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Preparation method of ammonia sugar using shrimp and crab shells as raw material

A technology of shrimp and crab shells and ammonia sugar, which is applied in the field of ammonia sugar preparation using shrimp and crab shells as raw materials, can solve the problems of lower ammonia sugar yield and low degree of hydrolysis, achieve enhanced hydrolysis rate, reduce production cost, shorten enzyme Effect of time to remove protein

Active Publication Date: 2021-06-04
YANGZHOU RIXING BIO TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Studies have found that ammonia sugar can be obtained by hydrolyzing chitin in hydrochloric acid; in the prior art, there is a process for preparing ammonia sugar from chitin, but due to the inherent chemical properties of chitin itself, the degree of hydrolysis of chitin in hydrochloric acid is not high , thereby greatly reducing the yield of ammonia sugar prepared from chitin

Method used

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  • Preparation method of ammonia sugar using shrimp and crab shells as raw material

Examples

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Effect test

Embodiment 1

[0041] A method for preparing ammonia sugar using shrimp and crab shells as a raw material, comprising the steps of:

[0042] S1 extracts chitin from shrimp and crab shells;

[0043] S1-1 Carrying out high pressure pulverization and ultrasonic pulverization sequentially on the washed shrimp and crab shells to obtain pulverized shrimp and crab shells;

[0044] The high-pressure pulverization includes: pulverizing the cleaned shrimp and crab shells in a high-pressure pulverizer at 1.6 MPa for 1 min;

[0045] The ultrasonic crushing includes: ultrasonically crushing the shrimp and crab shells crushed under high pressure in distilled water for 5 minutes under a 350W ultrasonic wave;

[0046] S1-2 Under ultrasonic waves, the crushed shrimp and crab shells are sequentially subjected to acid hydrolysis to remove inorganic salts and enzymatic hydrolysis to remove proteins to obtain degradation products;

[0047] The acid hydrolysis includes: soaking the crushed shrimp and crab shell...

Embodiment 2

[0062] A method for preparing ammonia sugar using shrimp and crab shells as a raw material, comprising the steps of:

[0063] S1 extracts chitin from shrimp and crab shells;

[0064] S1-1 Perform high-pressure crushing and ultrasonic crushing on the washed shrimp and crab shells in sequence to obtain crushed shrimp and crab shells;

[0065] The high-pressure pulverization includes: pulverizing the cleaned shrimp and crab shells in a high-pressure pulverizer at 2 MPa for 5 minutes;

[0066] The ultrasonic crushing includes: ultrasonically crushing the shrimp and crab shells crushed under high pressure in distilled water for 8 minutes under a 400W ultrasonic wave;

[0067] S1-2 Under ultrasonic waves, the crushed shrimp and crab shells are sequentially subjected to acid hydrolysis to remove inorganic salts and enzymatic hydrolysis to remove proteins to obtain degradation products;

[0068] The acid hydrolysis includes: soaking the pulverized shrimp and crab shells in a citric ...

Embodiment 3

[0083] A method for preparing ammonia sugar using shrimp and crab shells as a raw material, comprising the steps of:

[0084] S1 extracts chitin from shrimp and crab shells;

[0085] S1-1 Perform high-pressure crushing and ultrasonic crushing on the washed shrimp and crab shells in sequence to obtain crushed shrimp and crab shells;

[0086] The high-pressure pulverization includes: pulverizing the cleaned shrimp and crab shells in a high-pressure pulverizer at 1.8 MPa for 3 minutes;

[0087] The ultrasonic crushing includes: ultrasonically crushing the shrimp and crab shells crushed under high pressure in distilled water for 6 minutes under a 380W ultrasonic wave;

[0088] S1-2 Under ultrasonic waves, the crushed shrimp and crab shells are sequentially subjected to acid hydrolysis to remove inorganic salts and enzymatic hydrolysis to remove proteins to obtain degradation products;

[0089] The acid hydrolysis includes: soaking the pulverized shrimp and crab shells in a citri...

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Abstract

The invention provides a method for preparing ammonia sugar using shrimp and crab shells as raw materials: it comprises the following steps: extracting chitin from shrimp and crab shells; modifying the chitin with a hydroxypropylation reagent, and then undergoing secondary hydrolysis to obtain Chitin secondary hydrolyzate; the chitin secondary hydrolyzate is sequentially concentrated, suction filtered and dried to obtain glucosamine. The preparation method of ammonia sugar using shrimp and crab shells as raw material of the present invention extracts chitin from shrimp and crab shells, and performs secondary hydrolysis after modifying the chitin with a hydroxypropylation reagent, which increases the concentration of chitin. Water solubility, thereby enhancing the hydrolysis rate of macromolecular polysaccharides in chitin into ammonia sugar, and then improving the yield of final product ammonia sugar in the process of preparing ammonia sugar from shrimp and crab shells.

Description

technical field [0001] The invention relates to the technical field of ammonia sugar preparation, in particular to a method for preparing ammonia sugar using shrimp and crab shells as raw materials. Background technique [0002] Glucosamine, the full name is D-glucosamine, referred to as glucosamine, is an important precursor for human body to synthesize articular cartilage tissue. The bones and joints of the human body are covered with a layer of cartilage at the joints, which is a protective pad for the joints and plays a role in cushioning and protecting the joints. If the cartilage degenerates and wears away, and loses its protective effect on the bones, it will lead to hyperosteogeny and osteoarthritis. Glucosamine is the core substance of articular cartilage, and is regarded by the medical community as the only substance that can fundamentally prevent and treat bone and joint diseases: the specific manifestations are as follows: [0003] Supplement bone nutrition, st...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/08C13K1/00A23L33/125
CPCA23V2002/00A23L33/125C08B37/0003C08B37/003C13K1/00A23V2200/30A23V2200/306A23J1/04A23J3/32A23J3/341A23L33/10A23L33/18
Inventor 平立凤丁振中曾哲灵冯小海李恒龚劲松高小燕徐俊山
Owner YANGZHOU RIXING BIO TECH