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207results about How to "Meet the testing requirements" patented technology

Method for simultaneously measuring elements of silicon, aluminum, calcium and barium

The invention discloses a method that can simultaneously analyze various elements, aims at solving the defects that currently the analysis of various elements cannot be finished at one time, and consequently the analysis time is long and the reagent usage is large, and discloses a method that can simultaneously measure the elements of silicon, aluminum, calcium and barium and comprises the following steps: a test sample is preprocessed through the acid dissolution method, microwave-digested, naturally cooled, and then placed into a volumetric flask with scales, diluted and shaken until well distributed, a solution with a standard working curve is prepared, an atomic emission spectrograph of inductance coupled plasmas is started and led to reach the measurement requirement, a plasma torch is lighted, the relative standard deviation of the plasma torch is led to be less than 5 percent, wavelength of each element is chosen, the working curves are plotted, and the content of each element is computed. The method combines the microwave digesting sample dissolution technique with the atomic emission spectrograph of inductance coupled plasmas, can simultaneously analyze nine elements including silicon, etc., is accurate and quick, has greatly reduced reagent usage, and reduces the environmental pollution that is caused by chemical reagents.
Owner:武钢集团有限公司

Automatic detection method for oblique incidence wave technology steel plate and device thereof

The invention aims at providing an automatic detection method of an oblique incidence body wave technical steel plate, which carries out comprehensive and fast detection to steel plates with the thickness of less than 75mm and accurately detects various defects, and a device thereof, and the device consists of an electromagnetic ultrasonic detection unit and a circuit system. The invention adopts the oblique incidence body wave mode to carry out detection to the steel plates, which not only is more sensitive to the detect in size, but also can detect the defects of cracks and the like, thus having more comprehensive detection result. The detection unit adopts a mode that transverse arrangement and longitudinal arrangement are combined, thus being more sensitive to the defects of the transverse and the longitudinal direction. The invention combines an ultrasonic transmission method and a reflection method, which not only has higher sensitivity to the defects, but also can position the defects precisely, thus having higher confidence level of the detection result. The invention has wider range for detecting the thickness of the wall of the steel plate, with the highest of 75mm, thus meeting the requirements for the steel plate with thick wall.
Owner:HARBIN INST OF TECH

Milk and milk product tetracycline antibiotic residual quantity checking method

The invention relates to a method for detecting the residue amount of terracycline antibiotics in milk and dairy products. The method utilizes an ultra performance liquid chromatography - electrospray tandem triple quadrupole mass spectrometer to determine the residue amount of the terracycline antibiotics. The method is as follows: a sample is extracted from Na2EDTA-McIlvaine buffer solution (pH4.0); proteins are removed by trichloroacetic acids; a columella is extracted through an HLB solid phase and then purified and enriched; the sample is separated by a chromatographic column, with the column temperature of 30 DEG C; gradient elution is performed by utilization of water solution (v/v) which contains 0.1 percent of methanoic acids and acetonitrile as a moving phase; and quantitative detection is performed by adoption of the multi-reaction monitoring means. The detection limit of instruments is between 1.0 and 2.0 mu g/kg; a related coefficient r reaches over 0.999 within the linear range of between 1 and 100 mu g/kg; and the recovery rate is between 81.7 and 100.7 percent (the addition levels are 10 mu g/kg, 50 mu g/kg and 100 mu g/kg). The method has the advantages of quickness, accuracy, high sensitivity and wide application scope.
Owner:INNER MONGOLIA MENGNIU DAIRY IND (GRP) CO LTD

Piston molded line cam lift synthetic checking instrument

InactiveCN101251370AImprove versatilityPrecision Rotary TorqueUsing optical meansGratingCoupling
The invention discloses a comprehensive inspection instrument for a piston profile cam lift range. A guide rail platform of a machine body is horizontally connected with a spindle drum and a tailstock, and is longitudinally connected with a bottom plate of a length measuring instrument, the left end of a driver seat on the spindle drum is provided with a round grating rotary encoder the middle of which is provided with an elastic slice winding a coupling to bear the torque force; a motor is connected with a worm and worm wheel mechanism, a pinion on a worm-wheel shaft is meshed with a gear outside the right side of the spindle drum, the gear is connected with an eccentric chuck, a catch plate and a lathe dog; a sliding shaft is arranged in a transition sleeve at the middle of the tailstock, a finial spindle is connected with a screw through a spring, the right side of the tailstock is provided with a shift fork device; the middle of a grating fixing base is provided with an adjusting screw, a compression spring and a measuring rod are arranged in the rear cavity of the adjusting screw, the grating fixing base is provided with a length grating ruler and a grating sensor; the round grating rotary encoder and the grating sensor are connected with a digital display control device. The comprehensive inspection instrument solves the problems that the prior art is not universal, time consuming and difficult in maintenance, and has the characteristics of high detection efficiency and measurement accuracy, long service life and low cost.
Owner:安徽华祥实业有限公司

Soil sample treatment device with vibration drying function for environmental detection

The invention discloses a soil sample treatment device with a vibration drying function for environmental detection. The soil sample treatment device comprises a casing, wherein a feeding hole is formed in the top of the casing; a pair of grinding rollers is arranged in the casing below the feeding hole; centers of the grinding rollers are supported by grinding roller shafts; a plurality of grinding teeth are uniformly arranged on the circumferences of the grinding rollers; an intercepting screen is arranged below the grinding rollers and is arc-shaped, and a bulge is formed in the center of the intercepting screen; a grinding plate is arranged below the intercepting screen; the grinding plate comprises a horizontal plate and an arc plate; the horizontal plate and the arc plate are spliced; a grinding roller is arranged above the horizontal plate; a vibration plate is arranged below the grinding plate; a resistive heater is arranged in the vibration plate; a vibration device is arranged in the middle on the lower side of the vibration plate and comprises a rack; the lower side of the rack is fixedly connected with the middle on the lower side of the vibration plate. The soil sample treatment device disclosed by the invention has the beneficial effects that soil is subjected to stepwise grinding treatment, so that the soil granularity meets a detection requirement.
Owner:郑州永泰澳新商贸有限公司

Meta-zinc tetraphenylporphyrin-based electrogenerated chemiluminescence body as well as preparation method and application thereof

The invention discloses a meta-zinc tetraphenylporphyrin-based electrogenerated chemiluminescence body. The chemiluminescence body is prepared from aniline imidazole, footballene pyrrolidine tricarboxylic acid and meta-zinc tetraphenylporphyrin. The invention also provides a preparation method of the chemiluminescence body, comprising the step that on the commercial footballene pyrrolidine tricarboxylic acid, reacting with the meta-zinc tetraphenylporphyrin in an axial coordination way by taking the aniline imidazole as a bridging object, so as to generate the efficient and stable novel electrogenerated chemiluminescence body. On this basis, according to the envelope characteristics of beta-cyclodextrin molecules, a stable electrogenerated chemiluminescence biological sensing system with beta-cyclodextrin enveloping fixed chemiluminescence body molecules is designed and built, realizes high sensitivity and high specificity detection on DNA (deoxyribonucleic acid), and is stable in electrogenerated chemiluminescence output signal and lower in detection lower limit. The detection system can be applied to biological medicine, clinical diagnosis, environmental monitoring and the like.
Owner:迈科若(苏州)医疗科技有限公司

Detection method for trace amount of organic tin in marine products

InactiveCN105181874AImprove extraction efficiencyImprove derivation efficiencyComponent separationPre treatmentPeak area
The invention belongs to the technical field of marine product detection, and particularly relates to a method for determining the trace amount of organic tin in marine products. The method comprises the steps that a to-be-determined sample is ground into powder after being preprocessed, the powder is soaked, extracted, frozen, purified, derived, processed through a cleanert florisil column and concentrated to obtain a to-be-determined sample solution; series of different-concentration organic tin mixed standard solutions are added in equivalent blank matrixes same as a sample matrix, soaked for a certain time and then processed through the mode same as the sample; a gas chromatography-tandem mass spectrum detection system is adopted to determine the standard mixed solutions, and a working curve is drawn; the to-be-determined sample solution is determined, the peak area ratio is obtained from a chromatogram chart of the to-be-determined sample solution, regression is performed on the working curve to obtain regression values, and then the concentration of all target objects in the to-be-determined sample can be calculated. The detection method can determine the concentration of butyltin and triphyltin simultaneously, is sensitive, accurate, rapid, simple and convenient and can be applied to detection of the organic tin in the marine products.
Owner:TONGJI UNIV

Method and device for detecting solid fraction and final stage of solidification of continuously cast slab

The invention discloses a method for detecting solid fraction and final stage of solidification of a continuously cast slab. The method comprises the following steps of: (1) applying oscillation excitation to the continuously cast slab, so that the continuously cast slab generates elastic deformation under oscillation excitation; (2) measuring the strain of elastic deformation of the continuously cast slab, the stress loads applied on the continuously cast slab by oscillation excitation, and the stress/strain phase difference of elastic deformation of the continuously cast slab with oscillation excitation after the continuously cast slab generates resonance to oscillation excitation; (3) calculating dynamic modulus of the continuously cast slab; and (4) obtaining the solid fraction and final stage of solidification of the continuously cast slab according to a solid fraction and dynamic modulus characteristic curve of the continuously cast slab. The invention also discloses a device for detecting solid fraction and final stage of solidification of a continuously cast slab. The method and the device provided by the invention can conduct nondestructive online measurement on the continuously cast slab, and can improve the solid fraction detection accuracy as well as the location accuracy of final stage of solidification of the continuously cast slab.
Owner:中冶赛迪电气技术有限公司

Method for simultaneously detecting 15 antibiotics in aquaculture sediment by combining microwave extraction-solid phase extraction pretreatment with liquid chromatography-mass spectrometry technology

The invention relates to a method for simultaneously detecting 15 antibiotics in aquaculture sediment by combining microwave extraction-solid phase extraction pretreatment with a liquid chromatography-mass spectrometry (LC-MS) technology. The method comprises the following steps: step (1) pretreating sediment samples, adding internal standard substances sulfamethoxazole-13C6, norfloxacin-D5, penicillin G potassium salt-D5, tetracycline-D6, olaquindox-D4, amoxicillin-13C6 and trimethoprim-D3 indicating a recovery rate, adding an acetonitrile-phosphate buffer solution for microwave extraction ofextraction liquid; step (2) performing solid phase extraction, enrichment and purification on target antibiotics; and step (3) quantitatively detecting 15 antibiotics of seven types in sediment witha liquid chromatograph/mass spectrometer. The method can simultaneously detect residues of 15 antibiotics containing 8 new antibiotics in the aquaculture sediment at a time by optimizing the internalstandard substances, screening appropriate pretreatment method and optimizing detection conditions, and has the advantages of high recovery rate, high sensitivity, high stability, low detection limit,more true and reliable detection results and the like.
Owner:SHANGHAI ACADEMY OF ENVIRONMENTAL SCIENCES

Universal seat detecting device

The invention discloses a universal seat detecting device, which comprises a detecting platform, two seat front leg fixing seats, two seat back leg fixing seats, two seat handrail detecting plate fixing seats, two seat backrest detecting plate fixing seats, two handrail detecting plates and two backrest detecting plates, wherein coordinate lines are engraved on the detecting platform; the two seat front leg fixing seats, the two seat back leg fixing seats, the two seat handrail detecting plate fixing seats and the two seat backrest detecting plate fixing seats are fixed on the detecting platform; the two seat front leg fixing seats are respectively used for fixing two front legs of an automobile seat; the two seat back leg fixing seats are respectively used for fixing two back legs of the automobile seat; the two seat handrail detecting plate fixing seats are respectively used for fixing the two handrail detecting plates; and the two seat backrest detecting plate fixing seats are respectively used for fixing the two backrest detecting plates; as the positions of four foundation fixing seats for fixing seat foundations can be randomly adjusted, good generality is obtained and detecting requirements of different seats can be satisfied; environment of the seats relative to a vehicle body can be detected; and the structure is simple, and the generality is excellent.
Owner:CHANGCHUN FAWAY ADIENT AUTOMOTIVE SYST CO LTD

Vapor headspace enrichment detection method for trace amount of volatile organic pollutants in seawater

The invention relates to a headspace gas chromatography detection technology, particularly discloses a vapor headspace enrichment detection method for a trace amount of volatile organic pollutants in seawater, and belongs to the technical field of water environment detection. The method sequentially comprises the four steps of water sample collection and storage, primary enrichment condensation, secondary enrichment condensation and headspace gas chromatography detection. According to the method, water vapor is used as sweeping gas, water is used as an absorbent, a water sample is secondarily distilled and condensed, and the condensed sample is enriched for headspace gas chromatography detection; a vapor headspace enrichment method is adopted, so that the using amount of an organic solvent in a process of enriching the volatile organic pollutants in the seawater is effectively reduced, and the interference of other components to a target object is prevented; an extraction process of the enrichment method is simple and convenient, the introduction of other solvents is avoided, the method is environment-friendly, low in limit of detection and high in recovery rate and reproducibility, and the requirements of detection of a trace amount of volatile organic pollutants in the seawater can be met.
Owner:MARINE FISHERIES RES INST OF ZHEJIANG

Molecular identification method for dalbergia odorifera chen in rosewood, and primer and probe of molecular identification method

The invention discloses an identification method for dalbergia odorifera chen in rosewood. According to the method, a primer, a probe and a molecular level PCR (polymerase chain reaction) detecting method are used, and the primer and the probe have exclusive specificity of the dalbergia odorifera chen. According to the method, detection sample capacity is low, proper DNA (deoxyribonucleic acid) information of wood serves as a basis, a species identification result of the dalbergia odorifera chen can be obtained quickly, accurately and objectively, and the shortcoming that the traditional identification method is high in subjectivity and is necessarily established on the basis that detected wood has a complete morphological structure which is easy to recognize is overcome. Therefore, the identification method can be used for performing enforcement detection for relevant departments such as an agriculture and forestry department, an industry and commerce department and an inspection and quarantine department, can also be used for consumer rights protection identification of a third-party detecting organization, and has an important role in standardizing markets, protecting consumer rights and interests and promoting protection and utilization of species resources.
Owner:THE INSPECTION & QUARANTINE TECH CENT ZHEJIANG ENTRY EXIT INSPECTION & QUARANTINE BUREAU
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