41 results about "Gel casting" patented technology

The invention discloses a preparation method of thermal shock resistant magnesium aluminate spinel transparent ceramic, and belongs to the technical field of ceramic materials. The preparation method comprises the following steps: (1) synthesizing crystalline MgAl2O4 nano powder by adopting an additive-free hydrothermal method; (2) depolymerizing the powder, performing water-based gel casting to prepare a green body, and performing staged debonding treatment on the green body; (3) carrying out two-step vacuum presintering on the green body; (4) carrying out hot isostatic pressing densification treatment in a subgrain growth temperature region of 1380-1420 DEG C; and (5) carrying out annealing treatment on the densified ceramic. High-purity crystalline powder is synthesized through an additive-free hydrothermal method, grain boundary impurities are eliminated, and the intermediate infrared transmittance is remarkably improved; by combining the synergistic effect of optimized two-step pre-sintering and hot isostatic pressing in a sub-grain region, precise refinement of the grain size is realized; and finally, the bending strength, the fracture toughness and the critical thermal shock temperature difference of the material are greatly improved under the strengthening mechanism of ultrafine grains and defect-free grain boundaries.

The invention relates to the technical field of silicon carbide ceramics, and discloses a high-precision silicon carbide vacuum chuck manufacturing method which comprises the following steps: uniformly mixing composite silicon carbide micro powder, a sintering aid, a dispersing agent, a cross-linking agent, acrylamide, hydroxyethyl methylacrylate and deionized water, and carrying out ball milling to obtain gel slurry; mixing the gel slurry with an initiator and a catalyst, injecting the mixture into a deep-hole mold, carrying out gel reaction, carrying out compression molding, finishing, taking out, putting into a sintering furnace, sintering, and cooling to room temperature, so as to obtain a suction cup prefabricated body; milling, polishing and cleaning the suction cup prefabricated body to obtain the silicon carbide vacuum suction cup; the compact and uniform silicon carbide ceramic suction cup is formed through the processes of gel casting, sintering, milling, polishing and cleaning, and the silicon carbide ceramic suction cup has high mechanical strength, heat-conducting property and specific stiffness.

This application relates to a preparation mold and method for gel casting of reaction-bonded silicon carbide barrels, belonging to the field of silicon carbide product technology. It includes an inner cylinder, an outer tube, and an outer cylinder. The outer tube is sleeved outside the inner cylinder. One end of the inner cylinder extends out of the outer tube and is connected to a first base plate. The outer tube abuts against the surface of the first base plate. A first molding cavity is formed between the inner wall of the outer tube and the outer wall of the inner cylinder. The first molding cavity is used for pouring paraffin wax and forming the inner barrel mold. The inner diameter of the outer cylinder is larger than the diameter of the inner barrel mold. A second base plate is provided on the inner wall of one end of the outer cylinder. After the inner barrel mold is inserted into the outer cylinder, it abuts against the second base plate. A second molding cavity is formed between the inner wall of the outer cylinder and the outer wall of the inner barrel mold. The second molding cavity is used for pouring gel-based sauce and forming the silicon carbide barrel blank. This application has the effect of improving the removal efficiency of the inner mold and the forming quality of the inner wall of the silicon carbide barrel blank in the gel casting process.

The invention relates to the technical field of grinding in material engineering, and discloses a high-porosity honeycomb pore ceramic bond grinding tool and a preparation method and application thereof.The preparation method of the mold comprises the following steps that S1, a solvent, a gelatinizing agent, a ceramic bond, a pore forming agent and a grinding material are pretreated to prepare sol slurry; s2, after gel treatment, the sol slurry forms a gel body, pore-forming agents in the gel body are mutually adsorbed through self-tightening treatment, gaps between the pore-forming agents are filled with a ceramic bonding agent and an abrasive material, and a grinding tool blank is obtained; and S3, the grinding tool blank is subjected to firing process treatment, and the target grinding tool is obtained. According to the preparation method disclosed by the invention, the pore-forming agent is used as a template, and the ceramic bond grinding tool prepared by a process method of stacking and self-assembling an in-situ gel casting mold through the pore-forming agent has the advantages of high porosity, high macro porosity, uniform pore size and uniform distribution, and has good mechanical properties and grinding properties such as cooling and chip containing.

The invention provides an aerogel production assembly that includes a mold with a mold base defined by a casting substrate, where the casting substrate includes a film. The invention also provides an aerogel production method that involves filling such a mold with a wet gel precursor solution. In other embodiments, the invention provides an aerogel production assembly that includes a film and a film handling system. In still other embodiments, the invention provides an aerogel production assembly that includes an advantageous aging clamp mechanism. Further, some embodiments of the invention provide an aerogel production method that involves a wet gel sheet casted to a casting substrate, where the casting substrate includes a film, and the method includes both peeling the film off the wet gel sheet and conveying the wet gel sheet onto a drying substrate.

This invention relates to the field of membrane materials technology, specifically to a biaxially stretched polyolefin film, its preparation process, and its applications. This invention solves the problem of uneven microstructure caused by non-uniform preheating and stretching of thick gel castings in existing technologies through a specific heat-setting process. It provides a gel film precursor with uniform three-dimensional properties (i.e., along the film production line's forward direction, width direction, and thickness direction) for subsequent stretching, thereby obtaining a microporous membrane with narrower pore size distribution and a more regular structure. It also solves the problem of the limiting stretching ratio restricted by the accumulation of stress within the connecting chains in existing stretching processes. By relaxing stress and widening the process safety window, it enables higher-ratio uniform biaxial stretching, thereby improving the final mechanical strength (such as tensile strength) and air permeability of the microporous membrane.

The utility model discloses an automatic agarose gel making instrument which comprises an instrument body, a heating base arranged at the bottom of one side of the instrument body, and a container tank placed on the heating base, and is characterized in that a tank cover is arranged at the top of the container tank, a motor is arranged at the upper end of the tank cover, a fixedly connected stirring rod is arranged at the lower end of the motor, and the stirring rod extends into the container tank; a plurality of stirring blades A and a plurality of stirring blades B are upwards arranged on the stirring rod from the bottom end, the stirring blades A and the stirring blades B are alternately arranged at intervals, and the structures of the stirring blades A and the stirring blades B form a vertical mirror image. The motor is arranged in a motor box at the top end of the tank cover. According to the automatic agarose gel making instrument, the stirring rod is provided with a plurality of groups of vertical mirror image stirring blades, so that the pushing directions of liquid flow are rich, a low-efficiency stirring area does not exist, and even if a container is large and the amount of a solution is large, the uniformity and sufficiency of stirring can be ensured.

The invention provides a method for preparing porous ceramic through gel casting of emulsion, and belongs to the technical field of porous ceramic materials, and the method comprises the following steps: adding a catalyst and an initiator into the emulsion, carrying out mechanical stirring and injection molding, and then putting the emulsion into a drying oven for heating and curing to obtain a porous ceramic biscuit; degreasing and sintering the obtained biscuit to obtain porous ceramic; the emulsion comprises ceramic powder and / or sol nanoparticles, an organic monomer, a cross-linking agent, a binder, a defoaming agent, deionized water, an oil phase and a surfactant. According to the invention, rapid curing molding of the emulsion is realized through a cross-linking polymerization reaction of the organic monomer and the cross-linking agent, the advantages of simple and convenient operation and adjustable pore structure of an emulsion template method are retained, and a novel efficient technical route is provided for rapid and controllable preparation of porous ceramics with a complex structure and high porosity.

The invention discloses a method for preparing a honeycomb porous wafer thinned grinding wheel based on an in-situ gel casting method, which comprises the following steps of: placing superfine diamond micro-powder in an acidic strong oxidizing solution, heating, centrifugally cleaning until the superfine diamond micro-powder is neutral, and drying to obtain pre-oxidized diamond micro-powder; adding the modified diamond micro-powder into a silane coupling agent solution for grafting reaction to obtain modified diamond micro-powder; the method comprises the following steps: dissolving an organic monomer and a cross-linking agent in deionized water according to a predetermined mass ratio, and stirring to obtain an organic monomer premixed solution; adding microcrystalline glass binder powder, a polymeric dispersant and modified diamond micro-powder into the organic monomer premixed liquid, and carrying out dispersion treatment to obtain high-solid-content ceramic slurry; adding a macroporous pore-forming agent into the ceramic slurry, stirring, fully discharging bubbles, adding an initiator and a catalyst, pouring into a forming mold, carrying out in-situ polymerization reaction on organic monomers to form a gel network, and further forming a wet blank; and the wet blank is dried, degummed and sintered to obtain the grinding wheel block with the honeycomb structure. And cutting the honeycomb-structure grinding wheel blocks, and pasting the honeycomb-structure grinding wheel blocks in the grooves of the grinding wheel base body in an array manner to form the honeycomb porous wafer thinning grinding wheel. The problem of agglomeration of the ultrafine diamond powder is solved, and the bending strength of the prepared grinding wheel can be improved while the high porosity is guaranteed.

The invention belongs to the technical field of inorganic non-metallic materials, and relates to a silicon carbide whisker toughened boron carbide composite material based on gel casting. The invention discloses a silicon carbide whisker toughened boron carbide composite material based on gel casting molding, the silicon carbide whisker toughened boron carbide composite material has a dumbbell-shaped B4C-SiCw-B4C structure, and the structure is characterized in that two ends of silicon carbide whiskers with the length-diameter ratio of more than 50: 1 are connected with boron carbide particles; the silicon carbide whisker toughened boron carbide composite material based on gel casting is prepared by the following steps: performing ball milling, gelatinization, carbonization treatment and siliconizing treatment on composite powder obtained by premixing silicon carbide whiskers and boron carbide of which the length-diameter ratio is greater than 50: 1 and a gel mixture. A small amount of silicon carbide whiskers with a high length-diameter ratio are introduced into boron carbide, so that the silicon carbide whiskers with the high length-diameter ratio in the obtained silicon carbide whisker toughened boron carbide composite material are promoted to be connected with B4C particles, a dumbbell-shaped B4C-SiCw-B4C structure is formed, crack propagation is effectively hindered, cracks are deflected or bridged, and effective toughening is achieved.

The invention provides a zirconia porcelain block based on gel casting, a preparation method and application. Comprising the following steps: injecting mixed slurry into a mold, adding an initiator and a catalyst in the injection process until the mixture is completely cured, demolding, and then carrying out drying and glue discharging treatment to obtain a glue-discharged green body; and carrying out mechanical processing on the degummed green body, and then carrying out rapid sintering to obtain the zirconium oxide porcelain block. Wherein the mixed slurry comprises a precursor solution and inorganic powder; the precursor solution comprises one or more of polyvinyl alcohol, chitosan and polyacrylic acid; the inorganic powder comprises the following components in parts by mass: 85-94 parts of zirconium oxide, 2-10 parts of yttrium oxide, 2-5 parts of hafnium oxide, 2-5 parts of aluminum oxide and 1-5 parts of other inorganic oxides. The preparation method disclosed by the invention is simple, convenient to operate, low in cost and easy for large-scale production and application.

The invention provides an aerogel production assembly that includes a mold with a mold base defined by a casting substrate, where the casting substrate includes a film. The invention also provides an aerogel production method that involves filling such a mold with a wet gel precursor solution. In other embodiments, the invention provides an aerogel production assembly that includes a film and a film handling system. In still other embodiments, the invention provides an aerogel production assembly that includes an advantageous aging clamp mechanism. Further, some embodiments of the invention provide an aerogel production method that involves a wet gel sheet casted to a casting substrate, where the casting substrate includes a film, and the method includes both peeling the film off the wet gel sheet and conveying the wet gel sheet onto a drying substrate.

The application discloses a ceramic slurry preparation equipment for gel casting, and relates to the technical field of preparation equipment.The ceramic slurry preparation equipment for gel casting comprises a vacuum stirring assembly, a temperature control assembly and a vacuum feeding assembly.The vacuum stirring assembly comprises a stirring barrel, a stirrer and a vacuum pump in communication with the stirring barrel.The stirrer is inserted into the stirring barrel to stir the slurry in the stirring barrel.The temperature control assembly comprises a cooling circulator in communication with the stirring barrel and a temperature sensor.The cooling circulator is used for cooling the slurry in the stirring barrel, and the temperature sensor is used for measuring the slurry temperature of the stirring barrel.The vacuum feeding assembly comprises a peristaltic pump and a sealed container in communication with the stirring barrel.The sealed container and the stirring barrel are respectively in communication with the peristaltic pump, and are used for precisely adding catalysts and initiators into the stirring barrel under the vacuum and isobaric environment.The application realizes the full automation of the preparation of the ceramic slurry for gel casting in the same equipment, and also reduces the generation of air bubbles in the preparation process of the ceramic slurry.

This invention provides a high-porosity ceramic-bonded diamond micropowder abrasive, its preparation method, and its application. The preparation method includes: preparing a ceramic-bonded diamond micropowder composite powder using a sol-gel method; preparing porous agglomerated diamond microspheres using an atomization granulation method with the ceramic-bonded diamond micropowder composite powder and an organic pore-forming agent as raw materials; preparing a calcium alginate aqueous solution using a multiple emulsion method and an atomization granulation method with sodium alginate and calcium salt as raw materials; and preparing a ceramic-bonded diamond micropowder abrasive using a gel casting method with the porous agglomerated diamond microspheres and calcium alginate aqueous spheres as the main raw materials. The above-mentioned diamond micropowder abrasive utilizes the organic pore-forming agent and sodium alginate aqueous spheres as pore-forming agents, allowing for precise control of the particle size and ratio of pores in the prepared diamond micropowder abrasive. It exhibits high porosity, good self-sharpening properties, and low grinding resistance, making it suitable for efficient and high-quality processing of semiconductor materials.

The invention relates to the field of sheet ceramic production, in particular to an energy-saving type water-based gel casting continuous forming device for sheet ceramics, one side of a roller frame is provided with an extruder, the other side of the roller frame is provided with a plurality of groups of rotatable winding drums through a support frame, one side far away from the winding drums is provided with a guide roller, and an execution roller is slidably mounted below the guide roller; and the strip-shaped film is sequentially wound on the guide roller, the execution roller and the winding drum. According to the film cutting device, the winding drum structure can excite the oil cylinder structure to stretch out the film inserting knife in the rotary material changing process, so that a film body is cut while being inserted into an empty roll, and the film body is compacted through the execution roller reset clockwise to guarantee the subsequent winding stability; and process defects and energy waste caused by traditional shutdown roll replacement can be avoided while non-shutdown roll replacement is realized.

This invention belongs to the field of ceramic refractory materials technology, specifically relating to a method for preparing an aluminosilicate fiber crucible with an anti-erosion coating, the crucible itself, and its applications. The method involves using aluminosilicate ceramic fibers, a solvent, organic monomers, and a crosslinking agent, followed by gel casting in a mold to form a three-dimensional skeleton structure of the aluminosilicate ceramic fibers. After drying and sintering, an aluminosilicate ceramic fiber crucible matrix is ​​obtained. A coating slurry is prepared using multi-stage Y₂O₃ powder and two grinding balls of different diameters. This slurry is then coated onto the inside of the aluminosilicate ceramic fiber crucible matrix. Finally, a multi-stage heating process is used for sintering to obtain an aluminosilicate fiber crucible with an anti-erosion coating. This invention improves the crucible's strength through gel casting and enhances its resistance to melt erosion by coating the inner wall of the crucible with a yttrium oxide coating, thus preventing interfacial reactions between the crucible and the melt.

A method includes forming a polymer solution having a crystallizable PVDF-family polymer and a liquid solvent, forming a gel from the polymer solution, forming a polymer thin film from the gel by calendering or solid state extrusion, stretching the polymer thin film, and applying an electric field to the polymer thin film to form a poled polymer thin film, where an electromechanical coupling factor (k31) of the poled polymer thin film is at least approximately 0.1. The polymer thin film may include up to approximately 90 wt. % of an additive and may be characterized by a bimodal molecular weight distribution of a crystallizable polymer where the molecular weight of the additive is less than the molecular weight of the crystallizable polymer. In some examples, the polymer(s) and the additive(s) may be independently selected from vinylidene fluoride, trifluoroethylene, chlorotrifluoroethylene, hexafluoropropene, vinyl fluoride, etc.

This invention relates to a catalytic material and its preparation method, addressing the problems of low design freedom in existing catalytic material preparation methods and competitive ultraviolet energy absorption between the catalyst and photosensitive resin during photopolymerization 3D printing. The preparation method of the catalytic material in this invention includes the following steps: S1, preparing a calcium oxide sacrificial mold using photopolymerization 3D printing; S2, preparing a catalyst-epoxy resin slurry; S3, gel casting: adding a curing agent to the catalyst-epoxy resin slurry, then injecting it into the calcium oxide sacrificial mold, and heating to cure to obtain a gelled wet preform; S4, demolding and drying the gelled wet preform to obtain a catalyst blank; S5, debinding and sintering the catalyst blank to obtain the catalytic material. This preparation method possesses high design freedom and realizes the preparation of catalytic materials with artificially designed ordered pore structures using catalyst slurries with high solid content.

This invention discloses a lens-type fluorescent composite ceramic for laser illumination and its preparation method, comprising a YAG ceramic lens and a fluorescent ceramic block disposed at the central focal point inside the YAG ceramic lens. The chemical formula of the fluorescent ceramic block is (Re). 1‑x Ce x )3Al5O 12 In the formula, Re represents one or more elements from Y, Lu, Ga, Gd, and Tb, where 0.0001 ≤ x ≤ 0.005. Preparation method: Fluorescent ceramic blocks are prepared using a dry pressing method; a gel casting slurry is prepared using YAG ceramic lens powder as raw material. The fluorescent ceramic block is then coated onto the central focal point of the YAG ceramic lens using a double gel casting process. The fluorescent composite ceramic is obtained through drying, debinding, sintering, annealing, and polishing. This method effectively improves luminous efficiency and heat dissipation capacity while flexibly controlling the light divergence angle. The prepared fluorescent composite ceramic achieves high lumen efficiency and high brightness luminous performance, making it suitable for long-term stable lighting in various fields.

The utility model discloses a die for gel casting, which comprises a lower base, and a lower die is clamped at the top of the lower base. The handle at the bottom is pushed backwards, the handle at the bottom drives the bottom clamping plate to move outwards, the bottom clamping plate relieves limiting and clamping of the lower die, the bottom clamping plate extrudes the spring towards the outer side at the corresponding position, the lower die is pulled out upwards, and the lower clamping strip is driven to move upwards while the lower die moves. The lower clamping strip is extruded by the lower base to move into the mounting groove, the lower clamping strip extrudes the second spring, the lower clamping strip relieves clamping of the lower base, the lower die can be pulled out, the upper die can be disassembled in the same mode, when mounting is needed, the steps are operated reversely, and the beneficial effect of efficient disassembly and assembly is achieved; and a tool is not needed to disassemble and assemble the bolt during disassembly and assembly, so that the disassembly and assembly process consumes less time, and the usability of the mold is improved.

The invention discloses a silicon carbide part preparation method based on gel casting, which comprises the following steps: mixing and ball-milling silicon carbide powder, carbon black, phenolic resin, a solvent, a dispersing agent and an acrylic acid cross-linking agent to obtain first slurry; a curing agent is added into the first slurry, ball milling and defoaming are continued, and second slurry is obtained; pouring the second slurry into a polypropylene mold, curing, and demolding to obtain a wet blank; and drying and sintering the wet blank to obtain the silicon carbide part. The method has high uniformity, low defect control and complex shape manufacturing capability, can be used for preparing large-size silicon carbide devices, and is suitable for industrial large-scale production. Phenolic resin and an acrylic acid cross-linking agent are adopted as binders, gradient curing can be carried out to prevent particle sedimentation and generate a uniform green body, phenolic resin is pyrolyzed to generate nanocarbon, pores can be filled, silicon point formation can be inhibited, nano silicon carbide can be generated in situ, and the density and the mechanical property of a sintered body are remarkably improved.

The invention provides an aerogel production assembly that includes a mold with a mold base defined by a casting substrate, where the casting substrate includes a film. The invention also provides an aerogel production method that involves filling such a mold with a wet gel precursor solution. In other embodiments, the invention provides an aerogel production assembly that includes a film and a film handling system. In still other embodiments, the invention provides an aerogel production assembly that includes an advantageous aging clamp mechanism. Further, some embodiments of the invention provide an aerogel production method that involves a wet gel sheet casted to a casting substrate, where the casting substrate includes a film, and the method includes both peeling the film off the wet gel sheet and conveying the wet gel sheet onto a drying substrate.

The invention discloses a porous nano ceramic reinforcement, a lightweight nano composite ceramic insulator and preparation thereof, silicon nitride is used as a matrix, a negative thermal expansion functional phase Zn (2-x) CuxP2O7 is compounded, and a three-level pore structure with macroscopic pores, microcosmic pores and nano pores is constructed through a multi-level pore forming agent and silane coupling agent interface modification technology. The reinforcement is prepared through an optimized gel casting and gradient sintering process, high strength under high porosity is achieved, and the overall material has the near-zero thermal expansion characteristic through the negative thermal expansion effect. The problems of size instability and internal thermal stress caused by dramatic temperature change are solved, and a foundation is laid for long-term reliable operation of the insulator in extreme climate.

A composite phosphor ceramic optical fiber with luminous efficiency and color rendering index includes a phosphor ceramic fiber core and a phosphor ceramic cladding, the phosphor ceramic fiber core uses a yellow phosphor ceramic doped with Ce ions, and the phosphor ceramic cladding uses a red phosphor ceramic co-doped with ions. The composite phosphor ceramic fiber is prepared by the gel casting. With this design structure, not only can the energy transfer between Ce ions and other ions cause a red shift in the spectrum to improve the color rendering index, but also the luminous efficiency can be significantly enhanced. In addition, a diameter of the composite phosphor ceramic optical fiber matches a laser spot size very well, effectively solving the “yellow ring effect” problem caused by the mismatch. It can effectively solve the heat dissipation problem during high power LD pumping and is conducive to long term stable lighting.

This invention discloses a method for preparing yttrium oxide ceramics by gel casting. The method first prepares modified yttrium oxide powder, then adds calcium carbonate for mixing, and finally uses Isobam gelling agent for green gel casting, followed by sintering to obtain yttrium oxide ceramics. Through powder pretreatment, an aqueous suspension containing yttrium oxide and calcium oxide is obtained, solving the dual problems of challenging sintering characteristics and thermal shock susceptibility of yttrium oxide. The preparation process of this invention is simple, the gel system used is non-toxic and harmless, environmentally friendly, and has high production efficiency. The prepared ceramics possess advantages such as high strength, good toughness, and good wear resistance.

The invention provides an aerogel production assembly that includes a mold with a mold base defined by a casting substrate, where the casting substrate includes a film. The invention also provides an aerogel production method that involves filling such a mold with a wet gel precursor solution. In other embodiments, the invention provides an aerogel production assembly that includes a film and a film handling system. In still other embodiments, the invention provides an aerogel production assembly that includes an advantageous aging clamp mechanism. Further, some embodiments of the invention provide an aerogel production method that involves a wet gel sheet casted to a casting substrate, where the casting substrate includes a film, and the method includes both peeling the film off the wet gel sheet and conveying the wet gel sheet onto a drying substrate.

The invention discloses mullite fiber porous ceramic as well as a preparation method and application thereof, and belongs to the technical field of ceramic fiber filters. The preparation method comprises the following steps: uniformly mixing an aluminum source compound and silica powder to obtain mixed powder; the aluminum source compound is a mixture of rho-Al2O3 and any one of gamma-Al2O3 and Al (OH) 3; wherein the amount of substance of aluminum in rho-Al2O3 accounts for 25%-75% of the amount of substance of aluminum in the aluminum source compound; uniformly mixing a hydroxypropyl methyl cellulose aqueous solution, the mixed powder and mullite fibers to obtain slurry; carrying out molding treatment on the slurry by adopting a gel-casting method to obtain a sample; the method comprises the following steps: carrying out heat preservation treatment on a sample in an air atmosphere at a first temperature to grow crystal grains, and heating to a second temperature to promote the development of a mullite crystal phase to obtain the mullite porous ceramic. The mullite fiber porous ceramic has excellent filtering efficiency.

The invention discloses a microwave dielectric filter based on an agarose-epoxy resin composite system and a preparation method of the microwave dielectric filter. Deionized water, a dispersing agent, a pH regulator and a surface modifier are taken to be prepared into a premixed liquid material, the premixed liquid material is subjected to ball milling to obtain premixed liquid, and microwave dielectric ceramic powder is added into the premixed liquid in batches to obtain slurry; carrying out ball milling on the slurry to obtain microwave dielectric ceramic slurry; deionized water, agarose powder and epoxy resin are taken to be prepared into gel, and the gel is heated, dissolved and mixed to obtain agarose-epoxy resin composite gel; mixing the microwave dielectric ceramic slurry with the agarose-epoxy resin composite gel, heating and stirring to obtain microwave dielectric ceramic slurry for gel casting, performing vacuum defoaming, injecting the microwave dielectric ceramic slurry into a microwave dielectric ceramic filter mold, putting the microwave dielectric ceramic filter mold into a constant-temperature and constant-humidity box, cooling, drying and demolding to obtain a biscuit, and performing degumming and sintering in a sintering furnace to obtain the microwave dielectric ceramic filter. The microwave dielectric filter based on the agarose-epoxy resin composite system is obtained by polishing and grinding, and the whole-process green manufacturing is realized by combining the biocompatibility of the agarose and the epoxy resin.

The invention discloses ceramic slurry preparation equipment for gel casting, and relates to the technical field of preparation equipment.The ceramic slurry preparation equipment for gel casting comprises a vacuum stirring assembly, a temperature control assembly and a vacuum feeding assembly.The vacuum stirring assembly comprises a stirring barrel, a stirrer and a vacuum pump communicating with the stirring barrel; the stirrer extends into the stirring barrel to stir slurry in the stirring barrel; the temperature control assembly comprises a cooling circulator communicated with the stirring barrel and a temperature sensor, the cooling circulator is used for cooling slurry in the stirring barrel, and the temperature sensor is used for measuring the temperature of the slurry in the stirring barrel; the vacuum feeding assembly comprises a peristaltic pump and a closed container communicated with the stirring barrel, the closed container and the stirring barrel are communicated with the peristaltic pump, and the vacuum feeding assembly is used for accurately adding a catalyst and an initiator into the stirring barrel in a vacuum isobaric environment. According to the invention, full automation of preparation of the ceramic slurry for gel casting is realized in the same equipment, and bubbles generated in the preparation process of the ceramic slurry are reduced.

The application discloses preparation of a composite metal heterojunction modification material and application of the composite metal heterojunction modification material in a lithium battery. 12 The application first synthesizes Bi4Ti3O 12 -NiCo2S4 heterojunction nanosheet-shaped composite metal sulfide heterojunction material by using a non-aqueous sol-gel casting method, and then uniformly coats the material on one side of a battery diaphragm in a slurry to obtain the composite metal heterojunction modification material. The heterojunction nanosheet structure in the composite metal heterojunction modification material can provide a channel for rapid diffusion of lithium ions, improve interface polarity, increase surface catalytic active sites, optimize affinity to polysulfides, and promote catalytic conversion, so that the rate performance and cycle stability performance of the lithium-sulfur battery are effectively improved.