Method for determining lead, cadmium, chromium and mercury in plastic through EDTA-2Na complexation digestion
An edta-2na, plastic technology, which is used in the preparation of test samples, material excitation analysis, thermal excitation analysis, etc., can solve the problem that mercury cannot be measured, and achieve the purpose of preventing mercury loss, effective analysis results, and avoiding precipitation. Effect
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[0023] The measuring instrument used in this method is: ICP-OES710-OES type inductively coupled plasma atomic emission spectrometer, the working conditions are: emission power: 1.20kW; plasma gas: 15.0L min -1 ;Auxiliary air flow: 1.50L min -1 ; Atomizing gas: 200kPa; One reading time: 5s; Stabilization time: 15s.
[0024] SM200 anti-heavy metal pollution type rotary grinder is equipped with a special bottom sieve without heavy metal pollution grinding, the sieve hole is 0.5mm; Zhejiang Shangyu Daoxu Wusi Instrument Sand Screen Factory national standard inspection sieve, the hole diameter is 0.5mm. In addition, for comparison, the traditional wet digestion instrument ----- EH35B intelligent sample digester should be used when testing the comparative example.
[0025] In addition, prepare lead, cadmium, chromium mixed element standard solution, mercury single element standard solution are 50mg L -1 .
[0026] The reagents used in the present invention are all high-grade pure...
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