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Filtrate loss reducer and application thereof to non-tackifying pure liquid-state CO2 sand fracturing

A fluid loss reducing agent, sand fracturing technology, applied in the field of oil fracturing, can solve the problems of corrosion of fracturing equipment, poor fracturing reformation effect, and reduced permeability, and achieves reduction of environmental pollution, shortened production period, Good effect of reducing filtration loss

Active Publication Date: 2017-06-13
RES INST OF SHAANXI YANCHANG PETROLEUM GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This type of hydraulic fracturing technology mainly has the following two defects: first, a large amount of water entering the reservoir will cause clay minerals to expand, disperse and migrate, resulting in reduced permeability and clogged pores; second, the huge water consumption makes fracturing difficult. The fluid flowback speed and flowback efficiency are low, and the fracturing effect is poor
However, in the pre-acid treatment in this process, the acid liquid is squeezed out. The acid liquid will cause corrosion of the fracturing equipment and increase the cost. Moreover, when the fracturing fluid is not completely flowed back, the residual acid liquid will cause certain damage to the reservoir. damage
[0007] Chinese application (CN 103924955 A) discloses a fracturing process using liquid CO 2 After initial fracturing, slick water is used for fracturing. Although the flowback period is shortened, this process still has the disadvantage of high water consumption, and the early acid treatment will cause certain losses to the equipment.

Method used

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  • Filtrate loss reducer and application thereof to non-tackifying pure liquid-state CO2 sand fracturing

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] 1. The fluid loss reducer is prepared from the following raw materials by weight: 15 g of 5# white oil, 0.7 g of NP-10, 0.3 g of TX-4, 2 g of octanoic acid, 3 g of KCl, and the mass concentration is 1% Carboxymethyl guar gum solution 5 g, water 12 g.

[0040] 2. The preparation method of the fluid loss control agent is as follows: Weigh the raw materials of each weight part, stir and mix 5# white oil and water, mix NP-10 and TX-4, add 5# white oil and water to mix After heating up to 50°C, add n-octanoic acid and stir, then add KCl and stir to dissolve, and finally add carboxymethyl guar gum solution with a mass concentration of 1%, let it stand for 5 hours, and set aside.

Embodiment 2

[0042] 1. The fluid loss control agent is prepared from the following raw materials by weight: 10g of 5# white oil, 0.5g of NP-10, 0.1g of TX-4, 10g of n-octanoic acid, 10g of KCl, carboxymethyl with a mass concentration of 1%. Base guar gum solution 15g, water 20g.

[0043] Its preparation method is with embodiment 1.

Embodiment 3

[0045] 1. The fluid loss reducer is prepared from the following raw materials in parts by weight: 25g of 5# white oil, 2g of NP-10, 1g of TX-4, 1g of n-octanoic acid, 1g of KCl, and carboxymethylguanidine with a mass concentration of 1%. Glue solution 4g, water 10g.

[0046] Its preparation method is with embodiment 1.

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Abstract

The invention discloses a filtrate loss reducer. The filtrate loss reducer is prepared from the following raw materials in parts by weight: 10-25 parts of 5# white oil, 0.5-2 parts of NP-1, 0.1-1 part of TX-4, 1-10 parts of n-caprylic acid, 1-10 parts of KCl, 4-15 parts of a carboxymethyl guanidine gum solution with the concentration of 1%. According to the filtrate loss reducer, the sand carrying capability of pure liquid-state CO2 fracturing liquid can be improved and the loss of the fracturing liquid is effectively reduced. Meanwhile, the invention further provides application of the filtrate loss reducer to a pure liquid-state CO2 sand fracturing process; the filtrate loss reducer is pumped into a stratum before pure liquid-state CO2 fracturing is constructed, and the sand fracturing is carried out; the filtrate loss reducer has the advantages of rapid backflow, increased backflow rate, shortened period of putting into production and the like; and water-based fracturing liquid does not need to be prepared in the process and backflow liquid does not need to be treated, so that the environment pollution degree is reduced, and the filtrate loss reducer has relatively good practical significance on regions with lacked water resources and regions with fragile ecological environments.

Description

technical field [0001] The invention belongs to the technical field of petroleum fracturing, in particular to a fluid loss reducer and its non-viscosifying pure liquid CO 2 Applications in sand fracturing. Background technique [0002] In China, unconventional oil and gas resources such as low permeability and ultra-low permeability are abundant. However, because the physical properties of unconventional reservoirs are generally poor, it is necessary to use reservoir stimulation technology to improve seepage conditions in order to achieve the purpose of effective production. [0003] The most commonly used reservoir stimulation technology is hydraulic fracturing technology, which uses water-based fracturing fluid to stimulate the reservoir. The hydraulic fracturing technology has problems such as large water consumption, damage to the reservoir by fracturing fluid residues, and incomplete flowback. defect. For example, the current fracturing method used in shale gas wells...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/68C09K8/90E21B43/267
CPCC09K8/68C09K8/90E21B43/267
Inventor 张锋三张军涛郭庆吴金桥申峰孙晓高志亮段玉秀景丰王卫刚杨先伦
Owner RES INST OF SHAANXI YANCHANG PETROLEUM GRP
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