Wine fried herba siegesbeckiae detection method
A technology of wine-roasted sagebrush and detection method, which is applied to measurement devices, instruments, material analysis by electromagnetic means, etc., can solve problems such as UPLC-Q-TOF/MS reports that have not yet been seen, and achieve clear distinction and separation. Good speed, short time-consuming effect
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[0031] Embodiment: detection method
[0032] 1. Experimental reagents
[0033] Methanol is chromatographically pure, from Fisher Corporation of the United States;
[0034] Ultrapure water was prepared by laboratory ELGA PURELAB Classic-UVF pure water machine, which was purchased from the UK;
[0035] All other reagents were commercially available domestic analytical grade.
[0036] 2. Experimental samples
[0037] Wine-steamed Scutellaria: According to the pharmacopoeia method, that is, the 2010 edition of "Chinese Pharmacopoeia" contains wine-steamed Scutellaria, and it is stipulated that for every 100kg of Scutellaria, use 20kg of rice wine and steam it thoroughly according to the wine steaming method (Appendix Ⅱ D). The specific method Method: take clean medicinal materials, add wine, mix well, put in a pot, stir-fry with a slow fire to the specified level, take it out, and let it cool.
[0038] Raw weed grass.
[0039] 3. Experimental conditions
[0040] 3.1 The chro...
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