared according to the literature method (Journal of Tianjin University. 2002; 35(2): 247~249; CN1308866A), and the elemental silver and / or silver ion content is 1.98%.

[0063] (2) Antibacterial composition preparation

[0064] Prepare the antibacterial composition according to the following formula:

[0065]

A1

A2

A3

A4

A5

A6

A7

Atractylodes stearin

2.00g

1.00g

0.50g

0.25g

0.10g

0.05g

--

Silver-containing antibacterial agent

--

1.00g

1.50g

1.75g

1.90g

1.95g

2.00g

Food grade paraffin

2.00g...

Embodiment 2

[0079] Antibacterial ink and antibacterial paper printing:

[0080] (1) Material

[0081] Atractylodes stearin, dried rhizomes of Atractylodes lanceolata, supercritical CO 2 The total volatile oil extract prepared by extraction (1kg Atractylodes lanceolata dried rhizome granules is put into a supercritical fluid extractor, with a flow rate of 35kg / h, a static extraction at a temperature of 50℃ and a pressure of 20MPa for 1hr, and a dynamic extraction for 3hr. The separation pressure is 10MPa and the temperature is 40 At ℃, the volatile oil is precipitated. The yield is 5.5%), and the sum of the atractyl alcohol and eucalyptol content detected by GC-MS is 83.2%;

[0082] Silver-loaded antibacterial agent, IONPUREIPL, Ishizuka Glass Co., Ltd product (Ishizuka Glass Co., Ltd.), with calcium magnesium phosphate borate as inorganic silver carrier,

[0083] Silver-magnesium-calcium-phosphate-borate-glass, its inorganic silver, namely elemental silver and / or silver ion content is about 2.2%;...

Embodiment 3

[0096] Antibacterial composition and its antibacterial spectrum test:

[0097] (1) Material

[0098] Atractylodes stearin, the ethanol reflux extract of the dried rhizome of Atractylodes lanceolata on the market, the sum of the atractylol and eucalyptol content detected by GC-MS is 53.2%;

[0099] Silver-loaded antibacterial agent, silver-loaded antibacterial agent with zeolite as a carrier, self-made by reference (Zhong Zehui et al., Packaging Engineering, 2012; 33(1): 49~53), its inorganic silver is elemental silver and / or silver ion content It is about 1.8%.

[0100] (2) Preparation of antibacterial composition

[0101] After melting 0.5 g of atractylodes stearin into 250 ml of 95% ethanol, adding 3 g of silver-carrying antibacterial agent and stirring and mixing to obtain an antibacterial composition suspension.

[0102] (3) Antibacterial activity detection

[0103] The above-mentioned antibacterial suspension according to 80ml / m 2 The amount is applied to food packaging paper, the p...

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PUM

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Abstract

The invention relates to an antibacterial combination and a preparation method thereof as well as application of the antibacterial combination in preparation of antibacterial paper. The antibacterial combination contains atractylodes oil and an inorganic silver antibacterial agent. The antibacterial combination disclosed by the invention is sprayed on the surface of a piece of proper paper to prepare the antibacterial paper; the antibacterial paper can be used as food packaging paper, tobacco tipping paper and the like.

Description

Technical field [0001] The invention belongs to the field of chemistry and chemical engineering, and specifically relates to an antibacterial composition, its preparation method and its use in the preparation of antibacterial paper. The antibacterial composition contains atractylodes stearin and an inorganic silver antibacterial agent. The antibacterial paper can be prepared by spraying the antibacterial agent on the surface of a suitable paper. The antibacterial paper can be used as food packaging paper, tobacco tipping paper, and the like. Background technique [0002] With the continuous improvement of people's research and understanding of environmental microorganisms, while using the benefits of microorganisms, they are also very vigilant about their harmfulness as pathogens. In the long river of human history, various infectious diseases of various sizes have been prevalent in different periods and in different regions. These diseases have seriously threatened the survival ...

Claims

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Application Information

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IPC IPC(8): A01N65/12A01P1/00C09D11/106C09D11/14C09D11/102D21H27/00D21H27/10A01N59/16
Inventor 何金星李姿高娜
Owner YUNNAN YUXI TIPPING PAPER FACTORY
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