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Detection method for Curcuma zedoaria in Fuping capsule, and Fuping capsule detection method

A detection method, the technology of Fuping Capsules, which is applied in the detection field of traditional Chinese medicine, can solve the problem that quercetin cannot control the quality of medicines, etc.

Inactive Publication Date: 2017-08-18
GUIZHOU JINGCHENG PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, with the continuous improvement of the society's requirements for drug safety, drugs need to increase the establishment of specific content determination to control the quality of drugs. control

Method used

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  • Detection method for Curcuma zedoaria in Fuping capsule, and Fuping capsule detection method
  • Detection method for Curcuma zedoaria in Fuping capsule, and Fuping capsule detection method
  • Detection method for Curcuma zedoaria in Fuping capsule, and Fuping capsule detection method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Fuping Capsules are prepared into 1000 capsules from 300g of golden buckwheat, 300g of Viola chinensis, 150g of zedoary, 300g of Patrinia, 300g of Scutellaria chinensis, 300g of Rhododendron 300g, and 300g of goldenrod.

[0020] The original quality standard of Fuping Capsules (see National Standards [Surgical Gynecology Fascicle] WS-10003(ZD-2003)-2002) is determined by HPLC method to determine the content of quercetin in the sample, but after testing each flavor in the prescription According to the research on medicinal materials, all of them contain quercetin except for S. sagittarius, so the specificity of quercetin content control in the product is not strong. According to the requirements of the National Pharmacopoeia Commission, it is necessary to increase the establishment of a specific content determination. After analyzing the prescription, this Curcuma is used as the monarch drug in the prescription, so it is planned to study the content of Curcuma in the medi...

Embodiment 2

[0110] The detection method of Fuping Capsules includes the quality standard of Fuping Capsules in the National Standard Part [Surgical Gynecology Volume] WS-10003 (ZD-2003)-2002 and the content determination of Zedoary Curcuma in Example 1.

Embodiment 3

[0112] The detection method of Fuping capsules includes the detection method disclosed in Chinese patent 201410205683.4, Fuping capsule quality standard detection method and the content determination of curcuma in Example 1.

[0113] In Examples 2 and 3, the content determination of Curcuma was added to the Fuping Capsules quality standard of the prior art, because only Curcuma contains Gemaconone in the whole Fuping Capsule formula, so the content determination method has specificity and can Better control of drug quality.

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Abstract

The invention discloses a detection method for curcuma zedoaria in Fuping capsule. The detection method is characterized in that the curcuma zedoaria content is determined through gradient elution by using high performance liquid chromatography, wherein only the curcuma zedoaria in the Fuping capsule contains germacrone, such that the curcuma zedoaria content determination is exclusive. According to the present invention, the curcuma zedoaria content determination is performed in the Fuping capsule detection so as to effectively control the quality of the Fuping capsule.

Description

technical field [0001] The invention relates to a detection method of traditional Chinese medicine, in particular to a detection method of curcuma content in Fuping capsules and a detection method of Fuping capsules including the content detection method. Background technique [0002] Fuping capsule is a Chinese patent medicine for clearing heat, detoxifying, removing blood stasis and reducing swelling. It is used to treat pelvic inflammatory disease, adnexitis and other diseases. Rattan, Solidago, the current quality standard (National Standard Part [Surgical Gynecology Volume] WS-10003 (ZD-2003)-2002) with quercetin (C 15 h 10 o 7 ) content to reflect the inherent quality of the product. However, through research on the various medicinal materials in the prescription, all of them contain quercetin except for Saccharomyces chinensis, so the quality of the product cannot be controlled stably, and the safety and effectiveness of the product cannot be guaranteed. In order ...

Claims

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Application Information

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IPC IPC(8): G01N30/02
CPCG01N30/02G01N2030/027
Inventor 简卫光
Owner GUIZHOU JINGCHENG PHARMA
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