Multiple molecule contacting catalytic reaction apparatus and method
A contact catalysis and reaction device technology, applied in the field of multi-molecular contact catalysis reaction devices, can solve problems such as poisoning, catalyst poisoning, and reaction activity decline, and achieve the effect of improving reaction efficiency
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Embodiment 1
[0019] Referring to Fig. 1, described polymolecular contact catalytic reaction device comprises cylindrical reaction vessel 1, material conduit 2 and catalyst bed 3, and material conduit 2 is arranged in the reaction vessel along the vertical direction from the upper end of reaction vessel 1, and material conduit 2 The bottom is fixed on the catalyst bed 3, and the catalyst bed 3 is located in the middle of the reaction vessel. At least two openings 4 are provided on the conduit wall at one end of the catalyst bed, and the openings 4 are distributed densely at the top and sparsely at the bottom along the vertical direction of the material conduit 2, and distributed symmetrically in the horizontal direction; the diameter of the openings 4 is smaller than the catalyst particles.
[0020] Reaction with B 2 o 3 4.7% (wt) nickel-based catalyst, when loading the catalyst, a small amount of quartz sand or ceramic ring (ball) 5 is respectively installed at the upper and lower ends o...
Embodiment 2~3
[0023] Adopt the polymolecular contact catalytic reaction device of embodiment 1 to react, change the hydrogen volume space velocity to be 15000h respectively -1 and 45000h -1 , all the other reaction conditions are the same as in Example 1, and the ethylcyclohexane yield is listed in Table 1.
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