Preparation method and application of perylene diimide and graphene composite material
A technology of perylene diimide and composite materials, which is applied in the field of preparation of perylene diimide and graphene composite materials, and can solve problems such as low capacity, easy dissolution, and limited applications
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[0022] The following examples of the present invention are described in detail below. The following examples are implemented on the premise of the technical solution of the present invention, and detailed implementation methods and specific operating procedures are provided, but the protection scope of the present invention is not limited to the following the embodiment.
[0023] In a preferred embodiment of the present invention, the preparation method of the perylene diimide and graphene composite material G-P-300 includes the following steps.
[0024] 1. Synthesis and preparation of PDI
[0025] (1) 25 mmol of perylenetetracarboxylic dianhydride and 240 mmol of N,N-dimethyl-1,2-ethylenediamine were dissolved in 100 mL of DMF, and then reacted at 130° C. for 5 hours under nitrogen protection. After the reaction is completed, cool to room temperature, then add 500mL THF to form a suspension, filter under reduced pressure and wash with THF to remove excess N,N-dimethyl-1,2-et...
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