A garlic health care capsule for treating cardiac and cerebral vascular diseases and cancer as well as its preparing method
A technology of cardiovascular and cerebrovascular and ikinin, which is applied in the field of garlic sulfur compounds and its preparation, and can solve the problems of preparing ikinin that have not been seen yet
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0018] Add 100 ml of water to 100 grams of fresh garlic cloves, stir gently for 10 minutes, remove the sediment after centrifugation, and obtain about 120 ml of Alysol aqueous solution, containing about 1 gram of Alysol.
[0019] 20 grams of α-cyclodextrin (water content 8.4%) was ground into powder in a mortar, mixed with the above-mentioned aqueous solution of Alisol, and the white mixture thus obtained was further stirred for two hours to make the mixture uniform. Then, it was dried at room temperature. Grind into a fine powder to obtain 20 g of intermediate product. Dissolve the intermediate product in 6000 ml of water and stir for -5 hours. This slightly hazy mixture was extracted three times with 1 L of diethyl ether. The organic phases were extracted to remove water, mixed together and concentrated in a rotary dryer to remove ether.
[0020] 2 g of the residue thus obtained contained 40% ekinin by H-NMR analysis.
Embodiment 2
[0022] Mix 10 grams of γ-cyclodextrin (water content 10%) with 10 milliliters of water containing about 1 gram of Allison to make a uniform paste. The paste was dried under vacuum at 5°C. 10 g of the dried product thus obtained was pulverized, washed with ether and dried. The complex thus obtained was dissolved in 3000 ml of water and stirred for 5 hours, then extracted by the method of Example 1.
[0023] The final residue is about 0.8 grams and contains 50% ekinin.
Embodiment 3
[0025] The preparation method is the same as in Example 2, but the difference is that 40% Alison is used and ethanol diluted with 90% ethanol (2:1). Drying is carried out in a vacuum at 30°C. The powdery dry product flows in 100 ml of diethyl ether It was boiled for 4 hours. Then dissolved in 300 ml of water and extracted three times with 100 ml of ether. Each extraction was carried out in a fluid boil.
[0026] The 1 gram residue thus obtained contained 70% erkinin, 34% cis erkinin and 36% trans erkinin.
[0027] 98% pure Ekinin can be obtained by dissolving the above residue in water, extracting it with n-heptane and diethyl ether, and preparing it by HPLC.
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap