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404results about How to "Analytical results are reliable" patented technology

Iron alloy fusing sample preparation method for X-ray fluorescence spectrum analysis

The invention relates to an iron alloy fusing sample preparation method for X-ray fluorescence spectrum analysis, belonging to the technical field of materialization detection and aiming to solve the problem that fusing a film production alloy sample can erode a platinum crucible. The method comprises the steps of building up wall of the platinum crucible, preparing an oxidizing agent, pre-oxidizing an iron alloy sample and fusing and preparing sample from the iron alloy sample. The invention provides the fusing sample preparation method suitable for various iron alloys such as ferromanganese, silicomanganese, calcium silicon, ferrosilicon, ferromolybdenum, ferrotitanium, cymrite, ferrochrome, ferrocolumbium, ferrovanadium, silicon silicomanganese and the like. By adopting the method, a glass fusing piece can be manufactured without eroding the valuable platinum crucible, the sample can be completely oxidized in the sample preparation process, the sample preparation time is short, the prepared glass fusing piece is uniform and perfect, and the mineral effect and the granularity effect can be completely eliminated. The invention has safe and reliable method, simple and convenient operation and good repeatability, is suitable for various iron alloy samples and widens the application range of the fluorescence analysis.
Owner:HBIS COMPANY LIMITED HANDAN BRANCH COMPANY

Device and method for detecting attention focusing degree based on analysis of heart rate variability

The invention discloses a device and a method for detecting attention focusing degree based on the analysis of heart rate variability, mainly solving the problems of large interference and inconvenient testing of reference signals for attention judgment in the prior art. The method comprises the following testing steps: acquiring original electrocardiographic digital signals according to a MV5 lead mode; filtering the interference in the original electrocardiographic digital signals, extracting the position of a R wave and calculating heart rate variability signals; integrating and segmentingthe heart rate variability signals; performing empirical mode decomposition on each segment of the heart rate variability signals; calculating the approximate entropy of the heart rate variability signals and intrinsic mode function component signals; training a neutral network by using the calculated approximate entropy as an input vector of a reverse transmit neural network algorithm, and determining the parameters of codes of a neutral network; and detecting the attention focusing degree of a subject by utilizing the trained neutral network and outputting the test result. The invention hasthe advantages of large reference signal strength, convenient test and high accuracy, and is used for testing the attention focusing degree of a human body.
Owner:XIDIAN UNIV

X-ray fluorescence spectroscopy analysis fusion sample preparation method of aluminum, manganese, calcium and iron alloy

The invention discloses an X-ray fluorescence spectroscopy analysis fusion sample preparation method of an aluminum, manganese, calcium and iron alloy, which comprises the steps of: firstly, coating a uniform protection wall layer in a platinum crucible by using lithium tetraborate, then placing an aluminum, manganese, calcium and iron sample, an oxidizing agent, a lithium borate solvent and a releasing agent into the platinum crucible in which the protection wall is coated, uniformly mixing, and then pre-oxidizing the aluminum, manganese, calcium and iron sample; and finally, melting the pre-oxidized aluminum, manganese, calcium and iron sample, and cooling to obtain an aluminum, manganese, calcium and iron sample glass fuse piece, wherein the aluminum, manganese, calcium and iron sample is a detection sample or calibration sample of the aluminum, manganese, calcium and iron alloy, and the sample glass fuse piece is a detection sample glass fuse piece or calibration sample glass fuse piece of the aluminum, manganese, calcium and iron alloy. On the premise of no corrosion to the valuable platinum crucible, the glass fuse piece can be prepared, and the prepared sample is excellent and uniform, thus the mineral effect and the grain size effect are completely eliminated.
Owner:HBIS COMPANY LIMITED HANDAN BRANCH COMPANY

Construction method for compound thrombus clearing preparation bioactivity chromatography finger print

The present invention discloses a construction method for a compound thrombus clearing preparation bioactivity chromatography finger print. The construction method comprises the following steps: (1) preparing a compound thrombus clearing preparation test solution, precisely sucking 10 mul of the compound thrombus clearing preparation test solution, and injecting into a double-pump dual-gradient high performance liquid chromatograph to obtain a compound thrombus clearing preparation HPLC finger print; (2) preparing a mixed reference substance solution, precisely sucking 10 mul of the reference substance solution, and injecting into the double-pump dual-gradient high performance liquid chromatograph to obtain a reference substance HPLC finger print; (3) adopting a reference substance control method, and adopting an RRLC / MS / MS technical method to prove 21 chemical components in the finger print; and (4) analyzing correlation between the 21 chemical components and bioactivity difference, clarifying bioactivity component groups, and establishing a compound thrombus clearing preparation bioactivity chromatography finger print. According to the present invention, the compound thrombus clearing preparation HPLC finger print and the bioactivity component groups obtained from chromatograph efficiency analysis are combined to construct the compound thrombus clearing preparation bioactivity chromatography finger print so as to completely monitor safeties, effectiveness and quality uniformities of raw material herbs, semi-finished products and finished products.
Owner:SUN YAT SEN UNIV +1

Method for quickly determining gold, palladium, platinum, rhodium, iridium, silver, nickel, copper and iron in rare and precious metal system

The invention relates to a method for quickly determining gold, palladium, platinum, rhodium, iridium, silver, nickel, copper and iron in a rare and precious metal system. According to the detection principle of an inductively-coupled plasma-atomic emission spectrometry, the method comprises experimental conditions, sample treatment, working curve plotting, interference and elimination, detectionlimits and accuracy, wherein the experimental conditions comprise instrument selection, selection of analytical spectral lines, and determination of acidity of a system to be measured; the sample treatment comprises treatment and measurement of a test sample; the working curve plotting comprises preparation of a series of standard solutions, working curve plotting and calculation of analytical results; whether a spectral line of a coexistence element exists adjacent to the analytical spectral line of an element to be tested or not through the investigation and analysis of coexistence elementinterference is performed; determination is continuously performed for 11 times by using a blank solution excluding the element to be tested to obtain the detection limits and lower determination limits of the method; a precision experiment is conducted by repeatedly determining a sample for 11 times, and a standard recovery experiment of the sample is performed; and finally, compared with results obtained through the original determination method, the reliability of determined results of the method provided by the invention is further confirmed.
Owner:JINCHUAN GROUP LIMITED

Underground cavity analysis method considering nonlinear softening and dilation characteristics of surrounding rock

The invention discloses an underground cavity analysis method considering nonlinear softening and dilation characteristics of surrounding rock. According to the method, a hyperbolic softening model based on the characteristics of the Hoek-Brown criterion is established according to the characteristic that the strength parameter of the surrounding rock of a tunnel is weakened with the increasing of the strain of a plastic zone, the model is based on the characteristics of a resultant stress-strain curve of the surrounding rock, and reflects the nonlinear characteristics of the surrounding rock through example verification, the model is applied to analysis for the surrounding rock subjected to strain softening in underground construction, and a new method for an underground cavity analysis is established by considering the nonlinear softening and non-associated flow characteristics as well as a nonlinear failure criterion of a rock mass; the solutions of the stress of the underground cavity, the deformation of the cavity and the radius of the plastic zone are obtained; according to the method disclosed by the invention, the dilation characteristics of the surrounding rock are considered according to a non-associated flow criterion, and with regard to the deformations of the surrounding rock under different plastic models, application example results indicate that the strain dilation of a rock-soil material with dilation and strain softening is considered to be safe.
Owner:张斌伟 +1

Test method and test platform for performance of wind-photovoltaic-hydrogen comprehensive energy power generating system

The invention discloses a test method and a test platform for performance of a wind-photovoltaic-hydrogen comprehensive energy power generating system. The method comprises the following steps: establishing mathematic models of three parts, namely a windmill generator, a photovoltaic cell and a hydrogen cell; making the mathematic models into software modules and presetting the software modules and attribute parameters together into an industrial computer to design controllable simulation natural environment and test and calculate to obtain a performance theory curve of various parts of the power generating system; making a performance actual curve of the various parts through actual performance of the various parts; and comparing the curves to judge whether the performance of the comprehensive energy power generating system meets the requirement. The test method and the test platform can provide convenience for technicians to detect, analyze and study the working condition of the wind-photovoltaic-hydrogen comprehensive energy power generating system so as to perform optimization design on the wind-photovoltaic-hydrogen comprehensive energy power generating system, wherein the adopted novel mathematic model of the windmill generator can make analysis results more accurate and reliable.
Owner:CHONGQING UNIV

Method for evaluating damage accumulation inside steel structure thick plate

The invention provides a method for evaluating damage accumulation inside a steel structure thick plate. The method comprises the following steps that firstly, an elastoplasticity damage constitutive model for the steel structure thick plate is built, and the increment form of the model stress component is obtained through derivation; secondly, a corresponding material subprogram is complied for the increment form; thirdly, layered sampling is carried out on the steel structure thick plate in the thickness direction, and the elastoplasticity parameter and damage parameter of each layer of materials are determined; fourthly, a finite element model of the steel structure thick plate is built, the complied material subprogram is introduced into finite element analysis, and different material attributes are given to parameters of materials on different layers; the finite element model is loaded, the damage evolution course of the steel structure thick plate under the effect of the external load is simulated, and therefore corresponding evaluation is carried out. As for the characteristic that the steel structure thick plate is large in thickness, the damage evolution course of the thick plate under the effect of the external load is considered from the perspective of layered material properties, and the evaluation result better conforms to the real damage accumulation of the steel structure thick plate.
Owner:BEIJING JIAOTONG UNIV

Vibration stress numerical analysis method for turbomachinery blades

The invention discloses a vibration stress numerical analysis method for turbomachinery blades. The method comprises the steps of 1, building an FEM model of a solid region of an entire circle of the blades and CFD models of periodically symmetric fluid regions; 2, obtaining steady-state pressure intensity field distribution of meshes of the fluid regions of the blades and instant pressure intensity field distribution of each time step in a pneumatic period; 3, converting pressure intensity field distribution data; 4, performing finite element mode analysis of the entire circle of the blades; 5, obtaining node force load vectors of blade surfaces of all time steps; 6, solving a vibration displacement response by a mode superposition method; 7, expanding a displacement response result into a stress result; and 8, performing vibration stress result extraction and check. According to the method, the pressure intensity distribution of the blade surfaces is obtained by adopting a non-steady computing method, and an accurate air exciting-vibration force load is obtained by interpolation from the meshes of the fluid regions of the blades to the pressure intensity of the meshes of the solid region, so that the computing precision is improved; and each sector adopts a CPU+GPU heterogeneous parallel computing mode, so that the computing speed is greatly increased.
Owner:XI AN JIAOTONG UNIV

A method and an apparatus for end point detection in titration analysis

The invention discloses a method and an apparatus for end point detection in titration analysis. The method mainly comprises detecting the wavelength of transmission light of a test solution, and then based on the complementary color principle, showing the color of the test solution in the form of a wavelength of a color the same with the color, thereby to determine the end point of the titration analysis. The device comprises a sealing case, a small door is arranged on the box for placing the test solution to the sealing case, a small hole of a suitable size is disposed on the small door so that it is convenient for a person to dropwise add a standard solution into the test solution by a dropping device through the small hole, a magnetic stirrer is arranged below the small door, the test solution is placed on the magnetic stirrer, a while-light-emitting device is arranged beside the test solution to provide while light beam, a light wavelength detection device for detecting the wavelength of transmitted light of the test solution is arranged at the light-transmitting side of the test solution, the light wavelength detection device is electrically connected with a control cabinet, and the display screen of the control cabinet is arranged on the sealing case. According to the method and the apparatus, human errors are minimized, measurement precision is high, costs are low, reproducibility is good, and popularization is easy.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Method for determining content of lanthanum, cerium, praseodymium, neodymium and samarium in iron-containing dust sludge

The invention discloses a method for determining content of lanthanum, cerium, praseodymium, neodymium and samarium in iron-containing dust sludge. The method comprises the following steps: preparing a standard solution containing lanthanum, cerium, praseodymium, neodymium and samarium, preparing a rhodium internal standard solution, preparing a blank test sample with dissolved high-purity iron sample, and preparing a to-be-detected test sample with dissolved iron-containing dust sludge sample; introducing the standard solution into an inductance coupling plasma mass spectrometry to be measured to obtain a concentration calibration curve, then testing the blank test sample solution and the to-be-detected test sample solution in the inductance coupling plasma mass spectrometry, determining the concentration of the lanthanum, cerium, praseodymium, neodymium and samarium in the blank test sample and the to-be-detected test ample as CiO and Ci according to the concentration calibration curve, and then calculating the content of each element in the iron-containing dust sludge to-be-detected test sample according to the concentration difference value (Ci-CiO). The method has the characteristics of high sensitivity, high determination speed, simplicity in operation and small interference.
Owner:INNER MONGOLIA BAOTOU STEEL UNION

Clenbuterol hydrochloride assay kit and its preparation method and use method

The invention discloses a clenbuterol hydrochloride assay kit and its preparation method and use method. The clenbuterol hydrochloride assay kit comprises a kit body, a clenbuterol hydrochloride enzyme label plate, a clenbuterol hydrochloride standard solution, a clenbuterol hydrochloride enzyme conjugate, a diluent, a concentrated washing liquid, a first substrate and a second substrate. The preparation method provided by the invention comprises preparing the clenbuterol hydrochloride enzyme label plate, the clenbuterol hydrochloride standard solution, the clenbuterol hydrochloride enzyme conjugate, the diluent, the concentrated washing liquid, the first substrate and the second substrate. The use method provided by the invention comprises sample preparation, sample addition and detection, and detection result analysis. The clenbuterol hydrochloride assay kit has the advantages that sensitive, stable and reliable result analysis is realized; operation steps are less; sample pre-treatment is simple; adopted equipment can be popularized easily; and the clenbuterol hydrochloride assay kit can be utilized for determination of residual clenbuterol hydrochloride of pork, has sensitivity of 0.03 micrograms per kilogram, needs detection time shorter than detection time of an ELISA method by 30 minutes and satisfies requirements of rapid detection of clenbuterol hydrochloride residues.
Owner:QINGDAO HIGHTOP BIOTECH

Method for in-situ processing and structural characterization of composite inclusion in steel

The invention relates to a method for in-situ processing and structural characterization of a composite inclusion in steel. The method comprises the following steps: (1) accurately positioning and in-situ preparing a transmission electron microscope profile sample of an interesting composite inclusion by utilizing a focused ion beam; (2) analyzing element composition and element area distribution of the inclusion by virtue of an X-ray spectrometer attached on the transmission electron microscope; (3) obtaining a diffraction pattern of the low-index surface of each element gathered area in the inclusion by utilizing the electron diffraction technology of the transmission electron microscope; and (4) calibrating the phase corresponding to each diffraction spectrum by utilizing the diffraction pattern and combining the element composition and area distribution characteristics of the inclusion. According to the method, the phase distribution and composition of the interesting composite inclusion from core to surface can be quickly accurately obtained, a novel method is provided to studies on phase composition and formation mechanism inside the composite inclusion, and the defects of high randomness, low success rate, difficult inclusion completeness guarantee and the like of the composite inclusion transmission electron microscope sample can be overcome.
Owner:INST OF RES OF IRON & STEEL JIANGSU PROVINCE
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