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Synthesis process of tridemorph

A synthesis process, the technology of tridecamorpholine, applied in the direction of organic chemistry, etc., can solve the problems of inability to meet market demand, low process yield, long process flow, etc., and achieve raw material cost advantages, high process yield, and short process flow. Effect

Pending Publication Date: 2020-01-21
HEFEI YIFAN PHARMA MANAGEMENT
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  • Abstract
  • Description
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  • Application Information

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Problems solved by technology

The raw materials of this synthesis method are not easy to obtain, and the process is long and the process yield is low, which cannot meet the current market demand

Method used

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  • Synthesis process of tridemorph
  • Synthesis process of tridemorph
  • Synthesis process of tridemorph

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Embodiment Construction

[0025] The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some, not all, embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without creative efforts fall within the protection scope of the present invention.

[0026] Such as figure 1 A kind of synthetic technique of tridemorpholine shown, described synthetic technique comprises the following steps:

[0027] Step 1: adding 80-90 parts by weight of tridecyl alcohol and 3 parts by weight of catalyst into the reaction kettle, and then replacing the air with nitrogen and hydrogen respectively;

[0028] Step 2: heating the reactor to 180-200°C, and reducing the catalyst for 30 minutes;

[0029] Step 3: Then heat up to 200-28...

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Abstract

The invention discloses a synthesis process of tridemorph, which comprises the following steps: adding tridecanol and a catalyst into a reactor together, and carrying out air replacement with nitrogenand hydrogen respectively; heating the reaction kettle to 180-200 DEG C, and reducing the catalyst for 30 minutes; heating the raw materials to 200-280 DEG C and dropwise adding 2,6-dimethylmorpholine; then continuously controlling the temperature to be 200 to 280 DEG C until the reaction endpoint is reached; standing and settling the material obtained by the reaction for 8 hours, and separatingthe catalyst; and rectifying the separated filtrate to obtain the finished product tridemorph. According to the invention, tridecanol is adopted as a main raw material, and the raw material cost has great advantages; the preparation method is simple, the technological process is short, the tridecanol and 2,6-dimethylmorpholine are adopted for one-step reaction under the action of a catalyst, the equipment investment is small, and operation is easy and convenient; in addition, the method is high in process yield and less in pollution, and a small amount of generated high waste can be used as fuel.

Description

technical field [0001] The invention belongs to the field of chemical synthesis, in particular to a synthesis process of tridemorpholine. Background technique [0002] Tridemorpholine (N-isotridecyl 2,6-dimethylmorpholine), as a good systemic fungicide, has both eradication and protection effects, can be absorbed through leaves and roots, and is produced by ten The preparation made of trimorpholine can be used to prevent and control powdery mildew of cereal crops, coccicum solmonicolor on banana trees, caticum solmonicolor on tea trees, especially Hevea spores and Exibasidium destructor on rubber trees, and has a wide range of uses . At present, tridemorpholine products and preparations in the world are mainly produced by BASF Company, and its production scale is relatively large. It has passed the pilot test identification in Liaoning Chemical Industry Research Institute in China. The synthesis method is as follows: using tridecyl alcohol and halogenating agent as raw mate...

Claims

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Application Information

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IPC IPC(8): C07D265/30
CPCC07D265/30
Inventor 黄勇钱莉苹吴世刚韩爱华唐英武王其龙
Owner HEFEI YIFAN PHARMA MANAGEMENT
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