Method for detecting malaytea scurfpea fruit in malaytea scurfpea fruit containing preparations
A detection method, the technology of psoraleae, which is applied in the direction of measuring devices, material separation, and analysis of materials, can solve the problems of no detection, etc., and achieve the effects of eliminating miscellaneous peaks, flat liquid phase baseline, and accurate and stable results
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Embodiment 1
[0087] Example 1. The quality control method of psoralen in compound eucommia strong waist wine
[0088] 1. Instruments and reagents:
[0089] Instrument: SHIMADZU LC-10AD liquid chromatograph; SPD-M10A detector;
[0090] Chromatographic column: DIAMOSILTMC18 (250mm×4.6mm, 5m);
[0091] Reagents: methanol—chromatographically pure (Tianjin Siyou Biomedical Technology Development Company); water—high-purity water (provided by the National Center for Standard Materials), and the rest of the reagents are analytically pure;
[0092] Reference substance: psoralen reference substance (provided by China Institute for the Control of Biological Products, batch number 0739-200108); isopsoralen reference substance (provided by China Institute for the Control of Biological Products, batch number 0738-9907); both are used for content determination, The purity is 100%.
[0093] 2. Methods and results:
[0094] Chromatographic analysis conditions:
[0095] Mobile phase: methanol-water (4...
Embodiment 2
[0104] Embodiment two. The content assay method of psoralen and different psoralen in the compound psoralen tincture
[0105] 1. Preparation of the test solution: take 10ml of the sample, extract by shaking with ether, evaporate to dryness, add an appropriate amount of methanol to the residue to dissolve, quantitatively transfer it to a measuring bottle, add methanol to 10ml, shake well, and place in the treated medium. On the neutral alumina column, the neutral alumina column is filled with 100-200 mesh neutral alumina, collect the eluate flowing out after passing through the column, filter it with a 0.45 μm microporous membrane, and take the subsequent filtrate to obtain .
[0106] 2. Preparation of reference substance solution: Accurately weigh psoralen and isopsoralen reference substances that were dried under reduced pressure to constant weight, add methanol to prepare 20 mg / ml of psoralen and isopsoralen respectively solution, that is.
[0107] 3. Chromatographic condi...
Embodiment 3
[0109] Embodiment three. The comparison of the results of compound eucommia strong waist wine control example
[0110] The compound eucommia strong waist wine control example is a liquor obtained by deleting the psoralen composition on the basis of the original formula of the compound eucommia strong waist wine.
[0111] 1. Instruments and reagents: the same as in Example 1.
[0112] Reference substance: psoralen reference substance (provided by China Institute for the Control of Biological Products, batch number 0739-200108); isopsoralen reference substance (provided by China Institute for the Control of Biological Products, batch number 0738-9907); both are used for content determination, The purity is 100%.
[0113] 2. Methods and results:
[0114] Chromatographic analysis conditions:
[0115] Mobile phase: methanol-water (40:60);
[0116] Detection wavelength: 246nm;
[0117] Column temperature: 40°C;
[0118] Flow rate: 1ml / min;
[0119] The number of theoretical p...
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