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236results about How to "Reduce apparent viscosity" patented technology

Method for preparing special aromatic polyoxadiazole and flame-retardant high-temperature resistant polyoxadiazole fiber thereof

The invention discloses a method for preparing special aromatic polyoxadiazole and flame-retardant high-temperature resistant polyoxadiazole fiber thereof. The special aromatic polyoxadiazole is prepared by the following method that the special aromatic polyoxadiazole is prepared from terephthalic acid, compound of which the structural general formula is expressed as formula I and hydrazine salt serving as monomers through condensation polymerization reaction. The polyoxadiazole fiber with high flame retardancy and high temperature resistance is prepared by using the special aromatic polyoxadiazole as a raw material. The fiber number of the prepared polyoxadiazole fiber is 1 to 20 dtex, the breaking strength is 2.5 to 5 cN.dtex-1, the elongation at break is 10 to 40 percent, the initial modulus is 50 to 250 cN.dtex-1, the moisture regain is 5.0 to 12.0 percent, the limited oxygen index is 30 to 38 percent, and the initial decomposition temperature is above 480 DEG C. The fiber can be widely used in the fields of protective products, filter materials, electric insulating materials, frictional sealed materials, various industrial textiles, high-temperature resistant paper, aviation and aerospace materials and the like.
Owner:JIANGSU BAODE NEW MATERIAL

Aqueous macromolecule-isocyanic ester stalk artificial board and preparation thereof

The invention relates to a water-based macromolecule-isocyanate straw hard board and a preparation method thereof. Straws of rice, wheat, corn or other crops, a water-based macromolecule-isocyanate adhesive and a straw interface performance modifying agent are used as raw materials, and the straws are treated by section cutting, kneading and modification, adhesive application and heat pressing to produce the water-based macromolecule-isocyanate straw hard board. A mixture ratio of the absolute dry straws to the water-based macromolecule-isocyanate adhesive to the straw interface performance modifying agent by weight is 100 to 10-16 to 0.05-0.15. The straw hard board uses the water-based macromolecule-isocyanate adhesive to replace a pure isocyanate adhesive, radically improves the problems of toxic organic volatiles, poor prepressing performance, adhesion on boards, etc., remarkably reduces cost and really realizes green production, and the raw materials after the treatment of kneading and modification have good prepressing and molding performances and high one-off qualified rate. The water-based macromolecule-isocyanate straw hard board has the characteristics of unique design, long active period, excellent aging, water and heat resisting performances, simple operation, easy availability of equipment, no environmental pollution, easy implementation, etc., and produces huge entironmental, social and economical benefits after the water-based macromolecule-isocyanate straw hard board is popularized.
Owner:BEIHUA UNIV

High temperature-resisting cleaning CO2 foam fracturing liquid suitable for unconventional oil and gas reservoir development

The invention discloses high temperature-resisting cleaning CO2 foam fracturing liquid suitable for unconventional oil and gas reservoir development. The high temperature-resisting cleaning CO2 foam fracturing liquid in gas phase is CO2; the high temperature-resisting cleaning CO2 foam fracturing liquid in liquid phase is high temperature-resisting cleaning fracturing liquid; the foam mass is 52 percent to 75 percent. The high temperature-resisting cleaning CO2 foam fracturing liquid is prepared from the following raw materials in percentage by weight: 0.3 to 0.65 percent of thickening agent, 0.2 to 0.5 percent of viscosity synergist, 0.2 to 0.3 percent of pH (Potential of Hydrogen) value modifier, 0 to 0.2 percent of high-temperature stabilizing agent, 0.01 to 0.1 percent of gel breaker and water, wherein the thickening agent is prepared from acrylamide, vinylpyrrolidone, maleic acid, anionic functional monomers, an initiating agent, inorganic salt and the like; the viscosity synergist is mainly prepared from an anionic surfactant; the pH value modifier is mainly prepared from an organic acid. According to the high temperature-resisting cleaning CO2 foam fracturing liquid disclosed by the invention, the temperature-resisting ability is up to 140 DEG C, the sand carrying performance is excellent, the frictional resistance is low, the foam stability is strong, the content of residual slag is extremely low, the stratum compatibility is good, back flowing is easy, the construction effect is quickly obtained, and important significances to effective development of an unconventional oil and gas reservoir and protection of a reservoir stratum are obtained.
Owner:CHENGDU BAICHUN PETROLEUM TECH

Ultralow-density oil-base drilling fluid and preparation method thereof

The invention relates to an ultralow-density oil-base drilling fluid. The invention is characterized in that the ultralow-density oil-base drilling fluid is prepared from the following raw materials: base oil, a density reducer, a suspension stabilizer, an emulsifier, a tackifier, a fluid loss additive, a flow pattern regulator, an alkalinity regulator and a calcium chloride water solution. The base mixed oil is prepared by the following steps: mixing 3# white oil, 5# white oil and natural gas prepared oil, adding a flash point enhancer while stirring, and standing for 0.5-1 hour; and stirring at low speed at the temperature of 30-40 DEG C, and slowly adding oil-soluble nano fumed silica while stirring, wherein the addition process is controlled at 2-3 hours. The ultralow-density oil-base drilling fluid has the advantages of favorable emulsifying stability, favorable rheological properties, high inhibition property for mud shale, high emulsion-breaking voltage, low filter loss, low density (0.75-0.90 g/cm<3>), and high sand carrying and pressure bearing capacities, is beneficial to cleaning the borehole and enhancing the mechanical drilling speed, solves the problem of severe lost circulation in the low-pressure formation and long-section shatter zone formation, and is especially suitable for low-pressure oil gas pools and depletion water-sensitive formations.
Owner:成都西油华巍科技有限公司 +1

Continuous micro-reaction device and method for preparing meta-aramid resin and product

A continuous micro-reaction device for preparing meta-aramid resin comprises a prepolymerization system, a polycondensation system, an after-treatment system and a heat exchange system, wherein the prepolymerization system, the polycondensation system and the after-treatment system are connected in sequence, and the heat exchange system is connected with the prepolymerization system and the polycondensation system to control temperatures of the prepolymerization system and the polycondensation system. The continuous micro-reaction device is characterized in that the prepolymerisation system comprises a raw material storage device, a micro-mixer and a micro-reactor which are connected in sequence; the polycondensation system comprises a multistage micro-screw device, and the micro-reactor is connected with multistage micro-screw device. The continuous micro-reaction device for preparing the meta-aramid resin improves the heat transfer effect at the polycondensation stage and the mass transfer effect at the polycondensation stage during preparation of the meta-aramid resin, and achieves the purpose of improving the performance of a meta-aramid resin product. The invention further provides a continuous micro-reaction method for preparing the meta-aramid resin and the product.
Owner:ZHUZHOU TIMES NEW MATERIALS TECH

Reel-to-reel hot roller coining forming method for micro-nano structure on surface of polymer

InactiveCN106113479AAccelerate filling flowReduce apparent viscosityMicro nanoPolymeric surface
The invention relates to a reel-to-reel hot roller coining forming method for a micro-nano structure on the surface of polymer. The reel-to-reel hot roller coining forming method comprises the steps that a polymer material is conveyed to a preheat roller from an unreeling device, preheated to the attaching temperature and attached to a base band in a hot pressing mode; the polymer material attached to the base band is conveyed to the position between a mold roller and a pressure roller and heated to the coining temperature through the mold roller heated in advance, and then a mold cavity is filled with the polymer material through the action of the pressure roller; mold filling and supersonic vibration assembly starting are conducted at the same time, and the reel-to-reel hot roller coining process is completed with assistance of supersonic vibration; the polymer material is conveyed out from the position between the mold roller and the pressure roller, and then cooled and separated from the position inside the mold roller; and after demolding is completed, a polymer product is continuously cooled, separation of the polymer product and the base band is achieved, and finally reeling is conducted. According to the reel-to-reel hot roller coining forming method for the micro-nano structure on the surface of the polymer, the reel-to-reel hot roller coining process is improved through supersonic vibration, the mold filling process is accelerated, the duplication precision is improved, and the demolding force and demolding deformation are reduced; and the reel-to-reel hot roller coining forming method is advanced.
Owner:SHANGHAI JIAO TONG UNIV

Starch graft copolymer coal-water slurry dispersants and preparation method thereof

The invention provides a preparation method of starch graft copolymer coal-water slurry dispersants. After oxidation modification of starch, in a redox system, sodium p-styrene sulfonate and a large monomer are introduced to a starch chain through free radical polymerization reaction to compound a series of coal-water slurry dispersants with excellent performance and unique characteristics. Chief constituents of the starch graft copolymer coal-water slurry dispersants are as follows, by mass: 8-20% of starch, 2-8% of oxidants, 10-30% of monomers and 2-4% of initiators. The starch graft copolymer coal-water slurry dispersants prepared by the method are brown sticky emulsion, the solid content is 26-38%, the pH value is 7-9, and the viscosity is 40-130mPa.s. The preparation method of the starch graft copolymer coal-water slurry dispersants exploits the advantages of strong dispersity of the sodium p-styrene sulfonate and carboxylate to the full and combines effects of hydrogen bond in water molecules and polyhydroxy on a starch straight chain and the space steric hindrance effect of a long chain of the large monomer to enable coal-water slurry to have good dispersion perfoamance and good storage stability. The dispersants can achieve biodegradation and have low toxicity, and raw materials of the dispersants are easy to obtain and low in cost.
Owner:SHAANXI UNIV OF SCI & TECH

Seven-level adjustable reciprocating type electrorheological fluid damper

A seven-level adjustable reciprocating type electrorheological fluid damper mainly comprises a positive-pole conducting wire, a negative-pole conducting wire, a positive-pole piston cylinder cover, a negative-pole piston cylinder cover, positive-pole conducting rubber, negative-pole conducting rubber, a piston rod, an insulating piston cylinder, a positive pole, a negative pole, a backflow control path, a small piston, a middle piston, a large piston and electrorheological fluid. The positive-pole conducting rubber and the negative-pole conducting rubber replace sealing materials and play a role in sealing and conducting. Installation forms of the small piston, the middle piston and the large piston are determined by borne damping force, wherein when the damping force is large, stress is not clear, and movement speed is high, the dual-piston or three-piston form is adopted; when the damping force is small, the single-piston form is adopted. The backflow control path replaces a throttling control valve, no external electric field exists, the electrorheological fluid bears the force and flows between the positive pole and the negative pole through the backflow control path, and the seven-level adjustable reciprocating type electrorheological fluid damper is a hydraulic damper; when an external electric field is applied and shearing efficiency is high, apparent viscosity of the electrorheological fluid of the backflow control path changes, the section area of the backflow control path becomes smaller, the backflow control path is even blocked completely, and the electrorheological fluid effectively controls an engineering system by proving shearing force and extruding force.
Owner:QINGDAO AGRI UNIV

Seven-stage adjustable rotary type electrorheological fluid brake

The invention provides a seven-stage adjustable rotary type electrorheological fluid brake. The seven-stage adjustable rotary type electrorheological fluid brake mainly comprises a positive pole conducting wire, a negative pole conducting wire, a bearing cap, a bearing, an end closure, conductive rubber, a half round key, a rotating shaft, an insulated shell, a positive pole, a negative pole, a backflow control channel, a small turntable, a middle turntable, a large turntable, electrorheological fluid and a flat key, wherein the installation type of the small turntable, the middle turntable and the large turntable is decided by suffered braking force, when the braking force is large, the stress is not clear and the rotating speed is high, the dual-turntable and three-turntable type is adopted; when the braking force is small, the single-turntable type is adopted; the backflow control channel is used for replacing a throttling control valve, an external electric field is not applied, and the electrorheological fluid is stressed, flows between the upper part and the lower part of the insulated shell through the backflow control channel and is a hydraulic brake; when the external electric field is applied and the high shear rate is adopted, the apparent viscosity of the electrorheological fluid of the backflow control channel changes, so that the sectional area of the electrorheological fluid becomes small till being completely closed; and the electrorheological fluid realizes the effective brake on an engineering system by providing shear force and extrusion force.
Owner:QINGDAO AGRI UNIV

Coal gangue-based composite geopolymer grouting filling material and preparation method thereof

The invention discloses a coal gangue-based composite geopolymer grouting filling material and a preparation method thereof. The preparation method comprises a step of weighing raw materials in partsby mass. According to the method, coal gangue powder and slag powder are used as main raw materials; a KOH solid and a water glass solution form an alkali solution; slag powder with good activation performance and ground coal gangue powder with insufficient activation performance are subjected to alkali-excited activation by adopting an alkali excitation technology, active glass bodies in the slagpowder and active components such as SiO2 and Al2O3 in the coal gangue powder are leached out in a strong alkali environment to form a grouting material with a gelling effect, and compared with a cement material, the grouting material is lower in manufacturing cost and wide in material source; meanwhile, comprehensive and effective utilization of coal gangue is improved, stacking of a large amount of coal gangue is reduced, and good environmental protection and social benefits are achieved. Compared with a cement grouting material, the grouting material prepared by the invention is lower in bleeding rate and higher in stone rate, has a rapid hardening effect, can reduce water damage caused by permeation of water into a roadbed in a non-setting stage of slurry, and effectively reduces airshrinkage and crack extension after slurry hardening.
Owner:CHANGAN UNIV +1

Novel anti-shearing branch polymer oil displacement agent and synthetic method thereof

InactiveCN103320112AHigh apparent viscosityExhibits lower apparent viscosity under high shear conditionsDrilling compositionPolymer sciencePolymer solution
The invention discloses a novel anti-shearing branch polymer oil displacement agent and a synthetic method thereof. According to the technical scheme, the following raw materials and monomers in mass percent are used: 73.5-84.95% of acrylamide (AM), 15-25% of sodium acrylate NaAA and 0.05-1.5% of polyamidoamine modified branch skeleton GA taking 1,3-propane diamine as a core. The synthetic method of the novel anti-shearing branch polymer oil displacement agent comprises the following steps of: adding NaAA into a reactor, adding pure water, regulating pH to be 6.5-7.5 with NaOH, stirring and adding AM and GA, preparing a solution with the concentration of 15-30%, introducing nitrogen for 20 minutes, then adding an initiating agent, continuously introducing the nitrogen for 10-20 minutes, and reacting for 3-10 hours at 30-60 DEG C; and finally washing, smashing and drying, thus an AM/NaAA/GA ternary polymer is obtained. The novel anti-shearing branch polymer oil displacement agent shows good shearing dilutability, the problem of injection of medium and low permeation oil reservoirs can be better solved, under lower shearing action, viscosity of the polymer can be rapidly restored, good fluidity control ability and aqueous phase permeability reducing capacity are realized, capacity of a polymer solution for expanding swept volume is improved, and simulated crude oil recovery ratio can be effectively increased by about 12.3%.
Owner:SOUTHWEST PETROLEUM UNIV
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