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Rapid tobacco root cadmium content detection method based on laser induced breakdown spectroscopy technology

A laser-induced breakdown and detection method technology, which is applied in the direction of material excitation analysis, can solve the problems of LIBS signal influence and different detection parameters, and achieve the effects of improving applicability and stability, convenient system adjustment, and simple operation

Inactive Publication Date: 2018-05-18
ZHEJIANG FORESTRY UNIVERSITY
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Problems solved by technology

However, because the LIBS signal is easily affected by the matrix, and the detection parameters required for different objects are different, in order to ensure the stability of the collected signal and improve the detection accuracy, it is necessary to optimize the instrument parameters of the collected signal

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  • Rapid tobacco root cadmium content detection method based on laser induced breakdown spectroscopy technology
  • Rapid tobacco root cadmium content detection method based on laser induced breakdown spectroscopy technology

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Embodiment Construction

[0043] The method for rapid detection of cadmium content in tobacco roots based on the laser-induced breakdown spectroscopy technology of the present invention will be further described in detail below in conjunction with the examples and accompanying drawings.

[0044] A method for rapid detection of cadmium content in tobacco roots based on laser-induced breakdown spectroscopy, the specific steps are as follows:

[0045] (1) Prepare samples to be tested: divide 80 tobacco plants into 4 groups on average, set up 3 experimental groups and 1 control group, and use CdCl with concentrations of 40, 70, and 100 μmol / L respectively in the experimental groups 2 For solution stress, the control group was added with the same amount of water; after one month of treatment, the roots of each tobacco plant were harvested.

[0046] Clean the fresh tobacco roots with disodium EDTA solution and distilled water, then dry and grind them. The drying temperature is 70 degrees Celsius, and the bakin...

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Abstract

The invention discloses a rapid tobacco root cadmium content detection method based on a laser induced breakdown spectroscopy technology. According to the method, the parameters of an instrument for collecting LIBS spectral data are optimized, the specific tobacco root sample spectral line emitted by plasma after high-energy laser ablation is collected by using the optimized target parameters, thesignal at the cadmium element characteristic wavelength of 361.05 nm is selected as an input value, the cadmium content in the sample is used as an output value, the regression model of the signal atthe characteristic wavelength and the cadmium content is established by using a unary linear regression method, the determination coefficient R2 of the established model is 0.96, prediction set datais input into the regression model, the cadmium contents of the prediction set samples are detected, and the prediction determination coefficient R2 is 0.92. According to the present invention, the cadmium element in the tobacco root can be rapidly detected, the method has characteristics of simple operation, low cost and the like, and by optimizing the parameters, the detection accuracy, the stability and the applicability of the method are improved.

Description

technical field [0001] The invention relates to tobacco heavy metal element detection technology, in particular to a rapid detection method for cadmium content in tobacco roots based on laser-induced breakdown spectroscopy technology. Background technique [0002] During mining, smelting, and processing, heavy metals enter the atmosphere, water, and soil to cause environmental pollution, and then enter plants. Therefore, detection of plant heavy metal content has become an important method to judge the degree of environmental heavy metal pollution. At present, the detection methods of heavy metal elements in plants mainly include high performance liquid chromatography, spectrophotometry, atomic spectroscopy, inductively coupled plasma mass spectrometry and so on. However, these methods are complex in operation and high in cost, and cannot meet the requirements of quickly obtaining the content of heavy metals in plants. [0003] With the increasing global anti-smoking campa...

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Application Information

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IPC IPC(8): G01N21/63
CPCG01N21/63
Inventor 孔汶汶刘飞宋坤林刘小丹申婷婷彭继宇
Owner ZHEJIANG FORESTRY UNIVERSITY
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