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556results about How to "Reduce fluid loss" patented technology

Pumping stop sand setting fracture-height-controlling acid fracturing process method applicable to carbonate reservoir

The invention relates to a pumping stop sand setting fracture-height-controlling acid fracturing process method applicable to a carbonate reservoir. The method comprises the following work procedures that before the normal fracturing, low-viscosity slickwater is adopted for fracture making, and the initial fracture height is controlled; then, after the slickwater enters the stratum in a way of carrying support agent sand, the pumping stop is adopted for prompting the support agent sand to be settled near a fracture opening, so that each stage of support agent sand shields the back section in advance, a high-intensity artificial separation layer is formed, the stress state is changed, and the goal of effectively controlling the lower fracture height extending to prevent the communication with the lower part water body is achieved; low-viscosity fracturing fluid is injected for fracture making at a stable discharge capacity; after the fracturing fluid enters the stratum, acid liquid is injected for etching the stratum, and high-flow-guide capability artificial fractures are formed; after the acid liquid is extruded into the stratum, the pumping is stopped for measuring the pressure drop, and the construction is completed. The process has the advantages that the artificial separation layer can be formed, the fracture height vertical direction extending can be controlled, the stress state is changed, and the goals of effectively controlling the lower fracture height extending and preventing the communication with the lower part water body are achieved.
Owner:CHINA PETROLEUM & CHEM CORP

Acid fracturing process of oil gas well mining temperature control various mucic acid

ActiveCN101353958AReduce fluid lossEasy to form non-uniform etchingFluid removalDrilling compositionAcid etchingMucic acid
The invention relates to an acid fracturing method of a temperature-control and variable-viscosity acid in the exploitation of an oil-gas well, which comprises the steps that: a common chlorohydric acid pickling process is firstly used for removing the pollution of an embrasure; then, the temperature-control and variable-viscosity acid fracturing process, or an ahead-fluid temperature-control and variable-viscosity acid fracturing process, or a temperature-control and variable-viscosity acid fracturing enclosed acidizing process, or an ahead-fluid temperature-control and variable-viscosity acid fracturing enclosed acidizing process is adopted; the weight ratio of the components of the temperature-control and variable-viscosity acid are as follows: 100 portions of basic acid solution, 0.5 portion to 1.5 portions of the main agent of the temperature-control and variable-viscosity acid, 1 portion to 3 portions of a corrosion inhibitor of the temperature-control and variable-viscosity acid, 0.5 portion to 1 portion of an emulsion breaker, 0.5 portion to 1 portion of a ferric ion stabilizer and 0.5 portion to 1 portion of a high efficient discharge aiding agent; 2-percent KCL clear water is used for displacing the temperature-control and variable-viscosity acid into the stratum. The temperature-control and variable-viscosity acid is easily prepared on site, with low friction drag and strong pumpability, thereby being capable of being applied to high-discharge construction; under the high temperature condition of a storing layer, both the fresh acid and the residue acid have high viscosity, thus increasing the length of acid-etching cracks. After the construction is finished, the viscosity of the residue acid is reduced, which is beneficial to the back discharge of the residue acid.
Owner:PETROCHINA CO LTD

Controllable cross linked gel water blockage plugging material

The invention relates to a controllable cross linking gel water shutoff and lost circulation material used for oil-gas fields, which can block off a fractured, vuggy or malignant leaking formation and increase the strength and stability of gel. The technical proposal is as follows: acrylamide of certain amount is added into a breaker containing deionized water, after the acrylamide dissolved, N, N-methylene-bisacrylamide and initiating agent are added, the mixture stands still for 1h at room temperature after 0.5h of gelation, therefore, lump gel product is obtained and finally becomes gel particles after granulation, parching and sieving; the gel particles are then soaked in the solution of chromium trichloride, cross linker is fully absorbed in the gel particles, and the obtained material is dried for spare; the product is then added into the solution of polyvinyl alcohol and the packaged gel particles are obtained after packaging 1-3 times and drying; finally the packaged gel particles containing the cross linker are added into the solution of the water soluble polymer HPAM for slow cross linking reaction, thus obtaining quiescent strong gel. The material is characterized by simple manufacturing process, low cost, little filtration loss and good leak tightness and stability.
Owner:SOUTHWEST PETROLEUM UNIV

Tackifier for drilling fluid, and preparation method and application thereof

The invention provides a tackifier for a drilling fluid, and a preparation method and application thereof. The tackifier is a quadripolymer formed by polymerization of four alkene monomers, wherein the four alkene monomers are selected from a temperature-resistant salt-tolerant monomer, a hydrated monomer and an adsorptive monomer; the temperature-resistant salt-tolerant monomer is selected from an alkenyl sulfonic acid monomer; the hydrated monomer is selected from alkenyl carboxylic acid, alkenyl alkane ketone and double-bond-containing quaternary ammonium salt compounds; and the adsorptive monomer is selected from an alkenyl amide monomer. The tackifier provided by the invention can resist a high temperature of no less than 180 DEG C, is resistant to saturated salt, has remarkable tackifying effect, is low in toxicity and environmentally friendly, and can obviously improve the dehydration and wall building capability of the drilling fluid, thereby effectively reducing the dehydration. The invention solves the downhole complexity possibly caused by the fact that the drilling fluid system can not carry and suspend rock debris and thus can not clear boreholes in time due to reduced viscosity shearing force as a result of poor temperature resistance and salt tolerance of the tackifier in deep well, ultradeep well, horizontal well and extended reach well operations.
Owner:BC P INC CHINA NAT PETROLEUM CORP +2

High-temperature-resistant while-drilling plugging agent and preparation method thereof

The invention relates to a high-temperature-resistant while-drilling plugging agent and a preparation method thereof and belongs to the technical field of oil field chemical drilling fluid treating agents. The method comprises the following steps: preparing a stable emulsion from an oil soluble monomer A, an oil soluble crosslinking agent B, an azo-type initiator, an organic hydroperoxide and water in the presence of an emulsifier, and polymerizing the stable emulsion to obtain a powder M; and swelling the powder M by use of a swelling agent, adding a water soluble monomer C, a water soluble crosslinking agent D and a reductive initiator into the swelled powder M, and polymerizing the mixture at the room temperature to obtain the high-temperature-resistant while-drilling plugging agent. The high-temperature-resistant while-drilling plugging agent is in a powder shape, has relatively high temperature resistance, can resist the temperature up to 180 DEG C, and can be used for performing while-drilling plugging on deep wells and supper deep wells. The while-drilling plugging agent can be used for quickly effectively plugging the permeability leak, the micro order crack and gap leak, avoiding the repeated leak, participating in the formation of a filter cake, keeping the stability of a well wall and obviously reducing the drilling filler loss and the pollution to a reservoir, has no influence on the rheological property of the drilling fluid and has the advantages of good compatibility with various drilling fluid systems and relatively good combination property.
Owner:CHINA PETROLEUM & CHEM CORP +1

Filtrate loss reducer for high-temperature-resistant oil field drilling fluid and preparation method thereof

The invention relates to a filtrate loss reducer for high-temperature-resistant oil field drilling fluid, a preparation method of the filtrate loss reducer, and application of a treatment agent. A novel high-temperature-resistant filtrate loss reducer is synthesized by implementing the following steps: adopting lignin, acrylamide and 2-acrylamide-2-methyl propanesulfonate as synthetic monomers; enabling the synthetic monomers to perform graft copolymerization under the initiation of potassium peroxodisulfate, ammonium ferrous sulfate hexahydrate and hydrogen peroxide respectively; adding a crosslinking agent, namely N,N-methylene bisacrylamide to enhance the stabilizing force of the synthetic monomers under high temperature condition. The filtrate loss reducer disclosed by the invention adopts waste materials of a paper-making factory, is extensive in source and low in cost, and can be used for absorbing the excellent viscosity reduction capacity of lignin; the introduced acrylamide and 2-acrylamide-2-methyl propanesulfonate can be used for improving the precipitation capacity at a high temperature; N,N-methylene bisacrylamide is added as the crosslinking agent to ensure that a network structure is formed, the high temperature resistance can be improved, an oil and gas layer can be protected from collapsing, and the service life of an oil well can be prolonged. A product disclosed by the invention is applied to the oil field drilling fluid.
Owner:JILIN UNIV

Reversible Pickering emulsion, preparation method of reversible Pickering emulsion, and reversible high-temperature high-density drilling fluid

ActiveCN108841364ADoes not affect smooth reversalStability is not affectedDrilling compositionOil phaseAmine derivatives
The invention provides a reversible Pickering emulsion, and the reversible Pickering emulsion comprises an oil phase, an aqueous phase and a nanoparticle activated in situ by an amine surfactant or anamine derivative surfactant. The nanoparticle is a lipophilic, hydrophilic or amphiphilic nano oxide, and the amine surfactant is primary amine, secondary amine, tertiary amine surfactants or derivatives of the surfactants. The lipophilic nanoparticle is activated in situ by a short chain amine surfactant or a short chain amine derivative surfactant; the hydrophilic or amphiphilic nanoparticle isactivated in situ by a long chain amine surfactant or a long chain amine derivative surfactant. The invention further provides a drilling fluid comprising the emulsion. An enhancer for the drilling fluid is an amphiphilic hyperbranched polymer, the density of the prepared reversible high-temperature high-density drilling fluid is directly adjusted within 1.6g/cm<3> to 2.2g/cm<3>, and has the relatively excellent properties of rheological property, suspension stability, filter cake clearance, filter loss control, environmentally friendliness, and reversibility of a water-in-oil emulsion and anoil-in-water emulsion.
Owner:SOUTHWEST PETROLEUM UNIV

High-temperature-resistant high-density reversible water-in-oil/oil-in-water drilling fluid and preparation method thereof

The invention provides high-temperature-resistant high-density reversible water-in-oil / oil-in-water drilling fluid which is composed of the following raw materials in parts by weight: 30-70 parts of an oil phase, 30-70 parts of an aqueous phase, 2-5 parts of a reversible emulsifier, 1-3 parts of an auxiliary emulsifier, 0-2 parts of organic soil, 1-4 parts of a filtrate reducer, 0-1 part of an alkalinity regulator, 0-0.5 part of a wetting agent, 0-2 parts of an enhancer and 0-800 parts of weighting materials. The reversible emulsifier is fatty acyl polyamines and derivatives thereof, and has astructural general formula of R1(CH2)m(CONH)n(C6H4)x(NH)y(NH2)zR2; the filtrate reducer is an amphiphilic filtrate reducer. The amphiphilic filtrate reducer comprises but is not limited to an amphiphilic polymer filtrate reducer, a hydrophilic modified asphalt filtrate reducer and a hydrophobic modified humic acid filtrate reducer. The compounded auxiliary emulsifier is a high HLB (Hydrophile-Lipophile Balance) value surfactant. The drilling fluid disclosed by the invention has directly adjustable density of 0.8-1.8g / cm<3>, and has excellent properties such as rheological property, suspensionstability, filter cake clearance, filter loss control, environment friendliness and stable reversibility of water-in-oil emulsion and oil-in-water emulsion in a range of 100-180 DEG C.
Owner:SOUTHWEST PETROLEUM UNIV

Proppant-carrying acid fracturing method for high-temperature ultra-deep carbonate reservoir

The invention provides a proppant-carrying acid fracturing method for a high-temperature ultra-deep carbonate reservoir. The proppant-carrying acid fracturing method for the high-temperature ultra-deep carbonate reservoir comprises the following steps that (1) fracture forming is conducted through fracturing fluid; (2) ground crosslinked acid is adopted and is made to react with rock, so that an acid-etched fracture is generated in a formed fracture, and a proppant is carried with the ground crosslinked acid for supporting the acid-etched fracture; and (3) linear glue is used for replacement, and thus acid fracturing is completed. According to the proppant-carrying acid fracturing method for the high-temperature ultra-deep carbonate reservoir, the technique is simple, operation is convenient, and the construction effect is remarkable; and the proppant-carrying acid fracturing method is suitable for transforming construction of deep well carbonatite at the high temperature of 150-170 DEG C, a supporting fracture which has deep penetration and longer flow conductivity can be formed in a stratum, the productivity is increased and the production time is prolonged after acid fracturing and well fracturing, and the length of the formed fracture is larger than 120 m.
Owner:CHINA PETROLEUM & CHEM CORP +1
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