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Preparation method of highly brittle transparent rock-like material specimen

A rock material, brittle technology, applied in the field of preparation of highly brittle transparent rock material specimens with three-dimensional built-in fractures, can solve the problems that affect the experimental rules and the accuracy and authenticity of the results, the high degree of stress concentration in the front edge of the crack, and the degree of brittleness. Without high-level problems, the production process is simple and practical, the heat release is obvious, and the transparency is improved.

Inactive Publication Date: 2015-11-18
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Guo Yanshuang (2011) found an unsaturated polyester resin with a pull-down compression ratio of -50°C that can reach 1 / 5, and the degree of brittleness has improved, but the transparency is poor
Therefore, the brittleness of the materials used by the predecessors is not high.
In addition, due to the unsatisfactory toughening process and the material selection of the crack (metal sheet), the stress concentration in the pre-set crack front area is relatively high, and a certain plastic flow will be generated during the crack growth process, which will affect the experimental rules and results. accuracy and authenticity of
It can be seen that there have been serious shortcomings and deficiencies in the materials used by predecessors for many years.

Method used

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  • Preparation method of highly brittle transparent rock-like material specimen
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Embodiment Construction

[0032] The present invention will be further described below in conjunction with the accompanying drawings and embodiments.

[0033] A method for preparing a highly brittle transparent rock-like material specimen. The raw materials include CY-39 type resin and YS-T31 type curing agent, the mass ratio of the two is 100:34 or the volume ratio is 100:41; the specific steps are:

[0034] (1) Material weighing

[0035] Measure 500ml of CY-39 resin material and 200ml of YS-T31 curing agent.

[0036] (2) Material mixing

[0037] Pour the resin and curing agent into the mixing drum according to the mixing ratio, and stir continuously with a glass rod to make it fully mixed to form a mixture. When stirring, pay attention to the materials at the bottom of the container and the side wall, so that the materials at this part are also fully mixed, and then Put it in a vacuum box for half an hour to remove air bubbles;

[0038] (3) Casting molding and maintenance

[0039] Place the mold ...

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Abstract

The invention discloses a preparation method of a high-brittleness transparent rock material test piece. The preparation method comprises the steps of resin material selection, selection of materials for forming three-dimensional prefabricated built-in elliptical cracks, molding and space location. Raw materials comprise CY-39 type resin and YS-T31 type curing agent, wherein the mass ratio of the CY-39 type resin to the YS-T31 type curing agent is 100: 34, or and the volume ratio of the CY-39 type resin to the YS-T31 type curing agent is 100: 41. The preparation method comprises the following general steps: (1) weighing the materials; (2) mixing the materials; and (3) casting, molding and maintaining. Mica plates with the thickness of 0.12mm are used for forming the prefabricated cracks, and an elliptical steel mold with the corresponding size is used for cutting the mica plates into the required accurate size. The preparation method is characterized in that different parts of a left side face plate and a right side face place of the mold are drilled, a thin line is used for pulling, fixing and connecting the prefabricated cracks, the two ends of the thin line are fixed in holes of the two side face plates so as to play a role of accurate location, and three-dimensional crack test pieces with different numbers of cracks at different angles and different opposite locations are manufactured. The test piece prepared by the method has the characteristics of good brittleness, high transparency, easiness for molding and observing crack extension process and the like.

Description

technical field [0001] The invention relates to a rock-like highly brittle transparent resin material technology, in particular to a preparation method for a highly brittle transparent rock-like material specimen containing three-dimensional built-in cracks. Background technique [0002] The failure process of brittle materials and the evolution law of internal crack propagation have always been the focus and difficulty in the study of solid mechanics. Finding a test material with good brittleness, high transparency and easy presetting of internal cracks is the key point of the experimental research. The brittleness of a material is measured by the ratio of tensile strength to compressive strength. The use of brittle materials can more accurately reflect the stress and deformation characteristics of solids such as rocks. The selection of materials with high transparency can facilitate the observation of the expansion and evolution process of internal cracks. [0003] So f...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L101/00B29C39/26
Inventor 朱维申付金伟李邦翔
Owner SHANDONG UNIV
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