Method for preparing MgAlON transparent ceramic bisque by gel casting and molding
A technology for gel injection molding and transparent ceramics, applied in ceramic molding machines, manufacturing tools, etc., can solve problems such as unreported research, and achieve the effect of uniform microstructure, smooth surface and good shape
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[0036] Example 1:
[0037] A method for preparing MgAlON transparent ceramic green body by gel injection molding, which includes the following steps:
[0038] 1) Premix preparation: Dissolve 3.81g methacrylamide (abbreviated as MAM) and 0.76g of N,N'-methylenebisacrylamide (abbreviated as MBAM) in 20ml of deionized water to obtain a MAM concentration of 16wt% Solution, add 42.8wt% ammonium polyacrylate aqueous solution (referred to as PAA-NH 4 ) 0.29g is a dispersant (the amount of dispersant added is 0.398wt% of the mass of the MgAlON powder to be formed, calculated as 0.4wt%), after stirring evenly, adjust the pH of the solution to 10 with concentrated ammonia water to obtain a premixed solution;
[0039] 2) Preparation of ceramic slurry: Add 72.8g of MgAlON powder to the premix prepared in step 1), add alumina balls according to the mass ratio of the balls to 1.5:1, put them in the mixing bottle, mix, and ball mill for 8 hours to obtain Ceramic slurry with a solid content of 48vo...
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[0043] Example 2:
[0044] A method for preparing MgAlON transparent ceramic green body by gel injection molding, which includes the following steps:
[0045] 1) Premix preparation: Dissolve 3.81g of MAM and 0.38g of MBAM in 20ml of deionized water to form a solution with a MAM concentration of 16wt%, and add 0.34g of 42.8wt% PAA-NH 4 As a dispersant, after stirring evenly, adjust the pH value of the solution to 10 with concentrated ammonia water to obtain a premixed liquid;
[0046] 2) Preparation of ceramic slurry: Add 74.6g of MgAlON powder to the premix prepared in step 1), add alumina balls according to the mass ratio of the balls to 1.5:1, put them in the mixing bottle, mix and ball mill for 6 hours to obtain Ceramic slurry with a solid content of 50vol%;
[0047] 3) Injection molding: Vacuum the ceramic slurry prepared in step 2) for 20 minutes to 0.8×10 4 Pa, add 0.37g of 10wt% APS aqueous solution as initiator, 0.37g of TMEDA as catalyst, continue to vacuum for 3min to 0.8×10...
Example Embodiment
[0050] Example 3:
[0051] A method for preparing MgAlON transparent ceramic green body by gel injection molding, which includes the following steps:
[0052] 1) Premix preparation: Dissolve 3.81g of MAM and 0.25g of MBAM in 20ml of deionized water to form a solution with a MAM concentration of 16wt%, and add 0.38g of 42.8wt% PAA-NH 4 As a dispersant, after stirring evenly, adjust the pH value of the solution to 10 with concentrated ammonia water to obtain a premixed liquid;
[0053] 2) Preparation of ceramic slurry: add 76.4g of MgAlON powder to the premix prepared in step 1), add alumina balls according to the mass ratio of the balls to 1.5:1, put them in the mixing bottle, mix, and ball mill for 4 hours to obtain Ceramic slurry with a solid content of 52vol%;
[0054] 3) Injection molding: Vacuum the ceramic slurry prepared in step 2) for 5min to 1.2×10 4 Pa, add 0.38g of 10wt% APS aqueous solution as initiator, 0.38g of TMEDA as catalyst, stir evenly and continue to vacuum for 3mi...
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