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Water-soluble dropping pill prepared from porous material and preparation method thereof

A porous material, water-soluble technology, applied in the directions of essential oils/spices, fat generation, tobacco, etc., can solve the problems of cigarettes, slowness, and the amount of aroma release cannot be maintained, and achieves good appearance roundness and stable particle size. , the effect of uniform size

Pending Publication Date: 2021-07-09
WUHAN HUANGHELOU FLAVOR & SPICES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The water-soluble dripping pills disclosed in the prior art all use cross-linked and solidified sodium alginate as the coating layer, and the coating layer is directly coated with an aqueous solution containing water-soluble essence. In the future, the water-soluble solution containing essence coated inside will overflow quickly. With the overflow of the aqueous solution, the essence components will be released quickly, so that the early stage of the dropping pill is pinched, and the cigarette aroma is very rich; In the later stage of cigarette breaking, due to the continuous and rapid release of flavor components, the aroma of cigarettes gradually becomes thinner, and the amount of aroma release cannot be maintained in a relatively stable state, which cannot meet consumers' requirements for stable, slow, and long-term steady release of cigarette aroma during cigarette smoking. need

Method used

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Examples

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preparation example Construction

[0035] Embodiments of the present invention also provide a method of preparing water-soluble droplets, including the following steps:

[0036] (1) Paste the porous material to the water-soluble flavor solution for primary impregnation, preferably, once the immersion time is 0.5 to 2 h. After impregnation, the porous material loaded with water-soluble flavor is obtained, and the porous material after impregnation is used as an inner layer material; the water soluble flavor using different flavors can be selected according to the need for cigarette taste.

[0037] (2) Introducing the inner layer material into a calcium salt solution for sub-impregnation, obtaining a secondary impregnation material having a calcium salt surface is obtained; in the preferred embodiment of the invention, the calcium salt is calcium chloride or calcium lactate. The mass concentration of the calcium salt is 1 to 3%.

[0038] (3) The secondary impregnation material is first put into the alginate solution ...

Embodiment 1

[0043] The first embodiment of the present invention provides a water-soluble droplet pill prepared by a porous material, and the specific preparation process is as follows:

[0044] (1) Making the porous volcanic stone into spherical particles having a particle diameter of 2 to 2.5 mm, and put the spherical porous volcanic stone into the water-soluble flavor solution for one impregnation, at a time of 0.5 h, and remove it after impregnation The surface waterless drip state is placed under room temperature. After impregnation, the porous material loaded with water-soluble flavor is obtained, and the impregnated porous material is used as an inner layer material;

[0045] (2) The inner layer material is inserted into a calcium chloride solution in a concentration of 1%, and the secondary impregnation time is 5 min, and a secondary impregnation material having calcium chloride is adsorbed by the surface;

[0046] (3) The secondary impregnation material is first invested in a concent...

Embodiment 2

[0049] The present invention provides a water-soluble dripping pill prepared by a porous material, and the specific preparation process is as follows:

[0050] (1) Using the crusher to grind the porous volcanic stone into spherical particles having a particle diameter of 3 to 3.5 mm, put the spherical porous volcanic stone into the water-soluble flavor solution for once impregnation, once the impregnation time is 1 h, and remove it after impregnation, Place anhydrous dripping under the surface temperature conditions. After impregnation, the porous material loaded with water-soluble flavor is obtained, and the impregnated porous material is used as an inner layer material;

[0051] (2) The inner layer material is put into a calcium chloride solution having a concentration of 2% to the secondary impregnation, the secondary immersion time is 3 min, resulting in a secondary impregnation material having a calcium chloride in the surface;

[0052] (3) The secondary impregnation material...

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Abstract

The invention discloses a water-soluble dropping pill prepared from a porous material and a preparation method thereof. According to the water-soluble dropping pill prepared from the porous material, the water-soluble dropping pill comprises an inner layer, a middle layer and an outer layer; the inner layer is formed by loading water-soluble essence on the porous material, the middle layer is a gel layer formed by cross-linking reaction of sodium alginate and calcium salt, and the outer layer is a latex water locking layer formed by curing emulsion. According to the water-soluble dropping pill prepared from the porous material, the inner layer is formed by loading the water-soluble essence on the porous material, and compared with a traditional dropping pill with the inner layer only formed by the water-soluble essence, after the dropping pill is pinched broken, the water-soluble essence cannot directly and rapidly overflow out, the essence component is slowly released under the adsorption effect of the porous material so that the aroma release amount can be maintained in the stable state during the whole cigarette smoking process, and the requirements of consumers on the stable, slow and long-time stable release of the cigarette aroma during the cigarette smoking process can be met.

Description

Technical field [0001] The present invention relates to the field of smoke drops pills, in particular, the present invention relates to a water soluble droplet pill prepared by a porous material and a method of preparation. Background technique [0002] Adding moistening drops in the cigarette filter has become a common means of promoting cigarettes. The traditional moisturizing dripping pill is more oil-soluble, that is, the oil-soluble flavor fragrance is the inner material, supplemented The oily solvent such as olive oil, glycerol ester, and the dilution solvent of flavor. As disclosed in China Patent CN201810269876.4 discloses a preparation method of flavor, smoke dripping and dripping pills containing coffee molecules. The coffee flavor contains 5 ~ 12 parts of the coffee extract; 1 to 5 sergents; 1 to 15 softeners; The solvent is a mixture of edible tonnel and glycerylate. Chinese patent CN201810269647.2 discloses a flavor, cigarette dripping pill and dripping pills with Sh...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24D3/04
CPCC11B9/00A24D3/048
Inventor 苗丽坤陈胜孙炜炜刘吟
Owner WUHAN HUANGHELOU FLAVOR & SPICES
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