Method for preparing activated carbon electrode material for super capacitor
A technology of supercapacitors and electrode materials, applied in capacitors, electrolytic capacitors, circuits, etc., can solve problems such as high cost and pollution, and achieve the effects of less time, lower manufacturing costs, and a wide range of sources.
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Embodiment 1-5
[0027] The bamboo processing waste is crushed to a length of 1-15mm, dried at 100°C for 2 hours, and irradiated by a radiation source 60 Co, radiation dose rate 2.6×10 3 Gy / h, the irradiation dose is 10000Gy, and then impregnated with 30% potassium hydroxide solution for 24h, the mass ratio of alkali to carbon is 1:1, 2:1, 3:1, 4:1, 5:1 , put it into a microwave oven, microwave at a power of 700W for 12min, take it out and wash it with water, soak it in 10% (wt%) hydrochloric acid for 4h, then wash it to neutral, dry it in an oven at 100°C, and then crush it to -400 mesh to obtain activated carbon . The activated carbon of Examples 1-5 is used as a material to prepare a supercapacitor, using 30% (wt%) KOH aqueous solution as the electrolyte, the charge and discharge voltage range is 0.05-1.0V, and the charge and discharge current is 300mA / g. The corresponding data are shown in the table 1.
Embodiment 6-9
[0029] Crumble the bamboo processing waste to a length of 1-15mm, dry at 110°C for 1.5h, and use a radiation source 60 Co, radiation dose rate 2.6×10 3 Gy / h, the irradiation dose is 30000Gy, and then impregnated with 30% potassium hydroxide solution for 48h, the mass ratio of alkali to carbon is 3:1, put it into a microwave oven, under the power of 200W, 400W, 700W, 900W respectively Microwave for 12 minutes, and the steps after taking it out are the same as in Example 1-5. The corresponding data are shown in Table 2.
Embodiment 10-13
[0031] Crumble the bamboo processing waste to a length of 1-15mm, dry at 120°C for 1h, and use a radiation source 60 Co, radiation dose rate 2.6×10 3 Gy / h, the irradiation dose is 50000Gy, and then impregnated with 30% potassium hydroxide solution for 10h, the mass ratio of alkali to carbon is 3:1, microwave 10min, 12min, 15min, 20min under the power of 700W respectively, and take out the following steps With embodiment 1-5. The corresponding data are shown in Table 3.
[0032]
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