Heterometallic complex of carboxylate Schiff base iron zinc and preparation method thereof
A technology of Schiff base iron zinc and Schiff base iron, which is applied in the chemical field, can solve the problems of heterometal complex research unreported, and achieve the effects of strong photocatalytic degradation ability, good gas adsorption ability, and stable product performance
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[0027] Mix 3-methyl-5-carboxysalicylaldehyde and diaminocyclohexane with tetrahydrofuran as a solvent and stir at room temperature. The molar ratio is 2:1; THF add-on is 50-100 times of the corresponding 3-methyl-5-carboxy salicylaldehyde molar weight, obtains H 4 L ligand; H 4 L 1mmol and ferric chloride hexahydrate 1mmol were stirred in 80mL of ethanol solution for 7 hours, and left still under vacuum to obtain a dark red solid, which was dispersed in water and filtered, and dried in air to obtain H 2 (Fe-L) Cl complex; Take zinc chloride 0.03mmol and H 2 (Fe-L)Cl 0.015mmol, placed in a mixed solvent of dimethylformamide (1mL) / ethanol (1mL) / water (2mL), the mixture was placed in a 10mL glass bottle, and kept at 90°C for 96 hours, and then slowly lowered to room temperature at a rate of 10°C per hour. A red needle-like crystal carboxylic acid Schiff base iron-zinc heterometal complex was obtained with a yield of 25%.
[0028] The main infrared absorption peaks are: 3418(m...
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