A kind of preparation method of water-based anticorrosion coating
An anti-corrosion coating, water-based technology, applied in anti-corrosion coatings, epoxy resin coatings, coatings, etc., can solve problems such as high water conductivity, metal corrosion, flash corrosion, etc., achieve good weather resistance and corrosion resistance, and avoid agglomeration , the effect of increasing the cross-linking density
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[0026] 1. Preparation of N-carboxyethyl chitosan:
[0027] Add 4.0g chitosan (molecular weight less than 50,000) to 200mL water containing 2.8mL acrylic acid, and keep stirring for 2 days at 50°C. After the reaction is completed, add 1mol / L NaOH solution to the reaction mixture, adjust the pH value of the solution to 10, and convert all the carboxylic acids into sodium salts. Pour the mixed solution into acetone for reprecipitation, then dialyze in aqueous solution (dialysis membrane molecular weight cut-off is 8000-12000g / mol), remove unreacted acrylic acid. After two days of dialysis, lyophilization yielded 3.6 g of N-carboxyethyl chitosan.
[0028] 2. Preparation of chitosan / nano zinc oxide composite material:
[0029] Add 3.6 g of the obtained N-carboxyethyl chitosan into 300 mL of deionized water, stir vigorously at room temperature for 0.5 h, and fully dissolve to obtain a water-soluble chitosan solution. The above-mentioned water-soluble chitosan solution and nano-zi...
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